Science.gov

Sample records for zirconium 97

  1. Zirconium

    USGS Publications Warehouse

    Bedinger, G.M.

    2013-01-01

    Zirconium is the 20th most abundant element in the Earth’s crust. It occurs in a variety of rock types and geologic environments but most often in igneous rocks in the form of zircon (ZrSiO4). Zircon is recovered as a coproduct of the mining and processing of heavy mineral sands for the titanium minerals ilmenite and rutile. The sands are formed by the weathering and erosion of rock containing zircon and titanium heavy minerals and their subsequent concentration in sedimentary systems, particularly in coastal environments. A small quantity of zirconium, less than 10 kt/a (11,000 stpy), compared with total world production of 1.4 Mt (1.5 million st) in 2012, was derived from the mineral baddeleyite (ZrO2), produced from a single source in Kovdor, Russia.

  2. Colorimetric determination of zirconium in antiperspirant aerosols.

    PubMed

    Beavin, P

    1976-07-01

    A rapid direct dilution procedure for the estimation of soluble zirconium and a fusion procedure for the determination of total zirconium (soluble and insoluble forms) in cream base concentrates prepared from antiperspirant aerosols are described. The direct dilution procedure involves extraction of soluble zirconium with HCl (55 + 45). The filtered extract is reacted with alizarin red S to form a stable colored complex which is measured spectrophotometrically. The fusion procedure involves ashing the aerosol concentrate followed by fusion of the ash with potassium pyrosulfate to form an acid-soluble melt. Zirconium is precipitated from solution as the hydroxide and washed to eliminate interfering ions, particularly sulfate. After redissolving in HCl (55 + 45) and reacting with alizarin red S, total zirconium is measured. Zirconyl chloride octahydrate, assayed gravimetrically by hydroxide precipitation and conversion to the oxide, is used as the zirconium reference standard. Concentration range of zirconium measured was 200-500 mug/100 ml. Recoveries of standard zirconium added to commercial aerosols labeled to contain aluminum and zirconyl hydroxychlorides ranged from 97 to 101% by the fusion procedure. Analysis of these aerosols by direct dilution gave generally slightly lower results than by fusion. It is recommended that the procedures be collaboratively studied after further testing of their general applicability to a variety of drugs and cosmetics. PMID:939750

  3. PLUTONIUM-ZIRCONIUM ALLOYS

    DOEpatents

    Schonfeld, F.W.; Waber, J.T.

    1960-08-30

    A series of nuclear reactor fuel alloys consisting of from about 5 to about 50 at.% zirconium (or higher zirconium alloys such as Zircaloy), balance plutonium, and having the structural composition of a plutonium are described. Zirconium is a satisfactory diluent because it alloys readily with plutonium and has desirable nuclear properties. Additional advantages are corrosion resistance, excellent fabrication propenties, an isotropie structure, and initial softness.

  4. Studies in zirconium oxidation

    NASA Technical Reports Server (NTRS)

    Draley, J. E.; Drunen, C. J.; Levitan, J.

    1968-01-01

    Study provides insight into the oxidation mechanism of zirconium by combining electrical measurements with oxidation data. The measurement of electrical potential across growing scale on zirconium and the determination of conventional weight-change oxidation data were carried out at 550, 700, and 800 degrees C.

  5. Laser ablated zirconium plasma: A source of neutral zirconium

    SciTech Connect

    Yadav, Dheerendra; Thareja, Raj K.

    2010-10-15

    The authors report spectroscopic investigations of laser produced zirconium (Zr) plasma at moderate laser fluence. At low laser fluence the neutral zirconium species are observed to dominate over the higher species of zirconium. Laser induced fluorescence technique is used to study the velocity distribution of ground state neutral zirconium species. Two-dimensional time-resolved density distributions of ground state zirconium is mapped using planner laser induced fluorescence imaging and total ablated mass of neutral zirconium atoms is estimated. Temporal and spatial evolutions of electron density and temperature are discussed by measuring Stark broadened profile and ratio of intensity of emission lines, respectively.

  6. SEPARATING HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Lister, B.A.J.; Duncan, J.F.

    1956-08-21

    A dilute aqueous solution of zirconyl chloride which is 1N to 2N in HCl is passed through a column of a cation exchange resin in acid form thereby absorbing both zirconium and associated hafnium impurity in the mesin. The cation exchange material with the absorbate is then eluted with aqueous sulfuric acid of a O.8N to 1.2N strength. The first portion of the eluate contains the zirconium substantially free of hafnium.

  7. ZIRCONIUM-CLADDING OF THORIUM

    DOEpatents

    Beaver, R.J.

    1961-11-21

    A method of cladding thorium with zirconium is described. The quality of the bond achieved between thorium and zirconium by hot-rolling is improved by inserting and melting a thorium-zirconium alloy foil between the two materials prior to rolling. (AEC)

  8. Electroless deposition process for zirconium and zirconium alloys

    DOEpatents

    Donaghy, R. E.; Sherman, A. H.

    1981-08-18

    A method is disclosed for preventing stress corrosion cracking or metal embrittlement of a zirconium or zirconium alloy container that is to be coated on the inside surface with a layer of a metal such as copper, a copper alloy, nickel, or iron and used for holding nuclear fuel material as a nuclear fuel element. The zirconium material is etched in an etchant solution, desmutted mechanically or ultrasonically, oxidized to form an oxide coating on the zirconium, cleaned in an aqueous alkaline cleaning solution, activated for electroless deposition of a metal layer and contacted with an electroless metal plating solution. This method provides a boundary layer of zirconium oxide between the zirconium container and the metal layer. 1 fig.

  9. Electroless deposition process for zirconium and zirconium alloys

    DOEpatents

    Donaghy, Robert E.; Sherman, Anna H.

    1981-01-01

    A method is disclosed for preventing stress corrosion cracking or metal embrittlement of a zirconium or zirconium alloy container that is to be coated on the inside surface with a layer of a metal such as copper, a copper alloy, nickel, or iron and used for holding nuclear fuel material as a nuclear fuel element. The zirconium material is etched in an etchant solution, desmutted mechanically or ultrasonically, oxidized to form an oxide coating on the zirconium, cleaned in an aqueous alkaline cleaning solution, activated for electroless deposition of a metal layer and contacted with an electroless metal plating solution. This method provides a boundary layer of zirconium oxide between the zirconium container and the metal layer.

  10. M97

    NASA Astrophysics Data System (ADS)

    Murdin, P.

    2000-11-01

    M97 is a planetary nebula in Ursa Major, lying just south of the bowl of the Big Dipper, 2.25 degrees from Beta Ursae Majoris. This nebula was discovered in February 1781 by Mechain, who noted it was difficult to see; modern observers estimate it as either tenth or eleventh magnitude, placing it among the faintest objects in Messier's catalog. Lord Rosse in 1848 named it the OWL NEBULA because it...

  11. Synthesis of micro-dispersed zirconium oxide for glass manufacturing

    NASA Astrophysics Data System (ADS)

    Goncharuk, V.; Starodubtsev, P.; Maslennikova, I.

    2016-01-01

    A rather simple and original method for processing of zirconium-containing raw material form Algoma deposit (Khabarovsk region, Russia) was suggested, which comprised fluorination of the initial sample with a diluted HF solution followed by the thermal treatment of fluorination products and pyrohydrolysis of zirconium tetrafluoride. Water vapors obtained by hydrogen and oxygen burning in a hydrogen torch as well as by simple evaporation were used for pyrohydrolysis. The feed rate of the water and its temperature were regulated. The temperature of water vapors reached 800-1200 °C. Zirconium dioxide with a purity of 99.97% or more and a dispersity of 0.1 gm or less was synthesized.

  12. Plasma arc melting of zirconium

    SciTech Connect

    Tubesing, P.K.; Korzekwa, D.R.; Dunn, P.S.

    1997-12-31

    Zirconium, like some other refractory metals, has an undesirable sensitivity to interstitials such as oxygen. Traditionally, zirconium is processed by electron beam melting to maintain minimum interstitial contamination. Electron beam melted zirconium, however, does not respond positively to mechanical processing due to its large grain size. The authors undertook a study to determine if plasma arc melting (PAM) technology could be utilized to maintain low interstitial concentrations and improve the response of zirconium to subsequent mechanical processing. The PAM process enabled them to control and maintain low interstitial levels of oxygen and carbon, produce a more favorable grain structure, and with supplementary off-gassing, improve the response to mechanical forming.

  13. Process for purifying zirconium sponge

    SciTech Connect

    Abodishish, H.A.M.; Kimball, L.S.

    1992-03-31

    This patent describes a Kroll reduction process wherein a zirconium sponge contaminated with unreacted magnesium and by-product magnesium chloride is produced as a regulus, a process for purifying the zirconium sponge. It comprises: distilling magnesium and magnesium chloride from: a regulus containing a zirconium sponge and magnesium and magnesium chloride at a temperature above about 800{degrees} C and at an absolute pressure less than about 10 mmHg in a distillation vessel to purify the zirconium sponge; condensing the magnesium and the magnesium chloride distilled from the zirconium sponge in a condenser; and then backfilling the vessel containing the zirconium sponge and the condenser containing the magnesium and the magnesium chloride with a gas; recirculating the gas between the vessel and the condenser to cool the zirconium sponge from above about 800{degrees} C to below about 300{degrees} C; and cooling the recirculating gas in the condenser containing the condensed magnesium and the condensed magnesium chloride as the gas cools the zirconium sponge to below about 300{degrees} C.

  14. SEPARATING HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Lister, B.A.J.; Duncan, J.F.; Hutcheon, J.M.

    1956-08-21

    Substantially complete separation of zirconium from hafnium may be obtained by elution of ion exchange material, on which compounds of the elements are adsorbed, with an approximately normal solution of sulfuric acid. Preferably the acid concentration is between 0.8 N amd 1.2 N, amd should not exceed 1.5 N;. Increasing the concentration of sulfate ion in the eluting solution by addition of a soluble sulfate, such as sodium sulfate, has been found to be advantageous. The preferred ion exchange materials are sulfonated polystyrene resins such as Dowex 50,'' and are preferably arranged in a column through which the solutions are passed.

  15. ZIRCONIUM PHOSPHATE ADSORPTION METHOD

    DOEpatents

    Russell, E.R.; Adamson, A.S.; Schubert, J.; Boyd, G.E.

    1958-11-01

    A method is presented for separating plutonium values from fission product values in aqueous acidic solution. This is accomplished by flowing the solutlon containing such values through a bed of zirconium orthophosphate. Any fission products adsorbed can subsequently be eluted by washing the column with a solution of 2N HNO/sub 3/ and O.lN H/sub 3/PO/sub 4/. Plutonium values may subsequently be desorbed by contacting the column with a solution of 7N HNO/sub 3/ .

  16. Modification in band gap of zirconium complexes

    NASA Astrophysics Data System (ADS)

    Sharma, Mayank; Singh, J.; Chouhan, S.; Mishra, A.; Shrivastava, B. D.

    2016-05-01

    The optical properties of zirconium complexes with amino acid based Schiff bases are reported here. The zirconium complexes show interesting stereo chemical features, which are applicable in organometallic and organic synthesis as well as in catalysis. The band gaps of both Schiff bases and zirconium complexes were obtained by UV-Visible spectroscopy. It was found that the band gap of zirconium complexes has been modified after adding zirconium compound to the Schiff bases.

  17. SEPARATION OF HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Overholser, L.B.; Barton, C.J. Sr.; Ramsey, J.W.

    1960-05-31

    The separation of hafnium impurities from zirconium can be accomplished by means of organic solvent extraction. The hafnium-containing zirconium feed material is dissolved in an aqueous chloride solution and the resulting solution is contacted with an organic hexone phase, with at least one of the phases containing thiocyanate. The hafnium is extracted into the organic phase while zirconium remains in the aqueous phase. Further recovery of zirconium is effected by stripping the onganic phase with a hydrochloric acid solution and commingling the resulting strip solution with the aqueous feed solution. Hexone is recovered and recycled by means of scrubbing the onganic phase with a sulfuric acid solution to remove the hafnium, and thiocyanate is recovered and recycled by means of neutralizing the effluent streams to obtain ammonium thiocyanate.

  18. Charge transfer in zirconium films

    NASA Astrophysics Data System (ADS)

    Mel'Nichuk, B. L.; Stasyuk, Z. V.

    1991-12-01

    In superhigh-vacuum conditions (residual gas pressure less than 10-8 Pa), electro-conductive dimensional phenomena, the Hall constant, and the absolute differential thermoemf of zirconium films are investigated. The experimental results are analyzed within the framework of current model concepts regarding volume, surface, and grain-boundary scattering of charge carriers (the Mayadas-Schatzkes and Tel'e-Tosser-Pichard models). The charge-transfer parameters in zirconium are determined.

  19. Fine-grained zirconium-base material

    DOEpatents

    Van Houten, G.R.

    1974-01-01

    A method is described for making zirconium with inhibited grain growth characteristics, by the process of vacuum melting the zirconium, adding 0.3 to 0.5% carbon, stirring, homogenizing, and cooling. (Official Gazette)

  20. Ablation Resistant Zirconium and Hafnium Ceramics

    NASA Technical Reports Server (NTRS)

    Bull, Jeffrey (Inventor); White, Michael J. (Inventor); Kaufman, Larry (Inventor)

    1998-01-01

    High temperature ablation resistant ceramic composites have been made. These ceramics are composites of zirconium diboride and zirconium carbide with silicon carbide, hafnium diboride and hafnium carbide with silicon carbide and ceramic composites which contain mixed diborides and/or carbides of zirconium and hafnium. along with silicon carbide.

  1. Zirconium and hafnium in meteorites

    NASA Technical Reports Server (NTRS)

    Ehmann, W. D.; Chyi, L. L.

    1974-01-01

    The abundances of zirconium and hafnium have been determined in nine stony meteorites by a new, precise neutron-activation technique. The Zr/Hf abundance ratios for the chondrites vary in a rather narrow range, consistent with previously published observations from our group. Replicate analyses of new, carefully selected clean interior samples of the Cl chondrite Orgueil yield mean zirconium and hafnium abundances of 5.2 and 0.10 ppm, respectively. These abundances are lower than we reported earlier for two Cl chondrite samples which we now suspect may have suffered contamination. The new Cl zirconium and hafnium abundances are in closer agreement with predictions based on theories of nucleosynthesis than the earlier data.

  2. PROCESS OF DISSOLVING ZIRCONIUM ALLOYS

    DOEpatents

    Shor, R.S.; Vogler, S.

    1958-01-21

    A process is described for dissolving binary zirconium-uranium alloys where the uranium content is about 2%. In prior dissolution procedures for these alloys, an oxidizing agent was added to prevent the precipitation of uranium tetrafluoride. In the present method complete dissolution is accomplished without the use of the oxidizing agent by using only the stoichiometric amount or slight excess of HF required by the zirconium. The concentration of the acid may range from 2M to 10M and the dissolution is advatageously carried out at a temperature of 80 deg C.

  3. Thermodynamic properties of zirconium disulfide

    SciTech Connect

    Volovik, L.S.; Kovalevskaya, E.I.; Litvinenko, V.F.

    1986-02-01

    This paper uses a method of comparative calculation -- double comparison -for the quantitative evaluation of the themodynamic characteristics of zirconium disulfide. The method enables one to apply known characteristics of compounds of the given or an adjacent group to analogous compounds of elements. The enthalpy of zirconium disulfide was determined by a formula and the calculation was carried out on the basis of data on the enthalpy of hafnium, niobium, and tantalum disulfides measured by the mixing method in the temperature range 500-1800 K.

  4. Electrochemical process for zirconium alloy recycling

    SciTech Connect

    Snyder, T.S.; Stoltz, R.A.; Zuckerbrod, D.

    1990-05-08

    This patent describes a method of separating nickel from zirconium for recycling nickel-containing zirconium alloy. It comprises: placing the nickel-containing zirconium in a molten alt bath at 500{degrees} to about 722{degrees} C. with the molten salt in the molten salt bath consisting essentially of a mixture of 0 to about 46.5 mole % lithium fluoride, about 11.5 to about 40 mole % sodium fluoride and potassium fluoride to produce a molten salt bath containing dissolved zirconium and dissolved nickel; electrochemically plating the nickel from the molten salt bath at a voltage sufficient to plate nickel but less than the voltage to plate zirconium to provide an essentially nickel-free molten salt bath; and electrochemically plating the zirconium from the essentially nickel-free molten salt bath to provide an essentially nickel-free zirconium.

  5. SEPARATION PROCESS FOR ZIRCONIUM AND COMPOUNDS THEREOF

    DOEpatents

    Crandall, H.W.; Thomas, J.R.

    1959-06-30

    The separation of zirconium from columbium, rare earths, yttrium and the alkaline earth metals, such mixtures of elements occurring in zirconium ores or neutron irradiated uranium is described. According to the invention a suitable separation of zirconium from a one normal acidic aqueous solution containing salts, nitrates for example, of tetravalent zirconium, pentavalent columbium, yttrium, rare earths in the trivalent state and alkaline earths can be obtained by contacting the aqueous solution with a fluorinated beta diketonc alone or in an organic solvent solution, such as benzene, to form a zirconium chelate compound. When the organic solvent is present the zirconium chelate compound is directly extracted; otherwise it is separated by filtration. The zirconium may be recovered from contacting the organic solvent solution containing the chelated compound by back extraction with either an aqueous hydrofluoric acid or an oxalic acid solution.

  6. PROCESS OF PREPARING ZIRCONIUM OXYCHLORIDE

    DOEpatents

    Wilhelm, H.A.; Andrews, M.L.

    1960-06-28

    A process is given for preparing zirconyl chloride by mixing solid zirconyl chloride octahydrate and solid zirconium tetrachloride at room temperature whereby both chlorides are converted to zirconyl chloride trinydrate and hydrogen chloride is formed and volatilized by the reaction heat.

  7. Spectrophotometric determination of zirconium with xylenol orange

    SciTech Connect

    Antepenko, R J

    1982-05-14

    High purity hydride forming metal films are used as hydrogen isotope occluders and function as electrodes in neutron generator tubes. This use of zirconium occluder films requires reliable analytical methods for routine determination of the zirconium film weight in a production environment. In this study, a spectrophotometric method was evaluated for the determination of zirconium films. The method is based upon the formation of a highly colored zirconium complex with xylenol orange in a dilute perchloric acid medium. Dilute hydrofluoric acid is used in this procedure to selectively dissolve the zirconium film off the substrate. A perchloric acid fuming step is used to remove hydrofluoric acid from the solution. The zirconium solutions are depolymerized before complex formation by heating in 2 N perchloric acid. The zirconium complex exhibits a maximum absorbance in 0.2 to 0.3 M perchloric acid at a wavelength of 531 nanometers. Beer's law is obeyed for zirconium concentrations through 2.1 parts per million. Molybdenum, at concentrations equal to zirconium, does not interfere with the xylenol orange method.

  8. Process for producing zirconium based granules

    SciTech Connect

    Jade, S.S.

    1990-05-22

    This patent describes a process for the production f amorphous zirconium based granules. It comprises: adding about 2--15 wt % of a suitable phase stabilizer to an aqueous solutio, based upon the total weight of ZrO{sub 2} in solution, to produce an aqueous solution having a pH in the range of about 4 to 7 comprising a zirconium based complex and phase stabilizer and thereafter; drying the aqueous solution comprising the zirconium based complex and the phase stabilizer at a temperature below about 180{degrees} C. for a time sufficient to evaporate the aqueous solution thereby forming amorphous zirconium based granules containing the phase stabilizer.

  9. Method for preparing hydrous zirconium oxide gels and spherules

    DOEpatents

    Collins, Jack L.

    2003-08-05

    Methods for preparing hydrous zirconium oxide spherules, hydrous zirconium oxide gels such as gel slabs, films, capillary and electrophoresis gels, zirconium monohydrogen phosphate spherules, hydrous zirconium oxide spherules having suspendable particles homogeneously embedded within to form a composite sorbent, zirconium monohydrogen phosphate spherules having suspendable particles of at least one different sorbent homogeneously embedded within to form a composite sorbent having a desired crystallinity, zirconium oxide spherules having suspendable particles homogeneously embedded within to form a composite, hydrous zirconium oxide fiber materials, zirconium oxide fiber materials, hydrous zirconium oxide fiber materials having suspendable particles homogeneously embedded within to form a composite, zirconium oxide fiber materials having suspendable particles homogeneously embedded within to form a composite and spherules of barium zirconate. The hydrous zirconium oxide spherules and gel forms prepared by the gel-sphere, internal gelation process are useful as inorganic ion exchangers, catalysts, getters and ceramics.

  10. DISSOLUTION OF ZIRCONIUM-CONTAINING FUEL ELEMENTS

    DOEpatents

    Horn, F.L.

    1961-12-12

    Uranium is recovered from spent uranium fuel elements containing or clad with zirconium. These fuel elements are placed in an anhydrous solution of hydrogen fluoride and nitrogen dioxide. Within this system uranium forms a soluble complex and zirconium forms an insoluble complex. The uranium can then be separated, treated, and removed from solution as uranium hexafluoride. (AEC)

  11. Method of making crack-free zirconium hydride

    DOEpatents

    Sullivan, Richard W.

    1980-01-01

    Crack-free hydrides of zirconium and zirconium-uranium alloys are produced by alloying the zirconium or zirconium-uranium alloy with beryllium, or nickel, or beryllium and scandium, or nickel and scandium, or beryllium and nickel, or beryllium, nickel and scandium and thereafter hydriding.

  12. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  13. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  14. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  15. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  16. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  17. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE... zirconium or zirconium/nickel alloys by magnesium reduction of zirconium dioxide are exempt from...

  18. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE... zirconium or zirconium/nickel alloys by magnesium reduction of zirconium dioxide are exempt from...

  19. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE... zirconium or zirconium/nickel alloys by magnesium reduction of zirconium dioxide are exempt from...

  20. URANIUM DECONTAMINATION WITH RESPECT TO ZIRCONIUM

    DOEpatents

    Vogler, S.; Beederman, M.

    1961-05-01

    A process is given for separating uranium values from a nitric acid aqueous solution containing uranyl values, zirconium values and tetravalent plutonium values. The process comprises contacting said solution with a substantially water-immiscible liquid organic solvent containing alkyl phosphate, separating an organic extract phase containing the uranium, zirconium, and tetravalent plutonium values from an aqueous raffinate, contacting said organic extract phase with an aqueous solution 2M to 7M in nitric acid and also containing an oxalate ion-containing substance, and separating a uranium- containing organic raffinate from aqueous zirconium- and plutonium-containing extract phase.

  1. Penta-zirconium copper tribismuth.

    PubMed

    Balinska, Agnieszka; Tarasiuk, Ivan; Pavlyuk, Volodymyr

    2013-01-01

    Penta-zirconium copper tribismuth, Zr5CuBi3, crystallizes in the hexa-gonal Hf5CuSn3 structure type. The asymmetric unit contains two Zr sites (site symmetries 3.2 and m2m), one Cu site (site symmetry 3.m) and one Bi site (site symmetry m2m). The environment of the Bi atoms is a tetra-gonal anti-prism with one added atom and a coordination number (CN) of 9. The polyhedron around the Zr1 atom is a defective cubo-octa-hedron with CN = 11. The bicapped hexa-gonal anti-prism (CN = 14) is typical for Zr2 atoms. The Cu atom is enclosed in a eight-vertex polyhedron (octa-hedron with two centered faces). The metallic type of bonding was indicated by an analysis of the inter-atomic distances and electronic structure calculation data.

  2. Production of nuclear grade zirconium: A review

    NASA Astrophysics Data System (ADS)

    Xu, L.; Xiao, Y.; van Sandwijk, A.; Xu, Q.; Yang, Y.

    2015-11-01

    Zirconium is an ideal material for nuclear reactors due to its low absorption cross-section for thermal neutrons, whereas the typically contained hafnium with strong neutron-absorption is very harmful for zirconium as a fuel cladding material. This paper provides an overview of the processes for nuclear grade zirconium production with emphasis on the methods of Zr-Hf separation. The separation processes are roughly classified into hydro- and pyrometallurgical routes. The known pyrometallurgical Zr-Hf separation methods are discussed based on the following reaction features: redox characteristics, volatility, electrochemical properties and molten salt-metal equilibrium. In the present paper, the available Zr-Hf separation technologies are compared. The advantages and disadvantages as well as future directions of research and development for nuclear grade zirconium production are discussed.

  3. [Toxicity and pharmacokinetics of zirconium oxychloride in mice and rats].

    PubMed

    Delongeas, J L; Burnel, D; Netter, P; Grignon, M; Mur, J M; Royer, R J; Grignon, G

    1983-01-01

    The experimental toxicity of zirconium compounds is examined in the Mouse (acute toxicity) and in the Rat (short time toxicity). The absorption, the distribution and the elimination of zirconium are evaluated by zirconium cation assay in some biological fluids and tissues. After a single oral dose, zirconium oxyd is not toxic, zirconium oxychlorure slightly toxic and zirconium chlorure moderately toxic. At certain concentrations, cerebral and pulmonary disorders are observed, particularly with zirconium chlorure. In considering molar toxicity, the studied zirconium compounds are more toxic than certain aluminium salts mentioned in the literature. The zirconium oxychlorure doesn't influence the growth curve after iterative administrations (0.23 g zirconium/kg/day). Only a weak fraction of administered zirconium is absorbed and is electively fixed in the ovaries, in a lesser degree in the lung and the bone. In the ovary the zirconium induces vascular variation (hypervascularization) which appear one month after the end of the treatment. The absorbed zirconium is eliminated by the urinary tract. The fecal elimination can be essentially explained by an important quantity of non absorbed zirconium. PMID:6672464

  4. METHOD OF IMPROVING CORROSION RESISTANCE OF ZIRCONIUM

    DOEpatents

    Shannon, D.W.

    1961-03-28

    An improved intermediate rinse for zirconium counteracts an anomalous deposit that often results in crevices and outof-the-way places when ordinary water is used to rinse away a strong fluoride etching solution designed to promote passivation of the metal. The intermediate rinse, which is used after the etching solution and before the water, is characterized by a complexing agent for fluoride ions such as aluminum or zirconium nitrates or chlorides.

  5. DISSOLUTION OF ZIRCONIUM AND ALLOYS THEREFOR

    DOEpatents

    Swanson, J.L.

    1961-07-11

    The dissolution of zirconium cladding in a water solution of ammonium fluoride and ammonium nitrate is described. The method finds particular utility in processing spent fuel elements for nuclear reactors. The zirconium cladding is first dissolved in a water solution of ammonium fluoride and ammonium nitrate; insoluble uranium and plutonium fiuorides formed by attack of the solvent on the fuel materiai of the fuel element are then separated from the solution, and the fuel materiai is dissolved in another solution.

  6. ZIRCONIUM OXIDE NANOSTRUCTURES PREPARED BY ANODIC OXIDATION

    SciTech Connect

    Dang, Y. Y.; Bhuiyan, M.S.; Paranthaman, M. P.

    2008-01-01

    Zirconium oxide is an advanced ceramic material highly useful for structural and electrical applications because of its high strength, fracture toughness, chemical and thermal stability, and biocompatibility. If highly-ordered porous zirconium oxide membranes can be successfully formed, this will expand its real-world applications, such as further enhancing solid-oxide fuel cell technology. Recent studies have achieved various morphologies of porous zirconium oxide via anodization, but they have yet to create a porous layer where nanoholes are formed in a highly ordered array. In this study, electrochemical methods were used for zirconium oxide synthesis due to its advantages over other coating techniques, and because the thickness and morphology of the ceramic fi lms can be easily tuned by the electrochemical parameters, such as electrolyte solutions and processing conditions, such as pH, voltage, and duration. The effects of additional steps such as pre-annealing and post-annealing were also examined. Results demonstrate the formation of anodic porous zirconium oxide with diverse morphologies, such as sponge-like layers, porous arrays with nanoholes ranging from 40 to 75 nm, and nanotube layers. X-ray powder diffraction analysis indicates a cubic crystallographic structure in the zirconium oxide. It was noted that increased voltage improved the ability of the membrane to stay adhered to the zirconium substrate, whereas lower voltages caused a propensity for the oxide fi lm to fl ake off. Further studies are needed to defi ne the parameters windows that create these morphologies and to investigate other important characteristics such as ionic conductivity.

  7. Zirconium Oxide Nanostructures Prepared by Anodic Oxidation

    SciTech Connect

    Dang, Ying Yi; Bhuiyan, Md S; Paranthaman, Mariappan Parans

    2008-01-01

    Zirconium oxide is an advanced ceramic material highly useful for structural and electrical applications because of its high strength, fracture toughness, chemical and thermal stability, and biocompatibility. If highly-ordered porous zirconium oxide membranes can be successfully formed, this will expand its real-world applications, such as further enhancing solid-oxide fuel cell technology. Recent studies have achieved various morphologies of porous zirconium oxide via anodization, but they have yet to create a porous layer where nanoholes are formed in a highly ordered array. In this study, electrochemical methods were used for zirconium oxide synthesis due to its advantages over other coating techniques, and because the thickness and morphology of the ceramic films can be easily tuned by the electrochemical parameters, such as electrolyte solutions and processing conditions, such as pH, voltage, and duration. The effects of additional steps such as pre-annealing and post-annealing were also examined. Results demonstrate the formation of anodic porous zirconium oxide with diverse morphologies, such as sponge-like layers, porous arrays with nanoholes ranging from 40 to 75 nm, and nanotube layers. X-ray powder diffraction analysis indicates a cubic crystallographic structure in the zirconium oxide. It was noted that increased voltage improved the ability of the membrane to stay adhered to the zirconium substrate, whereas lower voltages caused a propensity for the oxide film to flake off. Further studies are needed to define the parameters windows that create these morphologies and to investigate other important characteristics such as ionic conductivity.

  8. Electrochemical-metallothermic reduction of zirconium in molten salt solutions

    SciTech Connect

    McLaughlin, D.F.; Talko, F.

    1990-05-08

    This patent describes a method for separating hafnium from zirconium of the type wherein a feed containing zirconium and hafnium chlorides is prepared from zirconium-hafnium chloride and the feed is introduced into a distillation column, which distillation column has a reboiler connected at the bottom and a reflux condenser connected at the top and wherein a hafnium chloride enriched stream is taken from the top of the column and a zirconium enriched chloride stream is taken from the bottom of the column. It comprises: reducing the zirconium enriched chloride stream taken from the distillation column to metal by electrochemically reducing an alkaline earth metal in a molten salt bath with the molten salt in the molten salt bath consisting essentially of a mixture of at least one alkali metal chloride and at least one alkaline earth metal chloride and zirconium chloride, with the reduced alkaline earth metal reacting with the zirconium chloride to produce zirconium metal and alkaline earth metal chloride.

  9. Zirconium: biomedical and nephrological applications.

    PubMed

    Lee, David B N; Roberts, Martin; Bluchel, Christian G; Odell, Ross A

    2010-01-01

    Recent years have witnessed a rapid increase in the use of zirconium (Zr)-containing compounds in artificial internal organs. Examples include dental implants and other restorative practices, total knee and hip replacement, and middle-ear ossicular chain reconstruction. In nephrological practice, Zr-containing sorbents have been used in hemofiltration, hemodialysis, peritoneal dialysis, and in the design and construction of wearable artificial kidneys. Zr compounds continue to be widely and extensively used in deodorant and antiperspirant preparations. In the public health arena, Zr compounds have been studied or used in controlling phosphorus pollution and in the reclamation of poison and bacteria-contaminated water. Experimental and clinical studies support the general consensus that Zr compounds are biocompatible and exhibit low toxicity. Reports on possible Zr-associated adverse reactions are rare and, in general, have not rigorously established a cause-and-effect relationship. Although publications on the use of Zr compounds have continued to increase in recent years, reports on Zr toxicity have virtually disappeared from the medical literature. Nevertheless, familiarity with, and continued vigilant monitoring of, the use of these compounds are warranted. This article provides an updated review on the biomedical use of Zr compounds.

  10. Synthesis of zirconium oxide nanoparticle by sol-gel technique

    SciTech Connect

    Lim, H. S.; Ahmad, A.; Hamzah, H.

    2013-11-27

    Zirconium oxide nanoparticle is synthesized using sol-gel technique. Various mole ratio of ammonia solution and nitric acid relative to zirconium propoxide is added in the reaction to study the effect on the crystallinity and particle size on zirconium oxide particle. Zirconium oxide synthesized with nitric acid have the smallest particle size under FESEM image and show the increasing formation of crystalline tetragonal phase under XRD diffractogram.

  11. The chemical vapor deposition of zirconium carbide onto ceramic substrates

    SciTech Connect

    Glass, John A, Jr.; Palmisiano, Nick, Jr.; Welsh, R. Edward

    1999-07-01

    Zirconium carbide is an attractive ceramic material due to its unique properties such as high melting point, good thermal conductivity, and chemical resistance. The controlled preparation of zirconium carbide films of superstoichiometric, stoichiometric, and substoichiometric compositions has been achieved utilizing zirconium tetrachloride and methane precursor gases in an atmospheric pressure high temperature chemical vapor deposition system.

  12. Processing fissile material mixtures containing zirconium and/or carbon

    DOEpatents

    Johnson, Michael Ernest; Maloney, Martin David

    2013-07-02

    A method of processing spent TRIZO-coated nuclear fuel may include adding fluoride to complex zirconium present in a dissolved TRIZO-coated fuel. Complexing the zirconium with fluoride may reduce or eliminate the potential for zirconium to interfere with the extraction of uranium and/or transuranics from fission materials in the spent nuclear fuel.

  13. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  14. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 31 2011-07-01 2011-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  15. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  16. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  17. 40 CFR 721.10708 - Zirconium substituted heteropolycyclic (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium substituted heteropolycyclic... Specific Chemical Substances § 721.10708 Zirconium substituted heteropolycyclic (generic). (a) Chemical... as zirconium substituted heteropolycyclic (PMN P-13-152) is subject to reporting under this...

  18. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  19. Zirconium granuloma resulting from an aluminum zirconium complex: a previously unrecognized agent in the development of hypersensitivity granulomas.

    PubMed

    Skelton, H G; Smith, K J; Johnson, F B; Cooper, C R; Tyler, W F; Lupton, G P

    1993-05-01

    Zirconium compounds have been associated with the development of hypersensitivity granulomas. However, aluminum zirconium complexes have not previously been shown to induce sensitization. We present the clinical and histologic findings of a case in which a patient developed an acute hypersensitivity reaction to an aluminum zirconium complex. PMID:8491884

  20. Zirconium modified nickel-copper alloy

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D. (Inventor)

    1977-01-01

    An improved material for use in a catalytic reactor which reduces nitrogen oxide from internal combustion engines is in the form of a zirconium-modified, precipitation-strengthened nickel-copper alloy. This material has a nominal composition of Ni-30 Cu-0.2 Zr and is characterized by improved high temperature mechanical properties.

  1. METHOD AND ALLOY FOR BONDING TO ZIRCONIUM

    DOEpatents

    McCuaig, F.D.; Misch, R.D.

    1960-04-19

    A brazing alloy can be used for bonding zirconium and its alloys to other metals, ceramics, and cermets, and consists of 6 to 9 wt.% Ni, 6 to 9 wn~.% Cr, Mo, or W, 0 to 7.5 wt.% Fe, and the balance Zr.

  2. Intercalation chemistry of zirconium 4-sulfophenylphosphonate

    SciTech Connect

    Svoboda, Jan; Zima, Vítězslav; Melánová, Klára; Beneš, Ludvík; Trchová, Miroslava

    2013-12-15

    Zirconium 4-sulfophenylphosphonate is a layered material which can be employed as a host for the intercalation reactions with basic molecules. A wide range of organic compounds were chosen to represent intercalation ability of zirconium 4-sulfophenylphosphonate. These were a series of alkylamines from methylamine to dodecylamine, 1,4-phenylenediamine, p-toluidine, 1,8-diaminonaphthalene, 1-aminopyrene, imidazole, pyridine, 4,4′-bipyridine, poly(ethylene imine), and a series of amino acids from glycine to 6-aminocaproic acid. The prepared compounds were characterized by powder X-ray diffraction, thermogravimetry analysis and IR spectroscopy and probable arrangement of the guest molecules in the interlayer space of the host is proposed based on the interlayer distance of the prepared intercalates and amount of the intercalated guest molecules. - Graphical abstract: Nitrogen-containing organic compounds can be intercalated into the interlayer space of zirconium 4-sulfophenylphosphonate. - Highlights: • Zirconium 4-sulfophenylphosphonate was examined as a host material in intercalation chemistry. • A wide range of nitrogen-containing organic compounds were intercalated. • Possible arrangement of the intercalated species is described.

  3. Superconductivity in zirconium-rhodium alloys

    NASA Technical Reports Server (NTRS)

    Zegler, S. T.

    1969-01-01

    Metallographic studies and transition temperature measurements were made with isothermally annealed and water-quenched zirconium-rhodium alloys. The results clarify both the solid-state phase relations at the Zr-rich end of the Zr-Rh alloy system and the influence upon the superconducting transition temperature of structure and composition.

  4. International strategic minerals inventory summary report; zirconium

    USGS Publications Warehouse

    Towner, R.R.

    1992-01-01

    Zircon, a zirconium silicate, is currently the most important commercial zirconium-bearing mineral. Baddeleyite, a natural form of zirconia, is less important but has some specific end uses. Both zircon and baddeleyite occur in hard-rock and placer deposits, but at present all zircon production is from placer deposits. Most baddeleyite production is from hard-rock deposits, principally as a byproduct of copper and phosphate-rock mining. World zirconium resources in identified, economically exploitable deposits are about 46 times current production rates. Of these resources, some 71 percent are in South Africa, Australia, and the United States. The principal end uses of zirconium minerals are in ceramic applications and as refractories, abrasives, and mold linings in foundries. A minor amount, mainly of zircon, is used for the production of hafnium-free zirconium metal, which is used principally for sheathing fuel elements in nuclear reactors and in the chemical-processing industry, aerospace engineering, and electronics. Australia and South Africa are the largest zircon producers and account for more than 70 percent of world output; the United States and the Soviet Union account for another 20 percent. South Africa accounts for almost all the world's production of baddeleyite, which is about 2 percent of world production of contained zirconia. Australia and South Africa are the largest exporters of zircon. Unless major new deposits are developed in countries that have not traditionally produced zircon, the pattern of world production is unlikely to change by 2020. The proportions, however, of production that come from existing producing countries may change somewhat.

  5. METHOD OF MAKING DELTA ZIRCONIUM HYDRIDE MONOLITHIC MODERATOR PIECES

    DOEpatents

    Vetrano, J.B.

    1962-01-23

    A method is given for preparing large, sound bodies of delta zirconium hydride. The method includes the steps of heating a zirconium body to a temperature of not less than l000 deg C, providing a hydrogen atmosphere for the zirconium body at a pressure not greater than one atmosphere, reducing the temperature slowly to 800 deg C at such a rate that cracks do not form while maintaining the hydrogen pressure substantially constant, and cooling in an atmosphere of hydrogen. (AEC)

  6. ELECTROLYTIC CLADDING OF ZIRCONIUM ON URANIUM

    DOEpatents

    Wick, J.J.

    1959-09-22

    A method is presented for coating uranium with zircoalum by rendering the uranium surface smooth and oxidefree, immersing it in a molten electrolytic bath in NaCI, K/sub 2/ZrF/sub 6/, KF, and ZrO/sub 2/, and before the article reaches temperature equilibrium with the bath, applying an electrolyzing current of 60 amperes per square dectmeter at approximately 3 volts to form a layer of zirconium metal on the uranium.

  7. Effects of titanium and zirconium on iron aluminide weldments

    SciTech Connect

    Mulac, B.L.; Edwards, G.R.; Burt, R.P.; David, S.A.

    1997-12-01

    When gas-tungsten arc welded, iron aluminides form a coarse fusion zone microstructure which is susceptible to hydrogen embrittlement. Titanium inoculation effectively refined the fusion zone microstructure in iron aluminide weldments, but the inoculated weldments had a reduced fracture strength despite the presence of a finer microstructure. The weldments fractured by transgranular cleavage which nucleated at cracked second phase particles. With titanium inoculation, second phase particles in the fusion zone changed shape and also became more concentrated at the grain boundaries, which increased the particle spacing in the fusion zone. The observed decrease in fracture strength with titanium inoculation was attributed to increased spacing of second phase particles in the fusion zone. Current research has focused on the weldability of zirconium- and carbon-alloyed iron aluminides. Preliminary work performed at Oak Ridge National Laboratory has shown that zirconium and carbon additions affect the weldability of the alloy as well as the mechanical properties and fracture behavior of the weldments. A sigmajig hot cracking test apparatus has been constructed and tested at Colorado School of Mines. Preliminary characterization of hot cracking of three zirconium- and carbon-alloyed iron aluminides, each containing a different total concentration of zirconium at a constant zirconium/carbon ratio of ten, is in progress. Future testing will include low zirconium alloys at zirconium/carbon ratios of five and one, as well as high zirconium alloys (1.5 to 2.0 atomic percent) at zirconium/carbon ratios of ten to forty.

  8. Manufacturing process to reduce large grain growth in zirconium alloys

    DOEpatents

    Rosecrans, P.M.

    1984-08-01

    It is an object of the present invention to provide a procedure for desensitizing zirconium-based alloys to large grain growth (LGG) during thermal treatment above the recrystallization temperature of the alloy. It is a further object of the present invention to provide a method for treating zirconium-based alloys which have been cold-worked in the range of 2 to 8% strain to reduce large grain growth. It is another object of the present invention to provide a method for fabricating a zirconium alloy clad nuclear fuel element wherein the zirconium clad is resistant to large grain growth.

  9. From Zirconium Nanograins to Zirconia Nanoneedles.

    PubMed

    Zalnezhad, E; Hamouda, A M S; Jaworski, J; Do Kim, Young

    2016-01-01

    Combinations of three simple techniques were utilized to gradually form zirconia nanoneedles from zirconium nanograins. First, a physical vapor deposition magnetron sputtering technique was used to deposit pure zirconium nanograins on top of a substrate. Second, an anodic oxidation was applied to fabricate zirconia nanotubular arrays. Finally, heat treatment was used at different annealing temperatures in order to change the structure and morphology from nanotubes to nanowires and subsequently to nanoneedles in the presence of argon gas. The size of the pure zirconium nanograins was estimated to be approximately 200-300 nm. ZrO2 nanotubular arrays with diameters of 70-120 nm were obtained. Both tetragonal and monoclinic ZrO2 were observed after annealing at 450 °C and 650 °C. Only a few tetragonal peaks appeared at 850 °C, while monoclinic ZrO2 was obtained at 900 °C and 950 °C. In assessing the biocompatibility of the ZrO2 surface, the human cell line MDA-MB-231 was found to attach and proliferate well on surfaces annealed at 850 °C and 450 °C; however, the amorphous ZrO2 surface, which was not heat treated, did not permit extensive cell growth, presumably due to remaining fluoride. PMID:27623486

  10. High temperature behavior of zirconium germanates

    SciTech Connect

    Utkin, A.V.; Baklanova, N.I.; Vasilyeva, I.G.

    2013-05-01

    The high temperature behavior of zirconium germanates ZrGeO₄ and Zr₃GeO₈ up to 2300 °C has been studied using the original photoemission thermal analysis technique with the comprehensive physicochemical study of solid and gaseous intermediate and final products. The two-stage process of incongruent sublimation of GeO₂ was established and the phase boundary of the homogeneity range for ZrGeO₄ and Zr₃GeO₈ were deduced from the thermal analysis, X-ray diffraction and Raman spectroscopy studies. A high tendency to sintering of the final ZrO₂ product is discussed. - Graphical abstract: The decomposition of zirconium germanates leads to the formation of gaseous GeO₂ and solid sintered ZrO₂ and occurs via two stages with the formation of intermediate ZrO₂-rich solid solution. Highlights: •Thermal behavior of ZrGeO₄ and Zr₃GeO₈ was studied using the original thermal analysis technique in wide temperature range. •The decomposition occurs via two stages with the formation of intermediate ZrO₂-rich solid solution. •The decomposition of zirconium germanates leads to the formation of gaseous GeO₂ and solid sintered ZrO₂. •The temperature of decomposition is strongly depended on the total gas pressure.

  11. Fluorometric determination of zirconium in minerals

    USGS Publications Warehouse

    Alford, W.C.; Shapiro, L.; White, C.E.

    1951-01-01

    The increasing use of zirconium in alloys and in the ceramics industry has created renewed interest in methods for its determination. It is a common constituent of many minerals, but is usually present in very small amounts. Published methods tend to be tedious, time-consuming, and uncertain as to accuracy. A new fluorometric procedure, which overcomes these objections to a large extent, is based on the blue fluorescence given by zirconium and flavonol in sulfuric acid solution. Hafnium is the only element that interferes. The sample is fused with borax glass and sodium carbonate and extracted with water. The residue is dissolved in sulfuric acid, made alkaline with sodium hydroxide to separate aluminum, and filtered. The precipitate is dissolved in sulfuric acid and electrolysed in a Melaven cell to remove iron. Flavonol is then added and the fluorescence intensity is measured with a photo-fluorometer. Analysis of seven standard mineral samples shows excellent results. The method is especially useful for minerals containing less than 0.25% zirconium oxide.

  12. From Zirconium Nanograins to Zirconia Nanoneedles

    NASA Astrophysics Data System (ADS)

    Zalnezhad, E.; Hamouda, A. M. S.; Jaworski, J.; Do Kim, Young

    2016-09-01

    Combinations of three simple techniques were utilized to gradually form zirconia nanoneedles from zirconium nanograins. First, a physical vapor deposition magnetron sputtering technique was used to deposit pure zirconium nanograins on top of a substrate. Second, an anodic oxidation was applied to fabricate zirconia nanotubular arrays. Finally, heat treatment was used at different annealing temperatures in order to change the structure and morphology from nanotubes to nanowires and subsequently to nanoneedles in the presence of argon gas. The size of the pure zirconium nanograins was estimated to be approximately 200-300 nm. ZrO2 nanotubular arrays with diameters of 70-120 nm were obtained. Both tetragonal and monoclinic ZrO2 were observed after annealing at 450 °C and 650 °C. Only a few tetragonal peaks appeared at 850 °C, while monoclinic ZrO2 was obtained at 900 °C and 950 °C. In assessing the biocompatibility of the ZrO2 surface, the human cell line MDA-MB-231 was found to attach and proliferate well on surfaces annealed at 850 °C and 450 °C however, the amorphous ZrO2 surface, which was not heat treated, did not permit extensive cell growth, presumably due to remaining fluoride.

  13. [The clinical application of zirconium-dioxide-ceramics. Case report].

    PubMed

    Somfai, Dóra; Zsigmond, Ágnes; Károlyházy, Katalin; Kispély, Barbara; Hermann, Péter

    2015-12-01

    Due to its outstanding physical, mechanical and esthetic properties, zirconium-dioxide is one of the most popular non-metal denture, capable of surpassing PFM in most cases. The recent advances of CAD/CAM technology makes it a good alternitve. Here we show the usefulness of zirconium-dioxide in everyday dental practice through three case reports. PMID:26863816

  14. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lead niobium titanium zirconium oxide... Specific Chemical Substances § 721.10602 Lead niobium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead niobium...

  15. 40 CFR 721.10601 - Lanthanum lead titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lanthanum lead titanium zirconium... Specific Chemical Substances § 721.10601 Lanthanum lead titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lanthanum...

  16. 40 CFR 721.10601 - Lanthanum lead titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lanthanum lead titanium zirconium... Specific Chemical Substances § 721.10601 Lanthanum lead titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lanthanum...

  17. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lead niobium titanium zirconium oxide... Specific Chemical Substances § 721.10602 Lead niobium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead niobium...

  18. 40 CFR 721.10598 - Lead strontium titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lead strontium titanium zirconium... Specific Chemical Substances § 721.10598 Lead strontium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead...

  19. 40 CFR 721.10598 - Lead strontium titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lead strontium titanium zirconium... Specific Chemical Substances § 721.10598 Lead strontium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead...

  20. NEUTRON REACTOR FUEL ELEMENT UTILIZING ZIRCONIUM-BASE ALLOYS

    DOEpatents

    Saller, H.A.; Keeler, J.R.; Szumachowski, E.R.

    1957-11-12

    This patent relates to clad fuel elements for use in neutronic reactors and is drawn to such a fuel element which consists of a core of fissionable material, comprised of an alloy of zirconium and U/sup 235/ enriched uranium, encased in a jacket of a binary zirconium-tin alloy in which the tin content ranges between 1 and 15% by weight.

  1. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  2. [The clinical application of zirconium-dioxide-ceramics. Case report].

    PubMed

    Somfai, Dóra; Zsigmond, Ágnes; Károlyházy, Katalin; Kispély, Barbara; Hermann, Péter

    2015-12-01

    Due to its outstanding physical, mechanical and esthetic properties, zirconium-dioxide is one of the most popular non-metal denture, capable of surpassing PFM in most cases. The recent advances of CAD/CAM technology makes it a good alternitve. Here we show the usefulness of zirconium-dioxide in everyday dental practice through three case reports.

  3. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  4. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  5. PROCESS FOR DISSOLVING BINARY URANIUM-ZIRCONIUM OR ZIRCONIUM-BASE ALLOYS

    DOEpatents

    Jonke, A.A.; Barghusen, J.J.; Levitz, N.M.

    1962-08-14

    A process of dissolving uranium-- zirconium and zircaloy alloys, e.g. jackets of fuel elements, with an anhydrous hydrogen fluoride containing from 10 to 32% by weight of hydrogen chloride at between 400 and 450 deg C., preferably while in contact with a fluidized inert powder, such as calcium fluoride is described. (AEC)

  6. Experimental study on flames propagating through zirconium particle clouds.

    PubMed

    Yin, Yi; Sun, Jinhua; Ding, Yibin; Guo, Song; He, Xuechao

    2009-10-15

    To reveal the mechanisms of flame propagation through the hardly volatile metal dust clouds clearly, the flame propagating through zirconium particle clouds has been examined experimentally. A high-speed video camera was used to record the propagation process of the flame. Combustion zone temperature was detected by a fine thermocouple. Based on the experimental results, structure of flame and combustion courses of zirconium particles were analyzed, the combustion propagation in zirconium dust was investigated, and the velocity and temperature characteristics of the combustion zone were also elucidated. The combustion zone propagating through zirconium particle clouds consists of luminous particles. Particle concentration plays an important role in the combustion zone propagation process. With the increase of zirconium particle concentration, the maximum temperature of the combustion zone increases at the lower concentration, takes a maximum value, and then decreases at the higher concentration. It is also found that the propagation velocity of the combustion zone has a linear relationship with its maximum temperature.

  7. Zirconium fluoride glass - Surface crystals formed by reaction with water

    NASA Technical Reports Server (NTRS)

    Doremus, R. H.; Bansal, N. P.; Bradner, T.; Murphy, D.

    1984-01-01

    The hydrated surfaces of a zirconium barium fluoride glass, which has potential for application in optical fibers and other optical elements, were observed by scanning electron microscopy. Crystalline zirconium fluoride was identified by analysis of X-ray diffraction patterns of the surface crystals and found to be the main constituent of the surface material. It was also found that hydrated zirconium fluorides form only in highly acidic fluoride solutions. It is possible that the zirconium fluoride crystals form directly on the glass surface as a result of its depletion of other ions. The solubility of zirconium fluoride is suggested to be probably much lower than that of barium fluoride (0.16 g/100 cu cm at 18 C). Dissolution was determined to be the predominant process in the initial stages of the reaction of the glass with water. Penetration of water into the glass has little effect.

  8. In situ hydrogen loading on zirconium powder

    PubMed Central

    Maimaitiyili, Tuerdi; Blomqvist, Jakob; Steuwer, Axel; Bjerkén, Christina; Zanellato, Olivier; Blackmur, Matthew S.; Andrieux, Jérôme; Ribeiro, Fabienne

    2015-01-01

    For the first time, various hydride phases in a zirconium–hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr–H phase diagram are obtained from a single experimental arrangement. PMID:26134803

  9. Short-time oxidation of zirconium.

    NASA Technical Reports Server (NTRS)

    Srivastava, L. P.; Archbold, T. F.

    1972-01-01

    Study of zirconium oxidation kinetics for maximum exposure times of 3 min and in the temperature range 440 to 850 C. 'Discontinuous' oxidation runs were employed whereby a specimen was inserted into the gas stream for a predetermined time, removed and weighed, and reinserted into the oxidation atmosphere. It is considered that the increase in the observed activation energy for the early stage parabolic oxidation is a manifestation of a change from an n-type oxide to a predominantly p-type oxide, in agreement with the authors' earlier conclusion (1971) based on pressure effects.

  10. ZIRCONIUM-TITANIUM-BERYLLIUM BRAZING ALLOY

    DOEpatents

    Gilliland, R.G.; Patriarca, P.; Slaughter, G.M.; Williams, L.C.

    1962-06-12

    A new and improved ternary alloy is described which is of particular utility in braze-bonding parts made of a refractory metal selected from Group IV, V, and VI of the periodic table and alloys containing said metal as a predominating alloying ingredient. The brazing alloy contains, by weight, 40 to 50 per cent zirconium, 40 to 50 per cent titanium, and the balance beryllium in amounts ranging from 1 to 20 per cent, said alloy having a melting point in the range 950 to 1400 deg C. (AEC)

  11. Shell model description of zirconium isotopes

    SciTech Connect

    Sieja, K.; Nowacki, F.; Langanke, K.; Martinez-Pinedo, G.

    2009-06-15

    We calculate the low-lying spectra and several high-spin states of zirconium isotopes (Z=40) with neutron numbers from N=50 to N=58 using a large valence space with the {sup 78}Ni inert core, which a priori allows one to study the interplay between spherical and deformed configurations, necessary for the description of nuclides in this part of the nuclear chart. The effective interaction is derived by monopole corrections of the realistic G matrix. We reproduce essential nuclear properties, such as subshell closures in {sup 96}Zr and {sup 98}Zr. The spherical-to-deformed shape transition in {sup 100}Zr is addressed as well.

  12. METHOD FOR DISSOLVING ZIRCONIUM-URANIUM COMPOSITIONS

    DOEpatents

    Gens, T.A.

    1961-07-18

    A method is descrioed for treating a zirconium-- uranium composition to form a stable solution from which uranium and other values may be extracted by contacting the composition with at least a 4 molar aqueous solution of ammonium fluoride at a temperature of about 100 deg C, adding a peroxide, in incremental amounts, to the heated solution throughout the period of dissolution until all of the uranium is converted to soluble uranyl salt, adding nitric acid to the resultant solution to form a solvent extraction feed solution to convert the uranyl salt to a solvent extractable state, and thereafter recovering the uranium and other desired values from the feed solution by solvent extraction.

  13. Cherenkov and Scintillation Properties of Cubic Zirconium

    NASA Technical Reports Server (NTRS)

    Christl, M.J.; Adams, J.H.; Parnell, T.A.; Kuznetsov, E.N.

    2008-01-01

    Cubic zirconium (CZ) is a high index of refraction (n =2.17) material that we have investigated for Cherenkov counter applications. Laboratory and proton accelerator tests of an 18cc sample of CZ show that the expected fast Cherenkov response is accompanied by a longer scintillation component that can be separated by pulse shaping. This presents the possibility of novel particle spectrometers which exploits both properties of CZ. Other high index materials being examined for Cherenkov applications will be discussed. Results from laboratory tests and an accelerator exposure will be presented and a potential application in solar energetic particle instruments will be discussed

  14. SEPARATION OF URANIUM FROM ZIRCONIUM AND NIOBIUM BY SOLVENT EXTRACTION

    DOEpatents

    Voiland, E.E.

    1958-05-01

    A process for separation of the uranium from zirconium and/or niobium values contained in 3 to 7M aqueous nitric acid solutions is described. This is accomplished by adding phosphoric acid anions to the nitric acid solution containing the uranium, zirconium, and/or niobium in an amount sufficient to make the solution 0.05 to 0.2M in phosphate ion and contacting the solution with an organic water-immiscible solvent such as MEK, whereby the uranyl values are taken up by the extract phase while the zirconium and niobium preferentially remain in the aqueous raffinate.

  15. METHOD OF PREPARING SINTERED ZIRCONIUM METAL FROM ITS HYDRIDES

    DOEpatents

    Angier, R.P.

    1958-02-11

    The invention relates to the preparation of metal shapes from zirconium hydride by powder metallurgical techniques. The zirconium hydride powder which is to be used for this purpose can be prepared by rendering massive pieces of crystal bar zirconium friable by heat treatment in purified hydrogen. This any then be ground into powder and powder can be handled in the air without danger of it igniting. It may then be compacted in the normal manner by being piaced in a die. The compact is sintered under vacuum conditions preferably at a temperature ranging from 1200 to 1300 deg C and for periods of one to three hours.

  16. RECOVERY OF URANIUM FROM ZIRCONIUM-URANIUM NUCLEAR FUELS

    DOEpatents

    Gens, T.A.

    1962-07-10

    An improvement was made in a process of recovering uranium from a uranium-zirconium composition which was hydrochlorinated with gsseous hydrogen chloride at a temperature of from 350 to 800 deg C resulting in volatilization of the zirconium, as zirconium tetrachloride, and the formation of a uranium containing nitric acid insoluble residue. The improvement consists of reacting the nitric acid insoluble hydrochlorination residue with gaseous carbon tetrachloride at a temperature in the range 550 to 600 deg C, and thereafter recovering the resulting uranium chloride vapors. (AEC)

  17. Determination of fracture strength of δ-zirconium hydrides embedded in zirconium matrix at high temperatures

    NASA Astrophysics Data System (ADS)

    Kubo, T.; Kobayashi, Y.; Uchikoshi, H.

    2013-04-01

    The fracture strength of δ-zirconium hydrides embedded in a zirconium matrix was determined at temperatures between 25 °C and 250 °C by ring tensile tests using Zircaloy-2 tubes. Essentially all of the present hydrides in the tubes were re-oriented in the radial direction by a temperature cycling treatment and then tensile stress was applied perpendicular to the hydrides to ensure that brittle fracture would occur at the hydrides. The hydrides failed in a brittle manner below 100 °C where-as the zirconium matrix itself underwent ductile fracture without hydride cracking at temperatures above 200 °C under plane stress condition. Brittle fracture of the hydrides continued to occur at temperatures up to 250 °C under plane strain condition, suggesting that the upper limit temperature for hydride fracture, Tupper, was raised by the triaxial stress state under the plane strain condition. The apparent fracture strength of the hydrides, σhydridef, was determined at temperatures below Tupper from the measured fracture strength of the tubes, making a correction for the compressive transformation stress in the hydrides. σhydridef was about 710 MPa at temperatures between 25 °C and 250 °C at both plane stress and plane strain conditions. The temperature dependency was very small in this temperature range. Tupper was almost equivalent to the cross-over temperature between σhydridef and the ultimate tensile strength (UTS), which suggests that, at temperatures above Tupper, the zirconium matrix would undergo ductile fracture before the stress in the hydride is raised above σhydridef, since UTS is smaller than σhydridef.

  18. Zirconium Hydride Space Power Reactor design.

    NASA Technical Reports Server (NTRS)

    Asquith, J. G.; Mason, D. G.; Stamp, S.

    1972-01-01

    The Zirconium Hydride Space Power Reactor being designed and fabricated at Atomics International is intended for a wide range of potential applications. Throughout the program a series of reactor designs have been evaluated to establish the unique requirements imposed by coupling with various power conversion systems and for specific applications. Current design and development emphasis is upon a 100 kilowatt thermal reactor for application in a 5 kwe thermoelectric space power generating system, which is scheduled to be fabricated and ground tested in the mid 70s. The reactor design considerations reviewed in this paper will be discussed in the context of this 100 kwt reactor and a 300 kwt reactor previously designed for larger power demand applications.

  19. Plastic deformation of polycrystalline zirconium carbide

    NASA Technical Reports Server (NTRS)

    Darolia, R.; Archbold, T. F.

    1976-01-01

    The compressive yield strength of arc-melted polycrystalline zirconium carbide has been found to vary from 77 kg per sq mm at 1200 C to 19 kg per sq mm at 1800 C. Yield drops were observed with plastic strain-rates greater than 0.003/sec but not with slower strain rates. Strain-rate change experiments yielded values for the strain-rate sensitivity parameter m which range from 6.5 at 1500 C to 3.8 at 1800 C, and the product dislocation velocity stress exponent times T was found to decrease linearly with increasing temperature. The deformation rate results are consistent with the Kelly-Rowcliffe model in which the diffusion of carbon assists the motion of dislocations.

  20. Mid-term survivorship and clinical outcomes of cobalt-chrome and oxidized zirconium on highly crosslinked polyethylene

    PubMed Central

    Petis, Stephen M.; Vasarhelyi, Edward M.; Lanting, Brent A.; Howard, James L.; Naudie, Douglas D.R.; Somerville, Lyndsay E.; McCalden, Richard W.

    2016-01-01

    Background The choice of bearing articulation for total hip arthroplasty in younger patients is amenable to debate. We compared mid-term patient-reported outcomes and survivorship across 2 different bearing articulations in a young patient cohort. Methods We reviewed patients with cobalt-chrome or oxidized zirconium on highly crosslinked polyethylene who were followed prospectively between 2004 and 2012. Kaplan–Meier analysis was used to determine predicted cumulative survivorship at 5 years with all-cause and aseptic revisions as the outcome. We compared patient-reported outcomes, including the Harris hip score (HHS), Western Ontario and McMaster University Osteoarthritis Index (WOMAC) and Short-form 12 (SF-12) scores. Results A total of 622 patients were followed during the study period. Mean follow-up was 8.2 (range 2.0–10.6) years for cobalt-chrome and 7.8 (range 2.1–10.7) years for oxidized zirconium. Mean age was 54.9 ± 10.6 years for cobalt-chrome and 54.8 ± 10.7 years for oxidized zirconium. Implant survivorship was 96.0% (95% confidence interval [CI] 94.9%–97.1%) for cobalt-chrome and 98.7% (95% CI 98.0%–99.4%) for oxidized zirconium on highly crosslinked polyethylene for all-cause revisions, and 97.2% (95% CI 96.2%–98.2%) for cobalt-chrome and 99.0% (95% CI 98.4%–99.6%) for oxidized zirconium for aseptic revisions. An age-, sex- and diagnosis-matched comparison of the HHS, WOMAC and SF-12 scores demonstrated no significant changes in clinical outcomes across the groups. Conclusion Both bearing surface couples demonstrated excellent mid-term survivorship and outcomes in young patient cohorts. Future analyses on wear and costs are warranted to elicit differences between the groups at long-term follow-up. PMID:26812409

  1. Investigation of Electrochemical Recovery of Zirconium from Spent Nuclear Fuels

    SciTech Connect

    Michael Simpson; II-Soon Hwang

    2014-06-01

    This project uses both modeling and experimental studies to design optimal electrochemical technology methods for recovery of zirconium from used nuclear fuel rods for more effective waste management. The objectives are to provide a means of efficiently separating zirconium into metallic high-level waste forms and to support development of a process for decontamination of zircaloy hulls to enable their disposal as low- and intermediate-level waste. Modeling work includes extension of a 3D model previously developed by Seoul National University for uranium electrorefining by adding the ability to predict zirconium behavior. Experimental validation activities include tests for recovery of zirconium from molten salt solutions and aqueous tests using surrogate materials. *This is a summary of the FY 2013 progress for I-NERI project # 2010-001-K provided to the I-NERI office.

  2. Origin of the blue luminescence band in zirconium oxide

    NASA Astrophysics Data System (ADS)

    Gulyaev, D. V.; Perevalov, T. V.; Aliev, V. Sh.; Zhuravlev, K. S.; Gritsenko, V. A.; Eliseev, A. P.; Zablotskii, A. V.

    2015-07-01

    The photoluminescence excitation and steady-state photoluminescence spectra of nonstoichiometric zirconium oxide films with a high concentration of oxygen vacancies have been investigated. A band with energy of about 2.7 eV in the blue spectral region dominates in photoluminescence spectra of prepared films. The photoluminescence intensity of this band increases as the depletion of zirconium oxide films with oxygen increases. The excitation maximum of the blue photoluminescence band corresponds to energy of 5.2 eV. It has been established by quantum-chemical modeling that the optical absorption peak of the oxygen vacancy in crystalline zirconium oxide is located at energy of 5.1 eV. The analysis of the results has demonstrated that the blue photoluminescence band at 2.7 eV with the excitation peak near 5.2 eV is caused by oxygen vacancies in zirconium oxide.

  3. Process for massively hydriding zirconium--uranium fuel elements

    DOEpatents

    Katz, N.H.

    1973-12-01

    A method is described of hydriding uranium-zirconium alloy by heating the alloy in a vacuum, introducing hydrogen and maintaining an elevated temperature until occurrence of the beta--delta phase transformation and isobarically cooling the composition. (Official Gazette)

  4. Nucleation Pathways For Freezing Of Two Grades Of Zirconium

    NASA Technical Reports Server (NTRS)

    Rhim, Won-Kyu; Rulison, Aaron; Bayuzick, Robert; Hofmeister, William; Morton, Craig

    1996-01-01

    Report discusses classical nucleation theory of freezing and describes experimental study of nucleation mechanisms that predominate during freezing of spherical specimens of initially molten zirconium levitated electrostatically in vacuum.

  5. PRECIPITATION OF ZIRCONIUM AND FLUORIDE IONS FROM SOLUTIONS

    DOEpatents

    Newby, B.J.

    1963-06-11

    A process is given for removing zirconium and fluorine ions from aqueous solutions also containing uranium(VI). The precipitation is carried out with sodium formate, and the uranium remains in solution. (AEC)

  6. Critical role of nitrogen during high temperature scaling of zirconium

    NASA Technical Reports Server (NTRS)

    Evans, E. B.; Tsangarakis, N.; Probst, H. B.; Garibotti, N. J.

    1973-01-01

    The mechanisms of scale cracking, scale color changes, and scale growth, and their interrelations, were studied in zirconium specimens at elevated temperatures in air, oxygen and nitrogen. Nitrogen was found to be responsible for monoclinic-to-cubic ZrO2 conversion, for scale cracking and breakaway on zirconium nitride, and for the formation of ZrN on the metal interface underneath an outer oxide layer.

  7. Quercetin as colorimetric reagent for determination of zirconium

    USGS Publications Warehouse

    Grimaldi, F.S.; White, C.E.

    1953-01-01

    Methods described in the literature for the determination of zirconium are generally designed for relatively large amounts of this element. A good procedure using colorimetric reagent for the determination of trace amounts is desirable. Quercetin has been found to yield a sensitive color reaction with zirconium suitable for the determination of from 0.1 to 50?? of zirconium dioxide. The procedure developed involves the separation of zirconium from interfering elements by precipitation with p-dimethylaminoazophenylarsonic acid prior to its estimation with quercetin. The quercetin reaction is carried out in 0.5N hydrochloric acid solution. Under the operating conditions it is indicated that quercetin forms a 2 to 1 complex with zirconium; however, a 2 to 1 and a 1 to 1 complex can coexist under special conditions. Approximate values for the equilibrium constants of the complexes are K1 = 0.33 ?? 10-5 and K2 = 1.3 ?? 10-9. Seven Bureau of Standards samples of glass sands and refractories were analyzed with excellent results. The method described should find considerable application in the analysis of minerals and other materials for macro as well as micro amounts of zirconium.

  8. Clinical evidence on titanium-zirconium dental implants: a systematic review and meta-analysis.

    PubMed

    Altuna, P; Lucas-Taulé, E; Gargallo-Albiol, J; Figueras-Álvarez, O; Hernández-Alfaro, F; Nart, J

    2016-07-01

    The use of titanium implants is well documented and they have high survival and success rates. However, when used as reduced-diameter implants, the risk of fracture is increased. Narrow diameter implants (NDIs) of titanium-zirconium (Ti-Zr) alloy have recently been developed (Roxolid; Institut Straumann AG). Ti-Zr alloys (two highly biocompatible materials) demonstrate higher tensile strength than commercially pure titanium. The aim of this systematic review was to summarize the existing clinical evidence on dental NDIs made from Ti-Zr. A systematic literature search was performed using the Medline database to find relevant articles on clinical studies published in the English language up to December 2014. Nine clinical studies using Ti-Zr implants were identified. Overall, 607 patients received 922 implants. The mean marginal bone loss was 0.36±0.06mm after 1 year and 0.41±0.09mm after 2 years. The follow-up period ranged from 3 to 36 months. Mean survival and success rates were 98.4% and 97.8% at 1 year after implant placement and 97.7% and 97.3% at 2 years. Narrow diameter Ti-Zr dental implants show survival and success rates comparable to regular diameter titanium implants (>95%) in the short term. Long-term follow-up clinical data are needed to confirm the excellent clinical performance of these implants.

  9. Zirconium behaviour during electrorefining of actinide-zirconium alloy in molten LiCl-KCl on aluminium cathodes

    NASA Astrophysics Data System (ADS)

    Meier, R.; Souček, P.; Malmbeck, R.; Krachler, M.; Rodrigues, A.; Claux, B.; Glatz, J.-P.; Fanghänel, Th.

    2016-04-01

    A pyrochemical electrorefining process for the recovery of actinides from metallic nuclear fuel based on actinide-zirconium alloys (An-Zr) in a molten salt is being investigated. In this process actinides are group-selectively recovered on solid aluminium cathodes as An-Al alloys using a LiCl-KCl eutectic melt at a temperature of 450 °C. In the present study the electrochemical behaviour of zirconium during electrorefining was investigated. The maximum amount of actinides that can be oxidised without anodic co-dissolution of zirconium was determined at a selected constant cathodic current density. The experiment consisted of three steps to assess the different stages of the electrorefining process, each of which employing a fresh aluminium cathode. The results indicate that almost a complete dissolution of the actinides without co-dissolution of zirconium is possible under the applied experimental conditions.

  10. EPDL97: the evaluated photo data library `97 version

    SciTech Connect

    Cullen, D.E.; Hubbell, J.H.; Kissel, L.

    1997-09-19

    The Evaluated Photon Data Library, 1997 version (EPLD97), is designed for use in photon transport calculations at Lawrence Livermore National Laboratory. This library includes photon interaction data for all elements with atomic number between Z = 1 (hydrogne) and 100 (fermium), including: photoionization, photoexcitation, coherent and incoherent scattering, and pair and triplet porduction cross sections. For use in applications data is provided for all elements over the energy range 1 eV to 100 GeV. This report documents the sources and treatment of the data included inthis library. EPDL97 completely supersedes the earlier 1989 version of EPDL and it is highly recommended that useres only use the most recent version of this library.

  11. Understanding the Irradiation Behavior of Zirconium Carbide

    SciTech Connect

    Motta, Arthur; Sridharan, Kumar; Morgan, Dane; Szlufarska, Izabela

    2013-10-11

    Zirconium carbide (ZrC) is being considered for utilization in high-temperature gas-cooled reactor fuels in deep-burn TRISO fuel. Zirconium carbide possesses a cubic B1-type crystal structure with a high melting point, exceptional hardness, and good thermal and electrical conductivities. The use of ZrC as part of the TRISO fuel requires a thorough understanding of its irradiation response. However, the radiation effects on ZrC are still poorly understood. The majority of the existing research is focused on the radiation damage phenomena at higher temperatures (>450{degree}C) where many fundamental aspects of defect production and kinetics cannot be easily distinguished. Little is known about basic defect formation, clustering, and evolution of ZrC under irradiation, although some atomistic simulation and phenomenological studies have been performed. Such detailed information is needed to construct a model describing the microstructural evolution in fast-neutron irradiated materials that will be of great technological importance for the development of ZrC-based fuel. The goal of the proposed project is to gain fundamental understanding of the radiation-induced defect formation in zirconium carbide and irradiation response by using a combination of state-of-the-art experimental methods and atomistic modeling. This project will combine (1) in situ ion irradiation at a specialized facility at a national laboratory, (2) controlled temperature proton irradiation on bulk samples, and (3) atomistic modeling to gain a fundamental understanding of defect formation in ZrC. The proposed project will cover the irradiation temperatures from cryogenic temperature to as high as 800{degree}C, and dose ranges from 0.1 to 100 dpa. The examination of this wide range of temperatures and doses allows us to obtain an experimental data set that can be effectively used to exercise and benchmark the computer calculations of defect properties. Combining the examination of radiation

  12. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Definitions. 97.402 Section 97.402 Education Office of... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this subpart. In addition, the following definitions also apply to this subpart: (a) Children are persons...

  13. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Definitions. 97.402 Section 97.402 Education Office of... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this subpart. In addition, the following definitions also apply to this subpart: (a) Children are persons...

  14. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Definitions. 97.402 Section 97.402 Education Office of... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this subpart. In addition, the following definitions also apply to this subpart: (a) Children are persons...

  15. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Definitions. 97.402 Section 97.402 Education Office of... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this subpart. In addition, the following definitions also apply to this subpart: (a) Children are persons...

  16. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Definitions. 97.402 Section 97.402 Education Office of... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this subpart. In addition, the following definitions also apply to this subpart: (a) Children are persons...

  17. PROCESS OF RECOVERING ZIRCONIUM VALUES FROM HAFNIUM VALUES BY SOLVENT EXTRACTION WITH AN ALKYL PHOSPHATE

    DOEpatents

    Peppard, D.F.

    1960-02-01

    A process of separating hafnium nitrate from zirconium nitrate contained in a nitric acid solution by selectively. extracting the zirconium nitrate with a water-immiscible alkyl phosphate is reported.

  18. In situ ion irradiation of zirconium carbide

    NASA Astrophysics Data System (ADS)

    Ulmer, Christopher J.; Motta, Arthur T.; Kirk, Mark A.

    2015-11-01

    Zirconium carbide (ZrC) is a candidate material for use in one of the layers of TRISO coated fuel particles to be used in the Generation IV high-temperature, gas-cooled reactor, and thus it is necessary to study the effects of radiation damage on its structure. The microstructural evolution of ZrCx under irradiation was studied in situ using the Intermediate Voltage Electron Microscope (IVEM) at Argonne National Laboratory. Samples of nominal stoichiometries ZrC0.8 and ZrC0.9 were irradiated in situ using 1 MeV Kr2+ ions at various irradiation temperatures (T = 20 K-1073 K). In situ experiments made it possible to continuously follow the evolution of the microstructure during irradiation using diffraction contrast imaging. Images and diffraction patterns were systematically recorded at selected dose points. After a threshold dose during irradiations conducted at room temperature and below, black-dot defects were observed which accumulated until saturation. Once created, the defect clusters did not move or get destroyed during irradiation so that at the final dose the low temperature microstructure consisted only of a saturation density of small defect clusters. No long-range migration of the visible defects or dynamic defect creation and elimination were observed during irradiation, but some coarsening of the microstructure with the formation of dislocation loops was observed at higher temperatures. The irradiated microstructure was found to be only weakly dependent on the stoichiometry.

  19. The organometallic chemistry of cycloheptatrienyl zirconium complexes.

    PubMed

    Glöckner, Andreas; Tamm, Matthias

    2013-01-01

    This tutorial review summarizes the organometallic chemistry derived from the half-sandwich complex [(η(7)-C(7)H(7))ZrCl(tmeda)], which was used as an efficient and versatile starting material for the incorporation of monoanionic ligands into the cycloheptatrienyl zirconium coordination sphere by conventional salt metathesis reactions. A broad variety of ligands was employed, affording novel and previously inaccessible cycloheptatrienyl (sandwich) complexes of the type [(η(7)-C(7)H(7))Zr(Y)]; Y comprises pentadienyl, cyclopentadienyl, allyl, phospholyl, boratabenzene, imidazolin-2-iminato and amido systems. The cycloheptatrienyl ring in these systems usually acts as an "innocent spectator ligand", but reactivity can arise from the second ligand Y or the Lewis acidity of the, formally, Zr(+iv) center, which was probed in selected examples and put in perspective to related studies. The corresponding results emphasize why the use of [(η(7)-C(7)H(7))ZrCl(tmeda)] is clearly an advancement in the chemistry of the still fairly unexplored area of cycloheptatrienyl transition metal complexes.

  20. Mechanical properties of zirconium alloys and zirconium hydrides predicted from density functional perturbation theory

    DOE PAGES

    Weck, Philippe F.; Kim, Eunja; Tikare, Veena; Mitchell, John A.

    2015-10-13

    Here, the elastic properties and mechanical stability of zirconium alloys and zirconium hydrides have been investigated within the framework of density functional perturbation theory. Results show that the lowest-energy cubic Pn-3m with combining macron]m polymorph of δ-ZrH1.5 does not satisfy all the Born requirements for mechanical stability, unlike its nearly degenerate tetragonal P42/mcm polymorph. Elastic moduli predicted with the Voigt–Reuss–Hill approximations suggest that mechanical stability of α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates is limited by the shear modulus. According to both Pugh's and Poisson's ratios, α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates can be considered ductile. The Debye temperatures predicted formore » γ-ZrH, δ-ZrH1.5 and ε-ZrH2 are θD = 299.7, 415.6 and 356.9 K, respectively, while θD = 273.6, 284.2, 264.1 and 257.1 K for the α-Zr, Zry-4, ZIRLO and M5 matrices, i.e. suggesting that Zry-4 possesses the highest micro-hardness among Zr matrices.« less

  1. Inhibition of ice growth and recrystallization by zirconium acetate and zirconium acetate hydroxide.

    PubMed

    Mizrahy, Ortal; Bar-Dolev, Maya; Guy, Shlomit; Braslavsky, Ido

    2013-01-01

    The control over ice crystal growth, melting, and shaping is important in a variety of fields, including cell and food preservation and ice templating for the production of composite materials. Control over ice growth remains a challenge in industry, and the demand for new cryoprotectants is high. Naturally occurring cryoprotectants, such as antifreeze proteins (AFPs), present one solution for modulating ice crystal growth; however, the production of AFPs is expensive and inefficient. These obstacles can be overcome by identifying synthetic substitutes with similar AFP properties. Zirconium acetate (ZRA) was recently found to induce the formation of hexagonal cavities in materials prepared by ice templating. Here, we continue this line of study and examine the effects of ZRA and a related compound, zirconium acetate hydroxide (ZRAH), on ice growth, shaping, and recrystallization. We found that the growth rate of ice crystals was significantly reduced in the presence of ZRA and ZRAH, and that solutions containing these compounds display a small degree of thermal hysteresis, depending on the solution pH. The compounds were found to inhibit recrystallization in a manner similar to that observed in the presence of AFPs. The favorable properties of ZRA and ZRAH suggest tremendous potential utility in industrial applications.

  2. Mechanical properties of zirconium alloys and zirconium hydrides predicted from density functional perturbation theory

    SciTech Connect

    Weck, Philippe F.; Kim, Eunja; Tikare, Veena; Mitchell, John A.

    2015-10-13

    Here, the elastic properties and mechanical stability of zirconium alloys and zirconium hydrides have been investigated within the framework of density functional perturbation theory. Results show that the lowest-energy cubic Pn-3m with combining macron]m polymorph of δ-ZrH1.5 does not satisfy all the Born requirements for mechanical stability, unlike its nearly degenerate tetragonal P42/mcm polymorph. Elastic moduli predicted with the Voigt–Reuss–Hill approximations suggest that mechanical stability of α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates is limited by the shear modulus. According to both Pugh's and Poisson's ratios, α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates can be considered ductile. The Debye temperatures predicted for γ-ZrH, δ-ZrH1.5 and ε-ZrH2 are θD = 299.7, 415.6 and 356.9 K, respectively, while θD = 273.6, 284.2, 264.1 and 257.1 K for the α-Zr, Zry-4, ZIRLO and M5 matrices, i.e. suggesting that Zry-4 possesses the highest micro-hardness among Zr matrices.

  3. An investigation of the luminescence behaviour of zirconium oxides

    NASA Astrophysics Data System (ADS)

    Yueh, Hsiang-Ken

    Corrosion of zirconium fuel cladding is a limiting factor in deciding the useful lifetime of fuel bundles for high burnups. Under irradiation conditions, the oxidation rate of zirconium is greatly enhanced. At present it is not clear how the alloying elements are incorporated into the oxide, and therefore, how they affect the corrosion behaviour. This prompted great interest in the investigation of the incorporation of alloying elements and impurities in the oxide during the zirconium oxidation process. Due to the low solubility of the alloying elements in the matrix oxide, the Energy Dispersive X-ray (EDX) technique does not have the sensitivity needed for their detection in areas away from the second phase particles where most of the transition metal additives (Fe, Cr, Ni) are segregated. In this study scanning electron microscopy and cathodoluminescence techniques are used to gain some insights into the effect of elements such as iron on the corrosion behaviour of zirconium alloys. Iron appears to migrate away from the second phase particles relatively easily, and to diffuse to free surfaces such as cracks within the oxide films. In these conditions it stimulates the cathodoluminescence locally. Other elements present in zirconium alloys either stimulate (Cu, Mo, Ti, Tb) light emission or suppress it (Sn, Nb), but do not appear to be localised in the oxide in the same way that iron is.

  4. STS-97 Post Flight Presentation

    NASA Technical Reports Server (NTRS)

    2001-01-01

    Various shots highlight the STS-97 Endeavour mission. Footage shows the crew suiting up and leaving the Operations and Checkout (O&C) Building, the launch, and landing. Various on-orbit activities are seen, such as docking with the International Space Station (ISS), the spacewalks (installing the PV Module P6), array deployment, meeting the Expedition 1 crew, eating, and undocking. Shots show the northern lights and a meteorite entering Earth's atmosphere from above. The Andes can be seen from the Orbiter while the P6 arrays are deploying.

  5. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants to waters of...

  6. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  7. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  8. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  9. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants to waters of...

  10. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  11. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  12. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  13. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 31 2011-07-01 2011-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  14. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  15. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  16. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  17. Synthesis and characterization of a mesoporous hydrous zirconium oxide used for arsenic removal from drinking water

    SciTech Connect

    Bortun, Anatoly; Bortun, Mila; Pardini, James; Khainakov, Sergei A.; Garcia, Jose R.

    2010-02-15

    Powder (20-50 {mu}m) mesoporous hydrous zirconium oxide was prepared from a zirconium salt granular precursor. The effect of some process parameters on product morphology, porous structure and adsorption performance has been studied. The use of hydrous zirconium oxide for selective arsenic removal from drinking water is discussed.

  18. Process for electrolytic deposition of metals on zirconium materials

    DOEpatents

    Donaghy, Robert E.

    1979-01-30

    A process for the electrolytic deposition of a metal layer on an article comprised of zirconium or a zirconium alloy is disclosed. The article is activated in an aged aqueous solution comprising from about 10 to about 20 grams per liter ammonium bifluoride and from about 0.75 to about 2 grams per liter of sulfuric acid. The solution is aged by immersion of pickled zirconium in the solution for at least about 10 minutes. The loosely adhering film formed on the article in the activating step is removed and the article is contacted with an electrolytic plating solution containing the metal to be deposited on the article in the presence of an electrode receiving current.

  19. Process for electroless deposition of metals on zirconium materials

    DOEpatents

    Donaghy, Robert E.

    1978-01-01

    A process for the electroless deposition of a metal layer on an article comprised of zirconium or a zirconium alloy is disclosed. The article is activated in an aged aqueous solution comprising from about 10 to about 20 grams per liter ammonium bifluoride and from about 0.75 to about 2 grams per liter of sulfuric acid. The solution is aged by immersion of pickled zirconium in the solution for at least about 10 minutes. The loosely adhering film formed on the article in the activating step is removed and the article is contacted with an electroless plating solution containing the metal to be deposited on the article upon sufficient contact with the article.

  20. Synthesis of zirconium oxynitride in air under DC electric fields

    NASA Astrophysics Data System (ADS)

    Morisaki, Nobuhiro; Yoshida, Hidehiro; Matsui, Koji; Tokunaga, Tomoharu; Sasaki, Katsuhiro; Yamamoto, Takahisa

    2016-08-01

    We synthesized zirconium oxynitride from yttria-stabilized zirconia (YSZ) in air by applying DC electric fields that produced a controlled electric current in the specimen. When YSZ was heated under an applied DC electric field, the electric current of the specimen steeply increased at a critical temperature, called a flash event, during flash sintering. By keeping the electric current of the specimen constant during the flash event and then holding the specimen at the critical temperature, YSZ was transformed into zirconium oxynitride under the optimal conditions of 50 V/cm, 500 mA, and 1000 °C. We confirmed that zirconium oxynitride formed using high-resolution transmission electron microscopy, electron energy-loss spectroscopy, and energy-dispersive spectrometry. To convert oxides to nitrides, reducing conditions are necessary to form excess oxygen vacancies. Our technique produced the strong reducing conditions necessary to form nitrides from the oxides by delivering a controlled electric current to the specimen.

  1. Studies on synthesis esterified zirconium glyphosates and their hydrophobic properties

    NASA Astrophysics Data System (ADS)

    Zhang, Yaqing; Li, Minglei; Ji, Xuemei; Xu, Qinghong

    2010-03-01

    A series of new organic-modified zirconium glyphosate compounds were synthesized based on the reactions between esterified glyphosates and ZrOCl 2. FT-IR spectra, solid-state 31P MAS NMR and elementary analysis proved the formation of these new compounds. Powder X-ray diffraction (PXRD) patterns and transmission electron microscope (TEM) images proved these compounds had lamellar structures. Scanning electronic microscope (SEM) images showed that solvents used in synthesis had great influence on the morphologies of products. Water contact angle measurements showed that the hydrophobic property of the products was a function of the number of carbon in esterified glyphosates, increased from 0° of zirconium glyphosate to 133° of dodecyl zirconium glyphosate. The present study offered a new route to synthesize organic-modified α-Zr(HPO 4) 2·H 2O (α-ZrP) materials with various morphology and controllable hydrophobic property.

  2. METHOD OF FABRICATING A URANIUM-ZIRCONIUM HYDRIDE REACTOR CORE

    DOEpatents

    Weeks, I.F.; Goeddel, W.V.

    1960-03-22

    A method is described of evenly dispersing uranlum metal in a zirconium hydride moderator to produce a fuel element for nuclear reactors. According to the invention enriched uranium hydride and zirconium hydride powders of 200 mesh particle size are thoroughly admixed to form a mixture containing 0.1 to 3% by weight of U/sup 235/ hydride. The mixed powders are placed in a die and pressed at 100 tons per square inch at room temperature. The resultant compacts are heated in a vacuum to 300 deg C, whereby the uranium hydride deoomposes into uranium metal and hydrogen gas. The escaping hydrogen gas forms a porous matrix of zirconium hydride, with uramum metal evenly dispersed therethrough. The advantage of the invention is that the porosity and uranium distribution of the final fuel element can be more closely determined and controlled than was possible using prior methods of producing such fuel ele- ments.

  3. Proof-of-Principle Measurements on Unirradiated Zirconium Alloys

    SciTech Connect

    Gerlach, David C.; Mitchell, Mark R.; Reid, Bruce D.; Gesh, Christopher J.; Hurley, David E.

    2007-04-18

    The ability to determine fuel assembly burnup has important non-proliferation implications since proliferation activities involve either irradiating fuel assemblies to a much lower level of burnup than is normal in commercial Light Water Reactor (LWR) practice, and/or irradiation of separate targets. Similarly, a method of determining burnup could be used to confirm declared operation for a reactor that is operating under IAEA safeguards. It is possible to determine fuel assembly burnup by measuring gamma radiation from specific fission products; however this technique is only useable after the fuel assembly has been out of the reactor for at least a year, and is not very useful after the assembly has been out of the reactor for 10 years or more. The use of isotope ratio measurements to measure the level of neutron exposure that material has received is well-known for graphite applications. The current project is an attempt to demonstrate that isotope ratio measurements can be performed on zirconium alloys used in LWR fuel assemblies. Zirconium alloys are used for structural elements of fuel assemblies and for the fuel element cladding. This report covers proof-of-principle measurements done on unirradiated zirconium alloys, these measurements show that: Titanium 48/Titanium 49 ratios can be measured in zirconium alloys using a Secondary Ionization Mass Spectrometer (SIMS) - enough Titanium was present in each of 6 samples tried to allow resolving the peaks associated with each isotope, and correction of interfering ions. The Ti 48/49 ratio measured in unirradiated zirconium alloy is, within a narrow error band, the same as that found in natural, unirradiated zirconium.

  4. Heavy Ion Irradiation Effects in Zirconium Nitride

    SciTech Connect

    Egeland, G.W.; Bond, G.M.; Valdez, J.A.; Swadener, J.G.; McClellan, K.J.; Maloy, S.A.; Sickafus, K.E.; Oliver, B.

    2004-07-01

    Polycrystalline zirconium nitride (ZrN) samples were irradiated with He{sup +}, Kr{sup ++}, and Xe{sup ++} ions to high (>1.10{sup 16} ions/cm{sup 2}) fluences at {approx}100 K. Following ion irradiation, transmission electron microscopy (TEM) and grazing incidence X-ray diffraction (GIXRD) were used to analyze the microstructure and crystal structure of the post-irradiated material. For ion doses equivalent to approximately 200 displacements per atom (dpa), ZrN was found to resist any amorphization transformation, based on TEM observations. At very high displacement damage doses, GIXRD measurements revealed tetragonal splitting of some of the diffraction maxima (maxima which are associated with cubic ZrN prior to irradiation). In addition to TEM and GIXRD, mechanical property changes were characterized using nano-indentation. Nano-indentation revealed no change in elastic modulus of ZrN with increasing ion dose, while the hardness of the irradiated ZrN was found to increase significantly with ion dose. Finally, He{sup +} ion implanted ZrN samples were annealed to examine He gas retention properties of ZrN as a function of annealing temperature. He gas release was measured using a residual gas analysis (RGA) spectrometer. RGA measurements were performed on He-implanted ZrN samples and on ZrN samples that had also been irradiated with Xe{sup ++} ions, in order to introduce high levels of displacive radiation damage into the matrix. He evolution studies revealed that ZrN samples with high levels of displacement damage due to Xe implantation, show a lower temperature threshold for He release than do pristine ZrN samples. (authors)

  5. Thermophysical properties of reaction processed zirconium diboride

    NASA Astrophysics Data System (ADS)

    Lonergan, Jason Michael

    This dissertation focuses on the thermophysical properties of high purity zirconium diboride ceramics. These ceramics have shown promise for potential applications such as leading edge materials for next generation hypersonic vehicles. The overall goal of this work was to improve the understanding of the thermal properties and maximize the thermal conductivity of ZrB2 . Four main areas were investigated in this work. First, the sintering kinetics and the intrinsic thermal properties of reaction processed ZrB 2 were studied and compared to ZrB2 produced by hot pressing commercial powders. The reaction process produced ceramics with higher thermal conductivity and enhanced densification. Next, Hf impurity concentrations were varied showing that decreasing Hf content increased thermal conductivity. Finally, isotope enrichments were performed showing that lighter isotopes increased lattice frequency and subsequently thermal conductivity. Fully enriched Zr10B2 had a thermal conductivity of 145 W/m*K which is the highest value for ZrB2 reported to date. Scattering models based on quantum mechanics were used with density functional theory to analyze the effects of impurities and isotopes on the electron and phonon density of states. Overall, this work adds insight into the fundamental mechanisms behind the thermophysical properties of ZrB2. Tailoring compositions to reduce Hf content and adjusting boron isotope concentration has led to improved thermal properties at all temperatures. The processing conditions, reported properties, and insights gained from models will help the realization of ZrB2 as a leading edge material for the next generation of hypersonic vehicles.

  6. Preliminary investigation of zirconium boride ceramals for gas-turbine blade applications

    NASA Technical Reports Server (NTRS)

    Hoffman, Charles A

    1953-01-01

    Zirconium boride ZrB2 ceramals were investigated for possible gas-turbine-blade application. Included in the study were thermal shock evaluations of disks, preliminary turbine-blade operation, and observations of oxidation resistance. Thermal shock disks of the following three compositions were studied: (a) 97.5 percent ZrB2 plus 2.5 percent B by weight; (b) 92.5 percent ZrB2 plus 7.5 percent B by weight; and (c) 100 percent ZrB2. Thermal shock disks were quenched from temperatures of 1800 degrees, 2000 degrees, 2200 degrees, and 2400 degrees F. The life of turbine blades containing 93 percent ZrB2 plus 7 percent B by weight was determined in gas-turbine tests. The blades were run at approximately 1600 degrees F and 15,000 to 26,000 rpm. The thermal shock resistance of the 97.5 percent ZrB2 plus 2.5 percent boron ceramals compares favorably with that of TiC plus Co and TiC plus Ni ceramals. Oxidation of the disks during the thermal shock evaluation was slight for the comparatively short time (8.3 hr) up through 2000 degrees F. Oxidation of a specimen was severe, however, after 100 hours at 2000 degrees F. The turbine blade performance evaluation of the 93 percent ZrB2 plus 7 percent B composition was preliminary in scope ; no conclusions can be drawn.

  7. In-situ stabilization of radioactive zirconium swarf

    SciTech Connect

    Hess, C.C.

    1999-08-31

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes. 6 figs.

  8. In-situ stabilization of radioactive zirconium swarf

    SciTech Connect

    Hess, Clay C.

    1997-12-01

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes.

  9. Radiochemical separation of zirconium and hafnium from other radionuclides.

    PubMed

    Hahn, R B

    1972-11-01

    Radiozirconium and radiohafnium may be separated from all other radionuclides except scandium and protactinium by precipitation with mandelic acid from 5-10 M hydrochloric acid, using commercial zirconyl chloride as carrier. Scandium and protactinium are removed by dissolving the precipitate in sodium carbonate, then adding barium nitrate to precipitate barium carbonate which acts as a scavenger. Zirconium mandelate is finally reprecipitated and the sample weighed and counted in this form. The method was checked by analysing commercial zirconyl chloride and standard rock samples for zirconium and hafnium by neutron-activation analysis.

  10. Radiochemical separation of zirconium and hafnium from other radionuclides.

    PubMed

    Hahn, R B

    1972-11-01

    Radiozirconium and radiohafnium may be separated from all other radionuclides except scandium and protactinium by precipitation with mandelic acid from 5-10 M hydrochloric acid, using commercial zirconyl chloride as carrier. Scandium and protactinium are removed by dissolving the precipitate in sodium carbonate, then adding barium nitrate to precipitate barium carbonate which acts as a scavenger. Zirconium mandelate is finally reprecipitated and the sample weighed and counted in this form. The method was checked by analysing commercial zirconyl chloride and standard rock samples for zirconium and hafnium by neutron-activation analysis. PMID:18961201

  11. In-situ stabilization of radioactive zirconium swarf

    DOEpatents

    Hess, Clay C.

    1999-01-01

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes.

  12. A new conducting nanocomposite -- PPy-zirconium (IV) oxide

    SciTech Connect

    Bhattacharya, A.; De, A.; Sarkar, S.; Ganguly, K.M.

    1996-05-01

    Pyrrole was polymerized in the presence of ultrafine zirconium (IV) oxide (ZrO{sub 2}) particles which act as a dispersant for pyrrole. Room temperature conductivities of the resulting polypyrrole-zirconium (IV) oxide nanocomposites having different ZrO{sub 2} particle concentrations were measured and were compared with that of bare polypyrrole. It was observed that the conductivities of the nanocomposites were higher than that of the polypyrrole without ZrO{sub 2} and increased with ZrO{sub 2} concentration up to a certain limit. From transmission electron microscope studies, particle size and morphology of the nanocomposites and ZrO{sub 2} particles were obtained.

  13. Oxidized Zirconium Bearing Surfaces in Total Knee Arthroplasty: Lessons Learned.

    PubMed

    Schüttler, Karl Friedrich; Efe, Turgay; Heyse, Thomas J; Haas, Steven B

    2015-10-01

    Polyethylene wear in total knee arthroplasty is a still unsolved problem resulting in osteolysis and long-term failure of knee joint replacement. To address the problem of polyethylene wear, research aimed for an optimal implant design and for an optimal combination of bearing surfaces. Oxidized zirconium was introduced to minimize surface wear and thus potentially increase long-term implant survival. This review comprises the current literature related to in vitro and in vivo studies evaluating performance of oxidized zirconium total knee arthroplasty and results from retrieval analyses. PMID:26216647

  14. Oxidized Zirconium Bearing Surfaces in Total Knee Arthroplasty: Lessons Learned.

    PubMed

    Schüttler, Karl Friedrich; Efe, Turgay; Heyse, Thomas J; Haas, Steven B

    2015-10-01

    Polyethylene wear in total knee arthroplasty is a still unsolved problem resulting in osteolysis and long-term failure of knee joint replacement. To address the problem of polyethylene wear, research aimed for an optimal implant design and for an optimal combination of bearing surfaces. Oxidized zirconium was introduced to minimize surface wear and thus potentially increase long-term implant survival. This review comprises the current literature related to in vitro and in vivo studies evaluating performance of oxidized zirconium total knee arthroplasty and results from retrieval analyses.

  15. Experiments on explosive interactions between zirconium-containing melt and water (ZREX).

    SciTech Connect

    Cho, D. H.

    1998-04-10

    The results of two series of experiments on explosive interactions between zirconium-containing melt and water are described. The first series of experiments involved dropping 1-kg batches of zirconium-zirconium dioxide mixture melt into a column of water while the second series employed 1.2-kg batches of zirconium-stainless steel mixture melt. Explosions took place only in those tests which were externally triggered. While the extent of zirconium oxidation in the triggered experiments was quite large, the explosion energies estimated from the experimental measurements were found to be small compared to the combined thermal and chemical energy available.

  16. Chemistry of zirconium related to the behavior of nuclear fuel cladding. Final report

    SciTech Connect

    Cubicciotti, D.

    1980-03-26

    Studies of the chemistry of the zirconium-iodine and zirconium-oxygen systems were undertaken to elucidate their thermodynamics and kinetics. It is anticipated that the results obtained will lead to an improved understanding of the chemical processes involved in chemically assisted fuel rod failures. This project not only has classified the thermodynamics of both the gas phase and the solids in the zirconium-iodine system, it has also provided valuable information on the chemisorption of iodine and of oxygen on zirconium surfaces at high temperatures. In addition, the kinetics of reactions on zirconium surfaces were studied. These results have already been helpful in understanding the stress corrosion cracking of Zircaloy.

  17. Antimicrobial effects of silver zeolite, silver zirconium phosphate silicate and silver zirconium phosphate against oral microorganisms

    PubMed Central

    Saengmee-anupharb, Sirikamon; Srikhirin, Toemsak; Thaweboon, Boonyanit; Thaweboon, Sroisiri; Amornsakchai, Taweechai; Dechkunakorn, Surachai; Suddhasthira, Theeralaksna; Kamaguchi, Arihide

    2013-01-01

    Objective To evaluate the antimicrobial activities of silver inorganic materials, including silver zeolite (AgZ), silver zirconium phosphate silicate (AgZrPSi) and silver zirconium phosphate (AgZrP), against oral microorganisms. In line with this objective, the morphology and structure of each type of silver based powders were also investigated. Methods The antimicrobial activities of AgZ, AgZrPSi and AgZrP were tested against Streptococcus mutans, Lactobacillus casei, Candida albicans and Staphylococcus aureus using disk diffusion assay as a screening test. The minimum inhibitory concentration (MIC) and minimum lethal concentration (MLC) were determined using the modified membrane method. Scanning electron microscope and X-ray diffraction were used to investigate the morphology and structure of these silver materials. Results All forms of silver inorganic materials could inhibit the growth of all test microorganisms. The MIC of AgZ, AgZrPSi and AgZrP was 10.0 g/L whereas MLC ranged between 10.0–60.0 g/L. In terms of morphology and structure, AgZrPSi and AgZrP had smaller sized particles (1.5–3.0 µm) and more uniformly shaped than AgZ. Conclusions Silver inorganic materials in the form of AgZ, AgZrPSi and AgZrP had antimicrobial effects against all test oral microorganisms and those activities may be influenced by the crystal structure of carriers. These results suggest that these silver materials may be useful metals applied to oral hygiene products to provide antimicrobial activity against oral infection. PMID:23570016

  18. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  19. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  20. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  1. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  2. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  3. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  4. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false License term. 97.25 Section 97.25... SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a 10-year term....

  5. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  6. 28 CFR 97.12 - Employee training.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 28 Judicial Administration 2 2010-07-01 2010-07-01 false Employee training. 97.12 Section 97.12... OR DETAINEE SERVICES § 97.12 Employee training. Private prisoner transport companies must require the completion of a minimum of 100 hours of employee training before an employee may transport violent...

  7. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  8. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  9. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  10. 29 CFR 97.41 - Financial reporting.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Financial reporting. 97.41 Section 97.41 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Reports, Records Retention, and Enforcement § 97.41 Financial... other forms as may from time to time be authorized by OMB, for: (i) Submitting financial reports...

  11. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  12. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  13. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  14. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  15. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Question pools. 97.523 Section 97.523... SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining one question pool for each written examination element. Each question pool must contain at least 10 times...

  16. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Question pools. 97.523 Section 97.523... SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining one question pool for each written examination element. Each question pool must contain at least 10 times...

  17. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Question pools. 97.523 Section 97.523... SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining one question pool for each written examination element. Each question pool must contain at least 10 times...

  18. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Question pools. 97.523 Section 97.523... SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining one question pool for each written examination element. Each question pool must contain at least 10 times...

  19. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 5 2012-07-01 2012-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR OCCUPATIONAL SAFETY AND HEALTH STANDARDS Occupational Health and Environmental Control § 1910.97...

  20. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 5 2010-07-01 2010-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR OCCUPATIONAL SAFETY AND HEALTH STANDARDS Occupational Health and Environmental Control § 1910.97...

  1. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 5 2014-07-01 2014-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR OCCUPATIONAL SAFETY AND HEALTH STANDARDS Occupational Health and Environmental Control § 1910.97...

  2. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 5 2011-07-01 2011-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor Regulations Relating to Labor (Continued) OCCUPATIONAL SAFETY AND HEALTH ADMINISTRATION, DEPARTMENT OF LABOR OCCUPATIONAL SAFETY AND HEALTH STANDARDS Occupational Health and Environmental Control § 1910.97...

  3. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  4. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  5. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  6. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  7. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  8. 29 CFR 97.11 - State plans.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true State plans. 97.11 Section 97.11 Labor Office of the... LOCAL GOVERNMENTS Pre-Award Requirements § 97.11 State plans. (a) Scope. The statutes for some programs require States to submit plans before receiving grants. Under regulations implementing Executive...

  9. 50 CFR 648.97 - Closed areas.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 50 Wildlife and Fisheries 12 2013-10-01 2013-10-01 false Closed areas. 648.97 Section 648.97... Multispecies and Monkfish Fisheries § 648.97 Closed areas. (a) Oceanographer Canyon Closed Area. No fishing vessel or person on a fishing vessel may enter, fish, or be in the area known as Oceanographer...

  10. 50 CFR 648.97 - Closed areas.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 50 Wildlife and Fisheries 8 2010-10-01 2010-10-01 false Closed areas. 648.97 Section 648.97... Multispecies and Monkfish Fisheries § 648.97 Closed areas. (a) Oceanographer Canyon Closed Area. No fishing vessel or person on a fishing vessel may enter, fish, or be in the area known as Oceanographer...

  11. 50 CFR 648.97 - Closed areas.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 50 Wildlife and Fisheries 12 2012-10-01 2012-10-01 false Closed areas. 648.97 Section 648.97... Multispecies and Monkfish Fisheries § 648.97 Closed areas. (a) Oceanographer Canyon Closed Area. No fishing vessel or person on a fishing vessel may enter, fish, or be in the area known as Oceanographer...

  12. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2010-04-01 2010-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  13. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  14. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  15. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  16. 40 CFR 97.619 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.619 Section 97.619 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.619...

  17. 40 CFR 97.250 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false 97.250 Section 97.250 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.250...

  18. 40 CFR 97.250 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.250 Section 97.250 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.250...

  19. 40 CFR 97.609 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.609 Section 97.609 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.609...

  20. 40 CFR 97.250 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.250 Section 97.250 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.250...

  1. 40 CFR 97.250 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.250 Section 97.250 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.250...

  2. 40 CFR 97.609 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.609 Section 97.609 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.609...

  3. 40 CFR 97.250 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false 97.250 Section 97.250 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.250...

  4. 40 CFR 97.619 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.619 Section 97.619 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.619...

  5. 40 CFR 97.629 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.629 Section 97.629 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.629...

  6. 29 CFR 97.33 - Supplies.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Supplies. 97.33 Section 97.33 Labor Office of the Secretary... GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.33 Supplies. (a) Title. Title to supplies acquired under a grant or subgrant will vest, upon acquisition, in the grantee or...

  7. 36 CFR 251.97 - Oral presentation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 36 Parks, Forests, and Public Property 2 2010-07-01 2010-07-01 false Oral presentation. 251.97 Section 251.97 Parks, Forests, and Public Property FOREST SERVICE, DEPARTMENT OF AGRICULTURE LAND USES Appeal of Decisions Relating to Occupancy and Use of National Forest System Lands § 251.97...

  8. 36 CFR 251.97 - Oral presentation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 36 Parks, Forests, and Public Property 2 2011-07-01 2011-07-01 false Oral presentation. 251.97 Section 251.97 Parks, Forests, and Public Property FOREST SERVICE, DEPARTMENT OF AGRICULTURE LAND USES Appeal of Decisions Relating to Occupancy and Use of National Forest System Lands § 251.97...

  9. 36 CFR 251.97 - Oral presentation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 36 Parks, Forests, and Public Property 2 2012-07-01 2012-07-01 false Oral presentation. 251.97 Section 251.97 Parks, Forests, and Public Property FOREST SERVICE, DEPARTMENT OF AGRICULTURE LAND USES Appeal of Decisions Relating to Occupancy and Use of National Forest System Lands § 251.97...

  10. 29 CFR 97.11 - State plans.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 1 2014-07-01 2013-07-01 true State plans. 97.11 Section 97.11 Labor Office of the... LOCAL GOVERNMENTS Pre-Award Requirements § 97.11 State plans. (a) Scope. The statutes for some programs require States to submit plans before receiving grants. Under regulations implementing Executive...

  11. 22 CFR 97.1 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 22 Foreign Relations 1 2010-04-01 2010-04-01 false Definitions. 97.1 Section 97.1 Foreign Relations DEPARTMENT OF STATE LEGAL AND RELATED SERVICES ISSUANCE OF ADOPTION CERTIFICATES AND CUSTODY DECLARATIONS IN HAGUE CONVENTION ADOPTION CASES § 97.1 Definitions. As used in this part: (a) Adoption...

  12. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 4 2010-10-01 2010-10-01 false Crank pins. 230.97 Section 230.97 Transportation... TRANSPORTATION STEAM LOCOMOTIVE INSPECTION AND MAINTENANCE STANDARDS Steam Locomotives and Tenders Driving Gear § 230.97 Crank pins. (a) General provisions. Crank pins shall be securely applied. Securing the fit of...

  13. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  14. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  15. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  16. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 3 2013-07-01 2013-07-01 false Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  17. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  18. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  19. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  20. 40 CFR 97.73 - Notifications.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Notifications. 97.73 Section 97.73 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS Monitoring and Reporting § 97.73 Notifications. (a) The NOX authorized...

  1. 47 CFR 97.203 - Beacon station.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Beacon station. 97.203 Section 97.203... SERVICE Special Operations § 97.203 Beacon station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be a beacon. A holder of...

  2. 47 CFR 97.203 - Beacon station.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Beacon station. 97.203 Section 97.203... SERVICE Special Operations § 97.203 Beacon station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be a beacon. A holder of...

  3. 47 CFR 97.203 - Beacon station.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Beacon station. 97.203 Section 97.203... SERVICE Special Operations § 97.203 Beacon station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be a beacon. A holder of...

  4. 40 CFR 282.97 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 26 2010-07-01 2010-07-01 false 282.97 Section 282.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) SOLID WASTES (CONTINUED) APPROVED UNDERGROUND STORAGE TANK PROGRAMS Approved State Programs § 282.97...

  5. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Element credit. 97.505 Section 97.505 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give...

  6. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Element credit. 97.505 Section 97.505 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give...

  7. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 1 2012-07-01 2012-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  8. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  9. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  10. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 1 2013-07-01 2013-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  11. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 1 2014-07-01 2013-07-01 true Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  12. 7 CFR 97.301 - Commissioner's answer.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Commissioner's answer. 97.301 Section 97.301... PLANT VARIETY AND PROTECTION Appeal to the Secretary § 97.301 Commissioner's answer. (a) The... Secretary in answer to the appellant's petition, including such explanation of the reasons for the action...

  13. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 32 National Defense 3 2012-07-01 2009-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  14. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 3 2010-07-01 2010-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  15. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 3 2011-07-01 2009-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  16. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 32 National Defense 3 2014-07-01 2014-07-01 false Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  17. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  18. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  19. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  20. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  1. 40 CFR 97.73 - Notifications.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Notifications. 97.73 Section 97.73 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS Monitoring and Reporting § 97.73 Notifications. (a) The NOX authorized...

  2. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  3. 25 CFR 700.97 - Residence.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 25 Indians 2 2013-04-01 2013-04-01 false Residence. 700.97 Section 700.97 Indians THE OFFICE OF NAVAJO AND HOPI INDIAN RELOCATION COMMISSION OPERATIONS AND RELOCATION PROCEDURES General Policies and Instructions Definitions § 700.97 Residence. (a) Residence is established by proving that the head of...

  4. 25 CFR 700.97 - Residence.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 25 Indians 2 2010-04-01 2010-04-01 false Residence. 700.97 Section 700.97 Indians THE OFFICE OF NAVAJO AND HOPI INDIAN RELOCATION COMMISSION OPERATIONS AND RELOCATION PROCEDURES General Policies and Instructions Definitions § 700.97 Residence. (a) Residence is established by proving that the head of...

  5. 25 CFR 700.97 - Residence.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 25 Indians 2 2012-04-01 2012-04-01 false Residence. 700.97 Section 700.97 Indians THE OFFICE OF NAVAJO AND HOPI INDIAN RELOCATION COMMISSION OPERATIONS AND RELOCATION PROCEDURES General Policies and Instructions Definitions § 700.97 Residence. (a) Residence is established by proving that the head of...

  6. 25 CFR 700.97 - Residence.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 25 Indians 2 2011-04-01 2011-04-01 false Residence. 700.97 Section 700.97 Indians THE OFFICE OF NAVAJO AND HOPI INDIAN RELOCATION COMMISSION OPERATIONS AND RELOCATION PROCEDURES General Policies and Instructions Definitions § 700.97 Residence. (a) Residence is established by proving that the head of...

  7. 29 CFR 97.30 - Changes.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Changes. 97.30 Section 97.30 Labor Office of the Secretary... GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.30 Changes. (a) General. Grantees... requirements and may make limited program changes to the approved project. However, unless waived by...

  8. 29 CFR 97.30 - Changes.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Changes. 97.30 Section 97.30 Labor Office of the Secretary... GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.30 Changes. (a) General. Grantees... requirements and may make limited program changes to the approved project. However, unless waived by...

  9. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    1997-10-01

    ... 48 Federal Acquisition Regulations System 5 1997-10-01 1997-10-01 false Title. 1352.217-97 Section... Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97 ) (Jan 1987) Unless title to materials and equipment acquired or produced for, or allocated...

  10. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2009-10-01

    ... 48 Federal Acquisition Regulations System 5 2009-10-01 2009-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  11. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2001-10-01

    ... 48 Federal Acquisition Regulations System 5 2001-10-01 2001-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  12. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    1998-10-01

    ... 48 Federal Acquisition Regulations System 5 1998-10-01 1998-10-01 false Title. 1352.217-97 Section... Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title to materials and equipment acquired or produced for, or allocated to,...

  13. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2007-10-01

    ... 48 Federal Acquisition Regulations System 5 2007-10-01 2007-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  14. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2005-10-01

    ... 48 Federal Acquisition Regulations System 5 2005-10-01 2005-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  15. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Question pools. 97.523 Section 97.523... SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining one question pool for each written examination element. Each question pool must contain at least 10 times...

  16. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  17. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  18. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  19. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  20. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  1. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  2. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  3. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  4. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  5. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  6. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  7. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  8. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  9. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Station control. 97.109 Section 97.109 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at...

  10. 40 CFR 97.419 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.419 Section 97.419 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.419...

  11. 40 CFR 97.519 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.519 Section 97.519 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.519...

  12. 40 CFR 97.529 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.529 Section 97.529 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.529...

  13. 40 CFR 97.409 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.409 Section 97.409 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.409...

  14. 40 CFR 97.419 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.419 Section 97.419 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.419...

  15. 40 CFR 97.509 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.509 Section 97.509 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.509...

  16. 40 CFR 97.609 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.609 Section 97.609 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program § 97.609...

  17. 40 CFR 97.529 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.529 Section 97.529 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.529...

  18. 40 CFR 97.429 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.429 Section 97.429 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.429...

  19. 40 CFR 97.509 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.509 Section 97.509 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.509...

  20. 40 CFR 97.429 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.429 Section 97.429 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.429...

  1. 40 CFR 97.519 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.519 Section 97.519 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.519...

  2. 40 CFR 97.409 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.409 Section 97.409 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.409...

  3. 40 CFR 97.429 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.429 Section 97.429 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.429...

  4. 40 CFR 97.529 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.529 Section 97.529 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.529...

  5. 40 CFR 97.509 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.509 Section 97.509 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.509...

  6. 40 CFR 97.519 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false 97.519 Section 97.519 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.519...

  7. 40 CFR 97.409 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false 97.409 Section 97.409 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.409...

  8. 40 CFR 97.419 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false 97.419 Section 97.419 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.419...

  9. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  10. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  11. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  12. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  13. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  14. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  15. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  16. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  17. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  18. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  19. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 32 National Defense 1 2014-07-01 2014-07-01 false Regulations. 9.7 Section 9.7 National Defense... MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7 Regulations. (a) Supplementary regulations and instructions. The Appointing Authority shall, subject to...

  20. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Regulations. 9.7 Section 9.7 National Defense... MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7 Regulations. (a) Supplementary regulations and instructions. The Appointing Authority shall, subject to...

  1. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 32 National Defense 1 2012-07-01 2012-07-01 false Regulations. 9.7 Section 9.7 National Defense... MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7 Regulations. (a) Supplementary regulations and instructions. The Appointing Authority shall, subject to...

  2. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Regulations. 9.7 Section 9.7 National Defense... MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7 Regulations. (a) Supplementary regulations and instructions. The Appointing Authority shall, subject to...

  3. 40 CFR 97.273 - Notifications.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Notifications. 97.273 Section 97.273 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS Monitoring and Reporting § 97.273 Notifications. The CAIR designated...

  4. 40 CFR 97.73 - Notifications.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Notifications. 97.73 Section 97.73 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS Monitoring and Reporting § 97.73 Notifications. (a) The NOX authorized...

  5. 40 CFR 97.54 - Compliance.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Compliance. 97.54 Section 97.54 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Tracking System § 97.54 Compliance. (a) NOX allowance transfer...

  6. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2014-04-01 2014-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  7. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2013-04-01 2013-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  8. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2011-04-01 2011-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  9. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2012-04-01 2011-04-01 true Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  10. 46 CFR 97.11-1 - Posting.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Posting. 97.11-1 Section 97.11-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Stability Letter § 97.11-1 Posting. If a stability letter is issued under § 170.120 of this chapter, it must be...

  11. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  12. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  13. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  14. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  15. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  16. 32 CFR 97.4 - Policy.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Policy. 97.4 Section 97.4 National Defense... INFORMATION IN LITIGATION AND TESTIMONY BY DoD PERSONNEL AS WITNESSES § 97.4 Policy. It is DoD policy that... from public disclosure....

  17. 46 CFR 97.53-1 - Officers.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Officers. 97.53-1 Section 97.53-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Exhibition of Merchant Mariner Credential § 97.53-1 Officers. All officers on a vessel must have their licenses or...

  18. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 1 2010-07-01 2010-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  19. 40 CFR 421.97 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 29 2011-07-01 2009-07-01 true 421.97 Section 421.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY Metallurgical Acid Plants Subcategory § 421.97...

  20. 40 CFR 421.97 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 29 2014-07-01 2012-07-01 true 421.97 Section 421.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY Metallurgical Acid Plants Subcategory § 421.97...

  1. 40 CFR 421.97 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 30 2013-07-01 2012-07-01 true 421.97 Section 421.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY Metallurgical Acid Plants Subcategory § 421.97...

  2. 40 CFR 421.97 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 30 2012-07-01 2012-07-01 false 421.97 Section 421.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY Metallurgical Acid Plants Subcategory § 421.97...

  3. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 1 2012-10-01 2012-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  4. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 1 2011-10-01 2011-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  5. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 1 2013-10-01 2013-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  6. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 42 Public Health 1 2010-10-01 2010-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  7. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 1 2014-10-01 2014-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  8. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  9. 40 CFR 97.355 - Banking.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Banking. 97.355 Section 97.355 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... System § 97.355 Banking. (a) CAIR NOX Ozone Season allowances may be banked for future use or transfer...

  10. 40 CFR 97.355 - Banking.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Banking. 97.355 Section 97.355 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... System § 97.355 Banking. (a) CAIR NOX Ozone Season allowances may be banked for future use or transfer...

  11. 29 CFR 97.31 - Real property.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 1 2013-07-01 2013-07-01 false Real property. 97.31 Section 97.31 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.31 Real property. (a) Title. Subject to the obligations and conditions set forth in this section, title to real...

  12. 29 CFR 97.31 - Real property.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Real property. 97.31 Section 97.31 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.31 Real property. (a) Title. Subject to the obligations and conditions set forth in this section, title to real...

  13. 19 CFR 4.97 - Salvage vessels.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 19 Customs Duties 1 2010-04-01 2010-04-01 false Salvage vessels. 4.97 Section 4.97 Customs Duties... VESSELS IN FOREIGN AND DOMESTIC TRADES General § 4.97 Salvage vessels. (a) Only a vessel of the United...) or (e) of this section, shall engage in any salvage operation in territorial waters of the...

  14. 50 CFR 648.97 - Closed areas.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 50 Wildlife and Fisheries 10 2011-10-01 2011-10-01 false Closed areas. 648.97 Section 648.97... Multispecies and Monkfish Fisheries § 648.97 Closed areas. (a) Oceanographer Canyon Closed Area. No fishing... Closed Area (copies of a chart depicting this area are available from the Regional Administrator...

  15. 50 CFR 648.97 - Closed areas.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 50 Wildlife and Fisheries 12 2014-10-01 2014-10-01 false Closed areas. 648.97 Section 648.97... Multispecies and Monkfish Fisheries § 648.97 Closed areas. (a) Oceanographer Canyon Closed Area. No fishing... Closed Area (copies of a chart depicting this area are available from the Regional Administrator...

  16. 40 CFR 97.73 - Notifications.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Notifications. 97.73 Section 97.73 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS Monitoring and Reporting § 97.73 Notifications. (a) The NOX authorized...

  17. 7 CFR 97.301 - Commissioner's answer.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Commissioner's answer. 97.301 Section 97.301... PLANT VARIETY AND PROTECTION Appeal to the Secretary § 97.301 Commissioner's answer. (a) The... Secretary in answer to the appellant's petition, including such explanation of the reasons for the action...

  18. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Authorized transmissions. 97.111 Section 97.111 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of...

  19. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Authorized transmissions. 97.111 Section 97.111 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of...

  20. 40 CFR 97.355 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.355 Section 97.355 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... System § 97.355 Banking. (a) CAIR NOX Ozone Season allowances may be banked for future use or transfer...

  1. 40 CFR 97.355 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.355 Section 97.355 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... System § 97.355 Banking. (a) CAIR NOX Ozone Season allowances may be banked for future use or transfer...

  2. 40 CFR 97.355 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.355 Section 97.355 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... System § 97.355 Banking. (a) CAIR NOX Ozone Season allowances may be banked for future use or transfer...

  3. 28 CFR 97.12 - Employee training.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 28 Judicial Administration 2 2011-07-01 2011-07-01 false Employee training. 97.12 Section 97.12 Judicial Administration DEPARTMENT OF JUSTICE (CONTINUED) STANDARDS FOR PRIVATE ENTITIES PROVIDING PRISONER OR DETAINEE SERVICES § 97.12 Employee training. Private prisoner transport companies must require the completion of a minimum of 100 hours...

  4. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  5. Characterization of uranium and uranium-zirconium deposits produced in electrorefining of spent nuclear fuel

    SciTech Connect

    Totemeier, T.C.

    1997-09-01

    This paper describes the metallurgical characterization of deposits produced in molten salt electrorefining of uranium and uranium - 10.% zirconium alloy. The techniques of characterization are described with emphasis on considerations given to the radioactive and pyrophoric nature of the samples. The morphologies observed and their implications for deposit performance are also presented - samples from pure uranium deposits were comprised of chains of uranium crystals with a characteristic rhomboidal shape, while morphologies of samples from deposits containing zirconium showed more polycrystalline features. Zirconium was found to be present as a second, zirconium metal phase at or very near the uranium-zirconium dendrite surfaces. Higher collection efficiencies and total deposit weights were observed for the uranium-zirconium deposits; this performance increase is likely a result of better mechanical properties exhibited by the uranium-zirconium dendrite morphology. 18 refs., 10 figs., 1 tab.

  6. Nanophase Nickel-Zirconium Alloys for Fuel Cells

    NASA Technical Reports Server (NTRS)

    Narayanan, Sekharipuram; Whitacre, jay; Valdez, Thomas

    2008-01-01

    Nanophase nickel-zirconium alloys have been investigated for use as electrically conductive coatings and catalyst supports in fuel cells. Heretofore, noble metals have been used because they resist corrosion in the harsh, acidic fuel cell interior environments. However, the high cost of noble metals has prompted a search for less-costly substitutes. Nickel-zirconium alloys belong to a class of base metal alloys formed from transition elements of widely different d-electron configurations. These alloys generally exhibit unique physical, chemical, and metallurgical properties that can include corrosion resistance. Inasmuch as corrosion is accelerated by free-energy differences between bulk material and grain boundaries, it was conjectured that amorphous (glassy) and nanophase forms of these alloys could offer the desired corrosion resistance. For experiments to test the conjecture, thin alloy films containing various proportions of nickel and zirconium were deposited by magnetron and radiofrequency co-sputtering of nickel and zirconium. The results of x-ray diffraction studies of the deposited films suggested that the films had a nanophase and nearly amorphous character.

  7. Studies on the Characteristic of Zirconium-Tritium Reaction

    NASA Astrophysics Data System (ADS)

    Huang, Gang; Long, Xing-Gui; Peng, Shu-Ming; Liang, Jian-Hua; Yang, Ben-Fu

    2011-02-01

    The p- c-T curves of tritium absorption and desorption of zirconium were measured using the method of step equilibrium by stepping up the tritium quantity on an experimental apparatus of metal hydride. The p- c-T curves for tritium have one plateau at temperature range from 450 to 500°C and two plateaus at temperature above 600°C. The thermodynamic parameters of the different phases were determined according to the van't Hoff equation. The hysteresis effect was observed in reversible process of tritium absorption and desorption of zirconium on our experimental condition. The tritium absorption behavior by zirconium in the temperature range from 450 to 620°C and desorption behavior of zirconium in the temperature range from 775 to 875°C have been investigated. A method of the reaction rate analysis was proposed and examined for determining the rate constant. The apparent activation energy obtained by this analysis for the absorption and the desorption were (-16.8 ± 0.8) kJ·mol-1 and (57.7 ± 1.6) kJ·mol-1, respectively.

  8. Mineral resource of the month: zirconium and hafnium

    USGS Publications Warehouse

    Gambogi, Joseph

    2007-01-01

    Zirconium and hafnium are corrosion-resistant metals that are grouped in the same family as titanium on the periodic table. The two elements commonly occur in oxide and silicate minerals and have significant economic importance in everything from ink, ceramics and golf shoes to nuclear fuel rods.

  9. Phosphorus Recovery Using Zirconium-Loaded Saponified Orange Juice Residue

    NASA Astrophysics Data System (ADS)

    Harada, Hiroyuki; Kondo, Mitsunori; Biswas, Biplob K.; Ohura, Seichirou; Inoue, Katsutoshi; Ishikawa, Susumu; Kawakita, Hidetaka; Ohto, Keisuke

    Zirconium was immobilized to orange juice residue, to investigate the feasibility of using zirconium-loaded saponified orange juice residue (Zr-SOJR) for phosphorus recovery from secondary effluent and the extraction solution from incinerated sewage sludge ash by using H2SO4 and HCl. These had phosphorus concentrations of 68.2 mg/dm3 and 5.9 mg/dm3, respectively. The phosphorus removal rate secondary effluent increased with an increasing solid/liquid ratio in batch experiments. The adsorption capacity of Zr-SOJR was also compared with those obtained using a synthetic phosphorus solution and using zirconium-loaded ferrite. The prepared absorbent was effective for phosphorus removal and exhibited a reasonably high sorption capacity, twice that of zirconium ferrite. Secondary effluent was treated by packed column, and this reached break-through after 300 bed volumes. The results from phosphorous extraction from the ash indicate that can be treated with acid to efficiently recover phosphorous and thus can be absorbed by Zr-SOJR.

  10. Method for calcining nuclear waste solutions containing zirconium and halides

    DOEpatents

    Newby, Billie J.

    1979-01-01

    A reduction in the quantity of gelatinous solids which are formed in aqueous zirconium-fluoride nuclear reprocessing waste solutions by calcium nitrate added to suppress halide volatility during calcination of the solution while further suppressing chloride volatility is achieved by increasing the aluminum to fluoride mole ratio in the waste solution prior to adding the calcium nitrate.

  11. Manufacturing process to reduce large grain growth in zirconium alloys

    DOEpatents

    Rosecrans, Peter M.

    1987-01-01

    A method of treating cold-worked zirconium alloys to reduce large grain gth during thermal treatment at temperatures above the recrystallization temperature of the alloy comprising heating the cold-worked alloy between about 1300.degree.-1350.degree. F. for 1 to 3 hours prior to treatment above its recrystallization temperature.

  12. Dynamic nuclear polarisation NMR of nanosized zirconium phosphate polymer fillers.

    PubMed

    Ziarelli, Fabio; Casciola, Mario; Pica, Monica; Donnadio, Anna; Aussenac, Fabien; Sauvée, Claire; Capitani, Donatella; Viel, Stéphane

    2014-09-11

    Surface functionalisation with organic modifiers of multi-layered zirconium phosphate (ZrP) nanoparticles used as polymer fillers can be directly probed by dynamic nuclear polarisation NMR, which provides unambiguous evidence of the presence of P-O-C chemical bonds at the surface of the ZrP layers, thereby confirming successful functionalisation.

  13. Method for applying corrosion resistant metallic coating of zirconium nitride

    SciTech Connect

    Bryan, W.J.; Corsetti, L.V.

    1993-07-13

    A process is described for enhancing the wear and corrosion resistance of a cladding tube for a nuclear fuel rod, comprising reactively depositing zirconium nitride on the surface of said cladding tube by a cathodic arc plasma deposition process to form a thin wear resistant coating.

  14. Layered zirconium phosphonate with inorganic–organic hybrid structure: Preparation and its assembly with DNA

    SciTech Connect

    Liu, Li-Min; Lu, Guo-Yuan; Jiang, Li-Ping; Zhu, Jun-Jie

    2014-07-01

    An aminoethoxy-functionalized zirconium phosphonate (Zr(O{sub 3}POCH{sub 2}CH{sub 2}NH{sub 2}){sub 2}·3H{sub 2}O), abbreviated as ZrRP (R=OCH{sub 2}CH{sub 2}NH{sub 2}), with layered structure has been synthesized. This layered compound possesses the characteristic of inorganic–organic hybrid, due to the covalently linked aminoethoxy in the host layer. The anion exchanged property of this zirconium phosphonate is suitable for the direct intercalation of negatively charged DNA, which is different from these reported zirconium phosphates or zirconium phosphonates. As a precursor, this prepared zirconium phosphonate was utilized to fabricate a novel DNA/ZrRP binary hybrid via a delamination-reassembly procedure. The release behavior of DNA from the DNA/ZrRP composite was investigated at different medium pH, because the combination between zirconium phosphonate sheets and DNA was pH-dependent sensitively. Moreover, the helical conformation of DNA was almost retained after the intercalation and release process. These properties of the DNA/ZrRP composite suggested the potential application of layered zirconium phosphonate as a non-viral vector in gene delivery. - Graphical abstract: The intercalation of DNA into zirconium phosphonate and the release of DNA from the interlayer of zirconium phosphonate. - Highlights: ●A layered aminoethoxy-functionalized zirconium phosphonate has been synthesized. ●DNA was intercalated directly into the prepared zirconium phosphonate. ●A novel zirconium phosphonate/DNA binary hybrid was fabricated. ●DNA can be reversibly released from the interlayer of zirconium phosphonate. ●The intercalation/release processes do not induce the denaturalization of DNA.

  15. Syntheses and structural characterization of zirconium-tin and zirconium-lead binary and ternary systems

    SciTech Connect

    Kwon, Y.U.

    1991-01-28

    The binary zirconium-tin system was reinvestigated. The A15 phase appears to be a line phase with a Zr{sub 4}Sn composition. The Zr{sub 5}Sn{sub 3} (Mn{sub 5}Si{sub 3}-type) and Zr{sub 5}Sn{sub 4} (Ti{sub 5}Ga{sub 4}-type) compounds are line phases below 1000{degree}C, the latter being a self-interstitial phase of the former. ZrSn{sub 2} is the tin-richest phase. There is an one-phase region between these phases with partial self-interstitials at high temperatures. The zirconium-lead system behaves similarly: there are an A15 phase with a Zr{sub {approximately}5.8}Pb composition, Zr{sub 5}Pb{sub 3} (Mn{sub 5}Si{sub 3}-type) and Zr{sub 5}Pb{sub 4} (Ti{sub 5}Ga{sub 4-type}) compounds, and a high temperature solid solution between Zr{sub 5}Pb{sub >3.5} and Zr{sub 5}Pb{sub 4} from below 1000{degree}C; however, the ZrSn{sub 2} analogue is not formed. The Mn{sub 5}Si{sub 3}-type phases in these systems can accommodate third elements interstitially to form stoichiometric compounds Zr{sub 5}Sn{sub 3}Z (Z = B, C, N, O, Al, Si, P, S, Cu, Zn, Ga, Ge, and As and Se) and Zr{sub 5}Pb{sub 3}Z (Z = Al, Si, P, S, Fe, Co, Ni, Cu, Zn, Ga, Ge, As, Se, Ag, Cd, In, Sn, Sb and Te) as well as their self-interstitial derivatives. The systems Zr-Sn-T, T = Fe, Co and Ni, did not produce stoichiometric interstitial phases Zr{sub 5}Sn{sub 3}T. Instead, the interstitial phases for these elements are formed only with excess tin that partially occupies the interstitial site together with a T element. Reducing the amount of tin in these systems yields two new phases; Zr{sub 5}Sn{sub 2+x}Fe{sub 1-x} (0 {le} {times} {le} 0.28) (W{sub 5}Si{sub 3}-type) and Zr{sub 6}Sn{sub 2}Fe (Zr{sub 6}Al{sub 2}Co-type) as characterized by X-ray single crystal analyses. A cobalt analogue for the latter was also synthesized.

  16. 46 CFR 97.12-5 - Manual.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Manual. 97.12-5 Section 97.12-5 Shipping COAST GUARD...-5 Manual. The manual on the “Stowage of Bulk Cargoes Such as Ore, Ore Concentrates, and Similar... compliance with the requirements of § 97.12-1(a). 1 Copies of this manual are on file at Coast...

  17. Nuclear-grade zirconium prepared by combining combustion synthesis with molten-salt electrorefining technique

    NASA Astrophysics Data System (ADS)

    Li, Hui; Nersisyan, Hayk H.; Park, Kyung-Tae; Park, Sung-Bin; Kim, Jeong-Guk; Lee, Jeong-Min; Lee, Jong-Hyeon

    2011-06-01

    Zirconium has a low absorption cross-section for neutrons, which makes it an ideal material for use in nuclear reactor applications. However, hafnium typically contained in zirconium causes it to be far less useful for nuclear reactor materials because of its high neutron-absorbing properties. In the present study, a novel effective method has been developed for the production of hafnium-free zirconium. The process includes two main stages: magnesio-thermic reduction of ZrSiO 4 under a combustion mode, to produce zirconium silicide (ZrSi), and recovery of hafnium-free zirconium by molten-salt electrorefining. It was found that, depending on the electrorefining procedure, it is possible to produce zirconium powder with a low hafnium content: 70 ppm, determined by ICP-AES analysis.

  18. The effect of zirconium on the cyclic oxidation of NiCrAl alloys

    NASA Technical Reports Server (NTRS)

    Barrett, C. A.; Khan, A. S.; Lowell, C. E.

    1981-01-01

    This paper examines results with cyclic oxidation tests of Ni(9-20) Cr(15-30) Al-(x)Zr alloys carried out at 1100 C and 1200 C in static air. The concentration of zirconium varies from 0 to 0.63 atomic percent. Significant aluminum penetration is found in metallographic and electron microscopic examination of oxidized surfaces. Small amounts of zirconium lead to minimal penetration, and with increased zirconium content pronounced oxide penetration is observed.

  19. Effects of solutes on damage production and recovery in zirconium

    SciTech Connect

    Zee, R.H.; Birtcher, R.C.; MacEwen, S.R.; Abromeit, C.

    1986-04-01

    Dilute zirconium-based alloys and pure zirconium were irradiated at 10 K with spallation neutrons at IPNS. Four types of alloys - Zr-Ti, Zr-Sn, Zr-Dy and Zr-Au - each with three concentration levels, were used. Low-temperature resistivity damage rates are enhanced by the presence of any of the four solutes. The greatest enhancement was produced by Au while the least by Dy. Within each alloy group, damage production also increased but at a decreasing rate, with increasing concentration. Post-irradiation annealing experiments, up to 400 K, showed that all four solutes suppress recovery due to interstitial migration, indicative of interstitial trapping by the solutes. Vacancy recovery is also suppressed by the presence of Sn, Dy or Au. The effect of Ti is to shift this stage to lower temperature. No clear correlation between the results with solute size was detected.

  20. Adhesion Improvement of Zirconium Coating on Polyurethane Modified by Plasmas

    NASA Astrophysics Data System (ADS)

    Gao, Yi; Hao, Xiaofei; Liu, Jiwei

    2016-02-01

    In order to improve the adhesion of the middle frequency magnetic sputtered zirconium coating on a polyurethane film, an anode layer source was used to pretreat the polyurethane film with nitrogen and oxygen ions. SEMs and AFM roughness profiles of treated samples and the contrast groups were obtained. Besides, XPS survey spectrums and high resolution spectrums were also investigated. The adhesion test revealed that ion bombardment could improve the adhesion to the polyurethane coating substrate. A better etching result of oxygen ions versus nitrogen predicts a higher bonding strength of zirconium coating on polyurethane and, indeed, the highest bonding strengths are for oxygen ion bombardment upto 13.3 MPa. As demonstrated in X-ray photoelectron spectroscopy, the oxygen ion also helps to introduce more active groups, and, therefore, it achieves a high value of adhesion strength.

  1. Corrosion testing of stainless steel-zirconium metal waste forms

    SciTech Connect

    Abraham, D.P.; Simpson, L.J.; Devries, M.J.; McDeavitt, S.M.

    1999-07-01

    Stainless steel-zirconium (SS-Zr) alloys have been developed as waste forms for the disposal of metallic waste generated during the electrometallurgical treatment of spent nuclear fuel. The waste forms incorporate irradiated cladding hulls, components of the alloy fuel, noble metal fission products, and actinide elements. The baseline waste form is a stainless steel-15 wt% zirconium (SS-15Zr) alloy. This article presents microstructures and some of the corrosion studies being conducted on the waste form alloys. Electrochemical corrosion, immersion corrosion, and vapor hydration tests have been performed on various alloy compositions to evaluate corrosion behavior and resistance to selective leaching of simulated fission products. The SS-Zr waste forms immobilize and retain fission products very effectively and show potential for acceptance as high-level nuclear waste forms.

  2. Corrosion behavior of stainless steel-zirconium alloy waste forms

    SciTech Connect

    Abraham, D.P.; Simpson, L.J.; DeVries, M.J.; Callahan, D.E.

    1999-07-01

    Stainless steel-zirconium (SS-Zr) alloys are being considered as waste forms for the disposal of metallic waste generated during the electrometallurgical treatment of spent nuclear fuel. The baseline waste form for spent fuels from the EBR-11 reactor is a stainless steel-15 wt.% zirconium (SS-15Zr) alloy. This article briefly reviews the microstructure of various SS-Zr waste form alloys and presents results of immersion corrosion and electrochemical corrosion tests performed on these alloys. The electrochemical tests show that the corrosion behavior of SS-Zr alloys is comparable to those of other alloys being considered for the Yucca Mountain geologic repository. The immersion tests demonstrate that the SS-Zr alloys are resistant to selective leaching of fission product elements and, hence, suitable as candidates for high-level nuclear waste forms.

  3. Alternative Processing of High Temperature Hafnium and Zirconium Based Materials

    NASA Technical Reports Server (NTRS)

    Gasch, Matthew; Gusman, Michael; Ellerby, Don; Irby, Edward; Johnson, Sylvia M.

    2003-01-01

    The behavior of refractory hafnium and zirconium based materials are being investigated at NASA Ames as part of ongoing research aimed at developing superior heat resistant materials for aerospace applications. Hafnium and zirconium diboride based materials have shown high temperature capabilities in simulated reentry environments indicating that these materials may successfully operate as reusable oxidation resistant components for leading edge applications. Due to the refractory nature of these materials, processing of fine-grained uniform microstructures poses a number of challenges. To better understand the process-property-microstructure relationship, processing of these materials has been carried out with conventional hot pressing in addition to the novel approach of Spark Plasma Sintering (SPS). The two processing methods are compared and contrasted in an evaluation of the sintering behavior of high temperature diboride based materials and preliminary physical and mechanical properties are presented.

  4. Controlled deposition of plasma activated coatings on zirconium substrates

    NASA Astrophysics Data System (ADS)

    Akhavan, Behnam; Bilek, Marcela

    2015-12-01

    Zirconium-based alloys are promising materials for orthopedic prostheses due to their low toxicity, superb corrosion resistivity, and favorable mechanical properties. The integration of such bio-implantable devices with local host tissues can strongly be improved by the development of a plasma polymerized acetylene and nitrogen (PPAN) that immobilizes bio-active molecules. The surface chemistry of PPAN is critically important as it plays a key role in affecting the surface free energy that alters the functionality of bio-active molecules at the surface. The cross-linking degree of PPAN is another key property that directly influences the water-permeability and thus also the stability of films in aqueous media. In this study we demonstrate that by simply tuning the zirconium bias voltage, control over the surface chemistry and cross-linking degree of PANN is achieved.

  5. Thermodynamic and kinetic studies of As(V) removal from water by zirconium oxide-coated marine sand.

    PubMed

    Khan, Tabrez Alam; Chaudhry, Saif Ali; Ali, Imran

    2013-08-01

    Arsenic contamination of groundwater is a major threat to human beings globally. Among various methods available for arsenic removal, adsorption is fast, inexpensive, selective, accurate, reproducible and eco-friendly in nature. The present paper describes removal of arsenate from water on zirconium oxide-coated sand (novel adsorbent). In the present work, zirconium oxide-coated sand was prepared and characterised by infrared and X-ray diffraction techniques. Batch experiments were performed to optimise different adsorption parameters such as initial arsenate concentration (100-1,000 μg/L), dose (1-8 g/L), pH of the solution (2-14), contact time (15-150 min.), and temperature (20, 30, 35 and 40 °C). The experimental data were analysed by Langmuir, Freundlich, Temkin and Dubinin-Radushkevich isotherm models. Furthermore, thermodynamic and kinetic parameters were evaluated to know the mode of adsorption between ZrOCMS and As(V). The maximum removal of arsenic, 97 %, was achieved at initial arsenic concentration of 200 μg/L, after 75 min at dosage of 5.0 g/L, pH 7.0 and 27 ± 2 °C. For 600 μg/L concentration, the maximum Langmuir monolayer adsorption capacity was found to be 270 μg/g at 35 °C. Kinetic modelling data indicated that adsorption process followed pseudo-second-order kinetics. The mechanism is controlled by liquid film diffusion model. Thermodynamic parameter, ΔH°, was -57.782, while the values of ΔG° were -9.460, -12.183, -13.343 and -13.905 kJ/mol at 20, 30, 35 and 40 °C, respectively, suggesting exothermic and spontaneous nature of the process. The change in entropy, ΔS°= -0.23 kJ/mol indicated that the entropy decreased due to adsorption of arsenate ion onto the solid adsorbent. The results indicated that the reported zirconium oxide-coated marine sand (ZrOCMS) was good adsorbent with 97 % removal capacity at 200 μg/L concentration. It is interesting to note that the permissible limit of arsenic as per World Health Organization is 10

  6. 7 CFR 97.157 - Professional conduct.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.157 Professional conduct. Attorneys and agents appearing before the Office shall conform to the standards of ethical and professional conduct, generally... 7 Agriculture 3 2010-01-01 2010-01-01 false Professional conduct. 97.157 Section...

  7. 32 CFR 97.5 - Responsibilities.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Responsibilities. 97.5 Section 97.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN RELEASE... Responsibilities. (a) The General Counsel, Department of Defense, shall provide general policy and...

  8. 32 CFR 97.5 - Responsibilities.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Responsibilities. 97.5 Section 97.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN RELEASE... Responsibilities. (a) The General Counsel, Department of Defense, shall provide general policy and...

  9. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY LIQUORS âTIED-HOUSEâ Exceptions §...

  10. 21 CFR 1.97 - Bonds.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 1 2013-04-01 2013-04-01 false Bonds. 1.97 Section 1.97 Food and Drugs FOOD AND... rendering it other than a food, drug, device, or cosmetic, in such manner as is prescribed for such bond in... this regulation in any case unless the district director is in full agreement with the action....

  11. 21 CFR 1.97 - Bonds.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 1 2012-04-01 2012-04-01 false Bonds. 1.97 Section 1.97 Food and Drugs FOOD AND... rendering it other than a food, drug, device, or cosmetic, in such manner as is prescribed for such bond in... this regulation in any case unless the district director is in full agreement with the action....

  12. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2014-04-01 2014-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY ALCOHOL âTIED-HOUSEâ Exceptions §...

  13. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2012-04-01 2012-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY LIQUORS âTIED-HOUSEâ Exceptions §...

  14. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2011-04-01 2011-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY LIQUORS âTIED-HOUSEâ Exceptions §...

  15. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2013-04-01 2013-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY ALCOHOL âTIED-HOUSEâ Exceptions §...

  16. 40 CFR 97.262 - Notification.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.262 Notification. (a) Notification of recordation. Within 5 business days of recordation of a CAIR SO2 allowance... of receipt of a CAIR SO2 allowance transfer that fails to meet the requirements of § 97.261(a),...

  17. 40 CFR 97.262 - Notification.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.262 Notification. (a) Notification of recordation. Within 5 business days of recordation of a CAIR SO2 allowance... of receipt of a CAIR SO2 allowance transfer that fails to meet the requirements of § 97.261(a),...

  18. 40 CFR 97.262 - Notification.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.262 Notification. (a) Notification of recordation. Within 5 business days of recordation of a CAIR SO2 allowance... of receipt of a CAIR SO2 allowance transfer that fails to meet the requirements of § 97.261(a),...

  19. 40 CFR 97.627 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Account error. 97.627 Section 97.627 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR SO2 Group 1 Trading Program §...

  20. 40 CFR 97.262 - Notification.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.262 Notification. (a) Notification of recordation. Within 5 business days of recordation of a CAIR SO2 allowance... of receipt of a CAIR SO2 allowance transfer that fails to meet the requirements of § 97.261(a),...

  1. 40 CFR 97.262 - Notification.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.262 Notification. (a) Notification of recordation. Within 5 business days of recordation of a CAIR SO2 allowance... of receipt of a CAIR SO2 allowance transfer that fails to meet the requirements of § 97.261(a),...

  2. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 36 Parks, Forests, and Public Property 1 2010-07-01 2010-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  3. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 36 Parks, Forests, and Public Property 1 2012-07-01 2012-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  4. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 36 Parks, Forests, and Public Property 1 2014-07-01 2014-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  5. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 36 Parks, Forests, and Public Property 1 2011-07-01 2011-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  6. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) NAVAL STORES REGULATIONS...

  7. 28 CFR 97.30 - Enforcement.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 28 Judicial Administration 2 2010-07-01 2010-07-01 false Enforcement. 97.30 Section 97.30 Judicial Administration DEPARTMENT OF JUSTICE (CONTINUED) STANDARDS FOR PRIVATE ENTITIES PROVIDING PRISONER OR DETAINEE... violation; (b) Be liable to the United States for the costs of prosecution; and (c) Make restitution to...

  8. 28 CFR 97.30 - Enforcement.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 28 Judicial Administration 2 2011-07-01 2011-07-01 false Enforcement. 97.30 Section 97.30 Judicial Administration DEPARTMENT OF JUSTICE (CONTINUED) STANDARDS FOR PRIVATE ENTITIES PROVIDING PRISONER OR DETAINEE... violation; (b) Be liable to the United States for the costs of prosecution; and (c) Make restitution to...

  9. 21 CFR 808.97 - Washington.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Washington. 808.97 Section 808.97 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES EXEMPTIONS FROM FEDERAL PREEMPTION OF STATE AND LOCAL MEDICAL DEVICE REQUIREMENTS Listing of Specific...

  10. 21 CFR 808.97 - Washington.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 21 Food and Drugs 8 2011-04-01 2011-04-01 false Washington. 808.97 Section 808.97 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES EXEMPTIONS FROM FEDERAL PREEMPTION OF STATE AND LOCAL MEDICAL DEVICE REQUIREMENTS Listing of Specific...

  11. 21 CFR 808.97 - Washington.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 21 Food and Drugs 8 2014-04-01 2014-04-01 false Washington. 808.97 Section 808.97 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES EXEMPTIONS FROM FEDERAL PREEMPTION OF STATE AND LOCAL MEDICAL DEVICE REQUIREMENTS Listing of Specific...

  12. 21 CFR 808.97 - Washington.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 21 Food and Drugs 8 2013-04-01 2013-04-01 false Washington. 808.97 Section 808.97 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES EXEMPTIONS FROM FEDERAL PREEMPTION OF STATE AND LOCAL MEDICAL DEVICE REQUIREMENTS Listing of Specific...

  13. 21 CFR 808.97 - Washington.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 21 Food and Drugs 8 2012-04-01 2012-04-01 false Washington. 808.97 Section 808.97 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL DEVICES EXEMPTIONS FROM FEDERAL PREEMPTION OF STATE AND LOCAL MEDICAL DEVICE REQUIREMENTS Listing of Specific...

  14. 47 CFR 97.525 - Accrediting VEs.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Accrediting VEs. 97.525 Section 97.525 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... accrediting VEs on the basis of race, sex, religion or national origin; nor on the basis of membership...

  15. 47 CFR 97.525 - Accrediting VEs.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Accrediting VEs. 97.525 Section 97.525 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... accrediting VEs on the basis of race, sex, religion or national origin; nor on the basis of membership...

  16. 47 CFR 97.525 - Accrediting VEs.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Accrediting VEs. 97.525 Section 97.525 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... accrediting VEs on the basis of race, sex, religion or national origin; nor on the basis of membership...

  17. 47 CFR 97.525 - Accrediting VEs.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Accrediting VEs. 97.525 Section 97.525 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... accrediting VEs on the basis of race, sex, religion or national origin; nor on the basis of membership...

  18. 47 CFR 97.521 - VEC qualifications.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false VEC qualifications. 97.521 Section 97.521 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... registered without regard to race, sex, religion, national origin or membership (or lack thereof) in...

  19. 47 CFR 97.521 - VEC qualifications.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false VEC qualifications. 97.521 Section 97.521 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... registered without regard to race, sex, religion, national origin or membership (or lack thereof) in...

  20. 47 CFR 97.521 - VEC qualifications.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false VEC qualifications. 97.521 Section 97.521 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... registered without regard to race, sex, religion, national origin or membership (or lack thereof) in...

  1. 47 CFR 97.525 - Accrediting VEs.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Accrediting VEs. 97.525 Section 97.525 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... accrediting VEs on the basis of race, sex, religion or national origin; nor on the basis of membership...

  2. 47 CFR 97.521 - VEC qualifications.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false VEC qualifications. 97.521 Section 97.521 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... registered without regard to race, sex, religion, national origin or membership (or lack thereof) in...

  3. 47 CFR 97.521 - VEC qualifications.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false VEC qualifications. 97.521 Section 97.521 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... registered without regard to race, sex, religion, national origin or membership (or lack thereof) in...

  4. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 14 Aeronautics and Space 2 2011-01-01 2011-01-01 false Aeronautical knowledge. 61.97 Section 61.97... knowledge. (a) General. A person who applies for a recreational pilot certificate must receive and log... knowledge areas of paragraph (b) of this section that apply to the aircraft category and class rating...

  5. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 14 Aeronautics and Space 2 2014-01-01 2014-01-01 false Aeronautical knowledge. 61.97 Section 61.97... knowledge. (a) General. A person who applies for a recreational pilot certificate must receive and log... knowledge areas of paragraph (b) of this section that apply to the aircraft category and class rating...

  6. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 14 Aeronautics and Space 2 2012-01-01 2012-01-01 false Aeronautical knowledge. 61.97 Section 61.97... knowledge. (a) General. A person who applies for a recreational pilot certificate must receive and log... knowledge areas of paragraph (b) of this section that apply to the aircraft category and class rating...

  7. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 14 Aeronautics and Space 2 2013-01-01 2013-01-01 false Aeronautical knowledge. 61.97 Section 61.97... knowledge. (a) General. A person who applies for a recreational pilot certificate must receive and log... knowledge areas of paragraph (b) of this section that apply to the aircraft category and class rating...

  8. 40 CFR 97.156 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Account error. 97.156 Section 97.156... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any CAIR NOX Allowance Tracking System account. Within 10 business days of making...

  9. 40 CFR 97.627 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.627 Section 97.627... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  10. 40 CFR 97.427 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Account error. 97.427 Section 97.427... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  11. 40 CFR 97.427 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Account error. 97.427 Section 97.427... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  12. 40 CFR 97.727 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Account error. 97.727 Section 97.727... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  13. 40 CFR 97.427 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.427 Section 97.427... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  14. 40 CFR 97.156 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Account error. 97.156 Section 97.156... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any CAIR NOX Allowance Tracking System account. Within 10 business days of making...

  15. 40 CFR 97.156 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.156 Section 97.156... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any CAIR NOX Allowance Tracking System account. Within 10 business days of making...

  16. 40 CFR 97.727 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.727 Section 97.727... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  17. 40 CFR 97.56 - Account error.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Account error. 97.56 Section 97.56... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any NOX Allowance Tracking System account. Within 10 business days of making...

  18. 40 CFR 97.56 - Account error.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Account error. 97.56 Section 97.56... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any NOX Allowance Tracking System account. Within 10 business days of making...

  19. 40 CFR 97.56 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Account error. 97.56 Section 97.56... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any NOX Allowance Tracking System account. Within 10 business days of making...

  20. 40 CFR 97.156 - Account error.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Account error. 97.156 Section 97.156... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any CAIR NOX Allowance Tracking System account. Within 10 business days of making...

  1. 40 CFR 97.56 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Account error. 97.56 Section 97.56... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any NOX Allowance Tracking System account. Within 10 business days of making...

  2. 40 CFR 97.56 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.56 Section 97.56... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any NOX Allowance Tracking System account. Within 10 business days of making...

  3. 40 CFR 97.727 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Account error. 97.727 Section 97.727... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  4. 40 CFR 97.627 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Account error. 97.627 Section 97.627... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  5. 40 CFR 97.527 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Account error. 97.527 Section 97.527... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any Allowance Management System account. Within 10 business days of making...

  6. 40 CFR 97.156 - Account error.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Account error. 97.156 Section 97.156... Account error. The Administrator may, at his or her sole discretion and on his or her own motion, correct any error in any CAIR NOX Allowance Tracking System account. Within 10 business days of making...

  7. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  8. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  9. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  10. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  11. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  12. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2013-04-01 2013-04-01 false Benzene. 21.97 Section 21... TREASURY ALCOHOL FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  13. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2011-04-01 2011-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  14. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  15. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2012-04-01 2012-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  16. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2014-04-01 2014-04-01 false Benzene. 21.97 Section 21... TREASURY ALCOHOL FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  17. 40 CFR 97.406 - Standard requirements.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program... each TR NOX Annual source and each TR NOX Annual unit at the source shall comply with the monitoring... accordance with §§ 97.430 through 97.435 shall be used to calculate allocations of TR NOX Annual...

  18. 40 CFR 97.406 - Standard requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program... each TR NOX Annual source and each TR NOX Annual unit at the source shall comply with the monitoring... accordance with §§ 97.430 through 97.435 shall be used to calculate allocations of TR NOX Annual...

  19. 40 CFR 97.406 - Standard requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program... each TR NOX Annual source and each TR NOX Annual unit at the source shall comply with the monitoring... accordance with §§ 97.430 through 97.435 shall be used to calculate allocations of TR NOX Annual...

  20. 40 CFR 97.506 - Standard requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading... each TR NOX Ozone Season source and each TR NOX Ozone Season unit at the source shall comply with the... Season allowances under §§ 97.511(a)(2) and (b) and 97.512 and to determine compliance with the TR...

  1. 40 CFR 97.506 - Standard requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading... each TR NOX Ozone Season source and each TR NOX Ozone Season unit at the source shall comply with the... Season allowances under §§ 97.511(a)(2) and (b) and 97.512 and to determine compliance with the TR...

  2. 40 CFR 97.506 - Standard requirements.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading... each TR NOX Ozone Season source and each TR NOX Ozone Season unit at the source shall comply with the... Season allowances under §§ 97.511(a)(2) and (b) and 97.512 and to determine compliance with the TR...

  3. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 4 2014-10-01 2014-10-01 false Crank pins. 230.97 Section 230.97 Transportation Other Regulations Relating to Transportation (Continued) FEDERAL RAILROAD ADMINISTRATION, DEPARTMENT OF TRANSPORTATION STEAM LOCOMOTIVE INSPECTION AND MAINTENANCE STANDARDS Steam Locomotives and Tenders Driving...

  4. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 36 Parks, Forests, and Public Property 1 2013-07-01 2013-07-01 false Assessment work. 9.7 Section... MANAGEMENT Mining and Mining Claims § 9.7 Assessment work. (a) An access permit and approved plan of operations must be obtained by a claimant prior to the performance of any assessment work required by...

  5. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... that has an inside diameter— (a) Larger than three inches, must meet the requirements in 33 CFR 154.500... cargo pump or pump discharge relief valve setting, but not less than 100 pounds per square inch. 46 CFR... 46 Shipping 2 2014-10-01 2014-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST...

  6. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... that has an inside diameter— (a) Larger than three inches, must meet the requirements in 33 CFR 154.500... cargo pump or pump discharge relief valve setting, but not less than 100 pounds per square inch. 46 CFR... 46 Shipping 2 2010-10-01 2010-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST...

  7. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... that has an inside diameter— (a) Larger than three inches, must meet the requirements in 33 CFR 154.500... cargo pump or pump discharge relief valve setting, but not less than 100 pounds per square inch. 46 CFR... 46 Shipping 2 2011-10-01 2011-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST...

  8. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... that has an inside diameter— (a) Larger than three inches, must meet the requirements in 33 CFR 154.500... cargo pump or pump discharge relief valve setting, but not less than 100 pounds per square inch. 46 CFR... 46 Shipping 2 2012-10-01 2012-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST...

  9. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... that has an inside diameter— (a) Larger than three inches, must meet the requirements in 33 CFR 154.500... cargo pump or pump discharge relief valve setting, but not less than 100 pounds per square inch. 46 CFR... 46 Shipping 2 2013-10-01 2013-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST...

  10. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2011-10-01 2011-10-01 false Station identification. 97.119 Section...

  11. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2010-10-01 2010-10-01 false Station identification. 97.119 Section...

  12. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2013-10-01 2013-10-01 false Station identification. 97.119 Section...

  13. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2012-10-01 2012-10-01 false Station identification. 97.119 Section...

  14. 29 CFR 97.43 - Enforcement.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Enforcement. 97.43 Section 97.43 Labor Office of the Secretary of Labor UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND COOPERATIVE AGREEMENTS TO STATE AND LOCAL GOVERNMENTS Post-Award Requirements Reports, Records Retention, and Enforcement §...

  15. 40 CFR 421.97 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 28 2010-07-01 2010-07-01 true 421.97 Section 421.97 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) EFFLUENT GUIDELINES AND STANDARDS NONFERROUS METALS MANUFACTURING POINT SOURCE CATEGORY Metallurgical Acid Plants Subcategory §...

  16. 40 CFR 97.55 - Banking.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Banking. 97.55 Section 97.55 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. NOX allowances may be banked for future use or transfer in a compliance account, an...

  17. 40 CFR 97.155 - Banking.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Banking. 97.155 Section 97.155 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR NOX allowances may be banked for future use or transfer in a compliance account or...

  18. 40 CFR 97.55 - Banking.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Banking. 97.55 Section 97.55 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. NOX allowances may be banked for future use or transfer in a compliance account, an...

  19. 40 CFR 97.255 - Banking.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Banking. 97.255 Section 97.255 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR SO2 allowances may be banked for future use or transfer in a compliance account or...

  20. 40 CFR 97.155 - Banking.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Banking. 97.155 Section 97.155 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR NOX allowances may be banked for future use or transfer in a compliance account or...

  1. 40 CFR 97.255 - Banking.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Banking. 97.255 Section 97.255 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR SO2 allowances may be banked for future use or transfer in a compliance account or...

  2. 40 CFR 97.55 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.55 Section 97.55 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. NOX allowances may be banked for future use or transfer in a compliance account, an...

  3. 40 CFR 97.55 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.55 Section 97.55 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. NOX allowances may be banked for future use or transfer in a compliance account, an...

  4. 40 CFR 97.626 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.626 Section 97.626 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR SO2 Group 1 allowance may be banked for future use or transfer in a compliance...

  5. 40 CFR 97.426 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.426 Section 97.426 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Annual allowance may be banked for future use or transfer in a compliance account...

  6. 40 CFR 97.155 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.155 Section 97.155 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR NOX allowances may be banked for future use or transfer in a compliance account or...

  7. 40 CFR 97.526 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.526 Section 97.526 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Ozone Season allowance may be banked for future use or transfer in a...

  8. 40 CFR 97.426 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.426 Section 97.426 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Annual allowance may be banked for future use or transfer in a compliance account...

  9. 40 CFR 97.726 - Banking.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false Banking. 97.726 Section 97.726 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR SO2 Group 2 allowance may be banked for future use or transfer in a compliance...

  10. 40 CFR 97.626 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.626 Section 97.626 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR SO2 Group 1 allowance may be banked for future use or transfer in a compliance...

  11. 40 CFR 97.155 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.155 Section 97.155 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR NOX allowances may be banked for future use or transfer in a compliance account or...

  12. 40 CFR 97.726 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.726 Section 97.726 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR SO2 Group 2 allowance may be banked for future use or transfer in a compliance...

  13. 40 CFR 97.526 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.526 Section 97.526 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Ozone Season allowance may be banked for future use or transfer in a...

  14. 40 CFR 97.526 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.526 Section 97.526 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Ozone Season allowance may be banked for future use or transfer in a...

  15. 40 CFR 97.155 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.155 Section 97.155 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) CAIR NOX allowances may be banked for future use or transfer in a compliance account or...

  16. 40 CFR 97.426 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.426 Section 97.426 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR NOX Annual allowance may be banked for future use or transfer in a compliance account...

  17. 40 CFR 97.726 - Banking.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Banking. 97.726 Section 97.726 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. (a) A TR SO2 Group 2 allowance may be banked for future use or transfer in a compliance...

  18. 40 CFR 97.55 - Banking.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false Banking. 97.55 Section 97.55 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Banking. NOX allowances may be banked for future use or transfer in a compliance account, an...

  19. Studies of microstructural imperfections of powdered Zirconium-based alloys

    SciTech Connect

    Chowdhury, P.S.; Mukherjee, P.

    2010-11-15

    Different model based approaches of X-ray diffraction line profile analysis have been applied on the heavily deformed zirconium-based alloys in the powdered form to characterize the microstructural parameters like domain size, microstrain and dislocation density. In characterizing the microstructure of the material, these methods are complimentary to each other. Though the parameters obtained by different techniques are differently defined and thus not necessarily comparable, the values of domain size and microstrain obtained from the different techniques show similar trends.

  20. Oxidation characteristics of molybdenum-zirconium oxide cermets

    NASA Technical Reports Server (NTRS)

    Heitzinger, B.

    1984-01-01

    The oxidation of molybdenum is affected by the factors of temperature, the oxygen pressure in the oxidizing atmosphere, and the time of exposure. Studies of the oxidation characteristics of Mo show that the oxidation rate increases strongly when the temperature exceeds 600 C. Investigations of the behavior of cermets with various percentages of zirconium oxide are discussed, taking into account oxidation conditions at temperatures under and above the melting point of molybdenum trioxide.

  1. Structure and thermal behavior of zirconium tungstate under heating

    NASA Astrophysics Data System (ADS)

    Dedova, E. S.; Shutilova, E. S.; Geber, R.; Gomze, L. A.; Kulkov, S. N.

    2016-07-01

    The morphology and properties of powders ZrW2O7(OH)2·2H2O and ZrW2O8, obtained under the conditions of hydrothermal synthesis was studied. Using the high-temperature X-ray analysis, the mechanism of formation of zirconium tungstate was established. The influence of temperature on the structure and properties of materials was studied using shadow-casting method.

  2. SEPARATION OF PLUTONIUM IONS FROM SOLUTION BY ADSORPTION ON ZIRCONIUM PYROPHOSPHATE

    DOEpatents

    Stoughton, R.W.

    1961-01-31

    A method is given for separating plutonium in its reduced, phosphate- insoluble state from other substances. It involves contacting a solution containing the plutonium with granular zirconium pyrophosphate.

  3. Melting behavior of one-dimensional zirconium nanowire.

    PubMed

    Hui, Li; Wang, B L; Wang, J L; Wang, G H

    2004-02-15

    In this paper, we analyze the melting behavior of zirconium nanowire using the results of a series of molecular dynamics simulations. Our calculation employs a well-fitted, tight-binding many-body potential for zirconium atoms. The melting point of the nanowire is predicted by the root-mean-square displacements for inner and outer shells. Our simulations predict two melting behaviors: one is the inner melting and the other is the outer melting. Our results reveal that the melting of nanowire starts from the inner shell atoms. The melting point of zirconium nanowire is lower than the bulk value (2125 K). Moreover, the melting point of the inner shell is lower than that of the outer shell. A coexistence of crystal and liquid units is observed in the melting process of nanowire. An investigation of local clusters is carried out to further analyze the melting mechanism of the nanowire. The presence of the local clusters 1331, 1321, 1211, etc. is an indication of disordered structures. The pair and angular correlation functions are also presented for the analysis of the melting behavior. It is not only the diffusion of single atom but the diffusion of clusters result in the occurrence of the melting.

  4. Quantitative EELS analysis of zirconium alloy metal/oxide interfaces.

    PubMed

    Ni, Na; Lozano-Perez, Sergio; Sykes, John; Grovenor, Chris

    2011-01-01

    Zirconium alloys have been long used for fuel cladding and other structural components in water-cooled nuclear reactors, but waterside corrosion is a primary limitation on both high fuel burn-up and extended fuel cycle operation. Understanding the processes that occur at the metal/oxide interface is crucial for a full mechanistic description of the oxidation process. In this paper we show that reliable quantification of the oxygen content at the metal/oxide interface can be obtained by Electron Energy Loss Spectrometry (EELS) if enough care is taken over both the preparation of Transmission Electron Microscopy (TEM) samples and the methodology for quantification of the EELS data. We have reviewed the accuracy of theoretically calculated inelastic partial scattering cross-sections and effective inelastic mean-free-paths for oxygen and zirconium in oxidized Zr-alloy samples. After careful recalibration against a ZrO₂ powder standard, systematic differences in the local oxygen profile across the interface in different zirconium alloys were found. The presence of a sub-stoichiometric oxide layer (a suboxide) was detected under conditions of slow oxide growth but not where growth was more rapid. This difference could arise from the different corrosion resistances of the alloys or, more likely, as a result of the transition in oxidation behaviour, which refers to a sharp increase in the oxidation rate when the oxide is a few microns thick.

  5. Continuous ion exchange separation of zirconium and hafnium

    SciTech Connect

    Begovich, J.M.; Sisson, W.G.

    1981-01-01

    A pressurized continuous annular chromatograph (CAC) has been developed for truly continuous ion exchange preparative separations. This device utilizes a slowly rotating annular bed of sorbent material, fixed multiple feed points, and fixed withdrawal locations. Most of our investigations have been performed with a 28-cm-diam by 60-cm-long CAC, but a larger model has recently been designed and constructed. A detailed study has been made of the separation of copper, nickel, and cobalt components from a simulated carbonate leach liquor of the Caron process for recovering nickel and cobalt from laterite ores. Recent studies have investigated the ion exchange separation of zirconium and hafnium from a sulfate feed solution. Nuclear reactor-grade zirconium, containing < 0.01 wt % hafnium, and hafnium, containing < 1% zirconium, have been continuously prepared using cation exchange resin in the pressurized CAC. This device, because of its continuous feed and product withdrawal, its adaptability to largescale operations, and its ability to separate many components, is expected to make chromatography a more competitive process in the industrial sector.

  6. Ferrier rearrangement promoted by an electrochemically generated zirconium catalyst.

    PubMed

    Stevanović, Dragana; Pejović, Anka; Damljanović, Ivan; Minić, Aleksandra; Bogdanović, Goran A; Vukićević, Mirjana; Radulović, Niko S; Vukićević, Rastko D

    2015-04-30

    In situ generated zirconium catalyst from a sacrificial zirconium anode was successfully applied to promote Ferrier rearrangement of 3,4,5-tri-O-acetyl-D-glucal and 6-deoxy-3,4-di-O-acetyl-L-glucal (3,4-di-O-acetyl-L-rhamnal) in the presence of three thiols and eleven thiophenols as nucleophiles. A simple constant current electrolysis (20 mA, 0.4 F mol(-1)) of an acetonitrile solution of lithium perchlorate (0.1 M) containing the corresponding glycal and S-nucleophiles, using a zirconium anode and a platinum cathode resulted in the successful synthesis of the corresponding 2,3-unsaturated peracetylated thioglycosides (with an average anomer ratio α/β=4.129 in the case of peracetylated D-glucal and 8.740 in the case of L-rhamnal). The same procedure proved to be appropriate in synthesizing dihydropyran derivatives ('C-glycosides') using allyltrimethylsilane as the nucleophile (only 'α-anomers' were obtained). All new compounds were fully characterized by spectral data, whereas single-crystal X-ray analysis was performed for two thioglycosides.

  7. 14 CFR 33.97 - Thrust reversers.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Block Tests; Turbine Aircraft Engines § 33.97 Thrust reversers. (a) If the engine incorporates a reverser, the endurance calibration, operation, and vibration tests prescribed...

  8. 40 CFR 97.256 - Account error.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.256... any error in any CAIR SO2 Allowance Tracking System account. Within 10 business days of making...

  9. 40 CFR 97.256 - Account error.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.256... any error in any CAIR SO2 Allowance Tracking System account. Within 10 business days of making...

  10. 40 CFR 97.256 - Account error.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.256... any error in any CAIR SO2 Allowance Tracking System account. Within 10 business days of making...

  11. 40 CFR 97.256 - Account error.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.256... any error in any CAIR SO2 Allowance Tracking System account. Within 10 business days of making...

  12. 40 CFR 97.256 - Account error.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Tracking System § 97.256... any error in any CAIR SO2 Allowance Tracking System account. Within 10 business days of making...

  13. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... No credit. (b) The administering VEs must give credit to an examinee holding a CSCE for each...

  14. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124 Conditions. With respect to any research project or any class of research projects the department or agency...

  15. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124 Conditions. With respect to any research project or any class of research projects the department or agency...

  16. 40 CFR 97.401 - Purpose.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.401... provisions for the Transport Rule (TR) NOX Annual Trading Program, under section 110 of the Clean Air Act...

  17. 40 CFR 97.501 - Purpose.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.501... provisions for the Transport Rule (TR) NOX Ozone Season Trading Program, under section 110 of the Clean...

  18. 40 CFR 97.501 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.501... provisions for the Transport Rule (TR) NOX Ozone Season Trading Program, under section 110 of the Clean...

  19. 40 CFR 97.401 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Annual Trading Program § 97.401... provisions for the Transport Rule (TR) NOX Annual Trading Program, under section 110 of the Clean Air Act...

  20. 40 CFR 97.501 - Purpose.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS TR NOX Ozone Season Trading Program § 97.501... provisions for the Transport Rule (TR) NOX Ozone Season Trading Program, under section 110 of the Clean...