Science.gov

Sample records for zirconium 97

  1. Zirconium

    USGS Publications Warehouse

    Bedinger, G.M.

    2013-01-01

    Zirconium is the 20th most abundant element in the Earth’s crust. It occurs in a variety of rock types and geologic environments but most often in igneous rocks in the form of zircon (ZrSiO4). Zircon is recovered as a coproduct of the mining and processing of heavy mineral sands for the titanium minerals ilmenite and rutile. The sands are formed by the weathering and erosion of rock containing zircon and titanium heavy minerals and their subsequent concentration in sedimentary systems, particularly in coastal environments. A small quantity of zirconium, less than 10 kt/a (11,000 stpy), compared with total world production of 1.4 Mt (1.5 million st) in 2012, was derived from the mineral baddeleyite (ZrO2), produced from a single source in Kovdor, Russia.

  2. Colorimetric determination of zirconium in antiperspirant aerosols.

    PubMed

    Beavin, P

    1976-07-01

    A rapid direct dilution procedure for the estimation of soluble zirconium and a fusion procedure for the determination of total zirconium (soluble and insoluble forms) in cream base concentrates prepared from antiperspirant aerosols are described. The direct dilution procedure involves extraction of soluble zirconium with HCl (55 + 45). The filtered extract is reacted with alizarin red S to form a stable colored complex which is measured spectrophotometrically. The fusion procedure involves ashing the aerosol concentrate followed by fusion of the ash with potassium pyrosulfate to form an acid-soluble melt. Zirconium is precipitated from solution as the hydroxide and washed to eliminate interfering ions, particularly sulfate. After redissolving in HCl (55 + 45) and reacting with alizarin red S, total zirconium is measured. Zirconyl chloride octahydrate, assayed gravimetrically by hydroxide precipitation and conversion to the oxide, is used as the zirconium reference standard. Concentration range of zirconium measured was 200-500 mug/100 ml. Recoveries of standard zirconium added to commercial aerosols labeled to contain aluminum and zirconyl hydroxychlorides ranged from 97 to 101% by the fusion procedure. Analysis of these aerosols by direct dilution gave generally slightly lower results than by fusion. It is recommended that the procedures be collaboratively studied after further testing of their general applicability to a variety of drugs and cosmetics.

  3. PLUTONIUM-ZIRCONIUM ALLOYS

    DOEpatents

    Schonfeld, F.W.; Waber, J.T.

    1960-08-30

    A series of nuclear reactor fuel alloys consisting of from about 5 to about 50 at.% zirconium (or higher zirconium alloys such as Zircaloy), balance plutonium, and having the structural composition of a plutonium are described. Zirconium is a satisfactory diluent because it alloys readily with plutonium and has desirable nuclear properties. Additional advantages are corrosion resistance, excellent fabrication propenties, an isotropie structure, and initial softness.

  4. Studies in zirconium oxidation

    NASA Technical Reports Server (NTRS)

    Draley, J. E.; Drunen, C. J.; Levitan, J.

    1968-01-01

    Study provides insight into the oxidation mechanism of zirconium by combining electrical measurements with oxidation data. The measurement of electrical potential across growing scale on zirconium and the determination of conventional weight-change oxidation data were carried out at 550, 700, and 800 degrees C.

  5. Laser ablated zirconium plasma: A source of neutral zirconium

    SciTech Connect

    Yadav, Dheerendra; Thareja, Raj K.

    2010-10-15

    The authors report spectroscopic investigations of laser produced zirconium (Zr) plasma at moderate laser fluence. At low laser fluence the neutral zirconium species are observed to dominate over the higher species of zirconium. Laser induced fluorescence technique is used to study the velocity distribution of ground state neutral zirconium species. Two-dimensional time-resolved density distributions of ground state zirconium is mapped using planner laser induced fluorescence imaging and total ablated mass of neutral zirconium atoms is estimated. Temporal and spatial evolutions of electron density and temperature are discussed by measuring Stark broadened profile and ratio of intensity of emission lines, respectively.

  6. SEPARATING HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Lister, B.A.J.; Duncan, J.F.

    1956-08-21

    A dilute aqueous solution of zirconyl chloride which is 1N to 2N in HCl is passed through a column of a cation exchange resin in acid form thereby absorbing both zirconium and associated hafnium impurity in the mesin. The cation exchange material with the absorbate is then eluted with aqueous sulfuric acid of a O.8N to 1.2N strength. The first portion of the eluate contains the zirconium substantially free of hafnium.

  7. ZIRCONIUM-CLADDING OF THORIUM

    DOEpatents

    Beaver, R.J.

    1961-11-21

    A method of cladding thorium with zirconium is described. The quality of the bond achieved between thorium and zirconium by hot-rolling is improved by inserting and melting a thorium-zirconium alloy foil between the two materials prior to rolling. (AEC)

  8. Electroless deposition process for zirconium and zirconium alloys

    DOEpatents

    Donaghy, R. E.; Sherman, A. H.

    1981-08-18

    A method is disclosed for preventing stress corrosion cracking or metal embrittlement of a zirconium or zirconium alloy container that is to be coated on the inside surface with a layer of a metal such as copper, a copper alloy, nickel, or iron and used for holding nuclear fuel material as a nuclear fuel element. The zirconium material is etched in an etchant solution, desmutted mechanically or ultrasonically, oxidized to form an oxide coating on the zirconium, cleaned in an aqueous alkaline cleaning solution, activated for electroless deposition of a metal layer and contacted with an electroless metal plating solution. This method provides a boundary layer of zirconium oxide between the zirconium container and the metal layer. 1 fig.

  9. Electroless deposition process for zirconium and zirconium alloys

    DOEpatents

    Donaghy, Robert E.; Sherman, Anna H.

    1981-01-01

    A method is disclosed for preventing stress corrosion cracking or metal embrittlement of a zirconium or zirconium alloy container that is to be coated on the inside surface with a layer of a metal such as copper, a copper alloy, nickel, or iron and used for holding nuclear fuel material as a nuclear fuel element. The zirconium material is etched in an etchant solution, desmutted mechanically or ultrasonically, oxidized to form an oxide coating on the zirconium, cleaned in an aqueous alkaline cleaning solution, activated for electroless deposition of a metal layer and contacted with an electroless metal plating solution. This method provides a boundary layer of zirconium oxide between the zirconium container and the metal layer.

  10. Removal of impurities from zirconium tetrafluoride using metallic zirconium chips

    NASA Astrophysics Data System (ADS)

    Rusakov, I. Yu.; Buinovskii, A. S.; Sofronov, V. L.

    2016-11-01

    The sublimation refining of zirconium tetrafluoride (ZTF) from impurities in the presence of metallic zirconium chips is studied. It is shown that, in the presence of metallic zirconium chips, the contents of aluminum, nickel, oxygen, chromium, iron, and silicon impurities in a desublimate decrease and the rate of ZTF sublimation increases. The method of refining is tested under laboratory and pilot conditions and can be recommended for commercial application.

  11. Superstoichiometric hydride of zirconium

    SciTech Connect

    Kupryazhkin, A.Ya.; Shchepetkin, A.A.; Zabolotskaya, E.V.; Pletnev, R.N.; Alyamovskii, S.I.; Kitaev, G.A.

    1987-12-01

    Superstoichiometric hydrides of zirconium have been obtained all the way up to the composition ZrH/sub 2.4/ by additional hydrogenation of ZrH/sub 2/ as a result of redistribution of hydrogen atoms between t- and o-positions. In the preparation of the hydrides the authors used zirconium iodide with an impurity content no greater than 10/sup -2/ to 10/sup -2/ mole %; the hydrogen and helium used in this work had a minimum purity of 99.95%. The content of hydrogen in the specimens was determined by a volumetric method. The x-ray diffraction analysis was performed in a DRON-2.0 unit (CuK/sub ..cap alpha../ radiation). PMR spectra were recorded in a broad-line spectrometer in the temperature interval 150-450 K.

  12. Plasma arc melting of zirconium

    SciTech Connect

    Tubesing, P.K.; Korzekwa, D.R.; Dunn, P.S.

    1997-12-31

    Zirconium, like some other refractory metals, has an undesirable sensitivity to interstitials such as oxygen. Traditionally, zirconium is processed by electron beam melting to maintain minimum interstitial contamination. Electron beam melted zirconium, however, does not respond positively to mechanical processing due to its large grain size. The authors undertook a study to determine if plasma arc melting (PAM) technology could be utilized to maintain low interstitial concentrations and improve the response of zirconium to subsequent mechanical processing. The PAM process enabled them to control and maintain low interstitial levels of oxygen and carbon, produce a more favorable grain structure, and with supplementary off-gassing, improve the response to mechanical forming.

  13. Process for purifying zirconium sponge

    SciTech Connect

    Abodishish, H.A.M.; Kimball, L.S.

    1992-03-31

    This patent describes a Kroll reduction process wherein a zirconium sponge contaminated with unreacted magnesium and by-product magnesium chloride is produced as a regulus, a process for purifying the zirconium sponge. It comprises: distilling magnesium and magnesium chloride from: a regulus containing a zirconium sponge and magnesium and magnesium chloride at a temperature above about 800{degrees} C and at an absolute pressure less than about 10 mmHg in a distillation vessel to purify the zirconium sponge; condensing the magnesium and the magnesium chloride distilled from the zirconium sponge in a condenser; and then backfilling the vessel containing the zirconium sponge and the condenser containing the magnesium and the magnesium chloride with a gas; recirculating the gas between the vessel and the condenser to cool the zirconium sponge from above about 800{degrees} C to below about 300{degrees} C; and cooling the recirculating gas in the condenser containing the condensed magnesium and the condensed magnesium chloride as the gas cools the zirconium sponge to below about 300{degrees} C.

  14. ZIRCONIUM PHOSPHATE ADSORPTION METHOD

    DOEpatents

    Russell, E.R.; Adamson, A.S.; Schubert, J.; Boyd, G.E.

    1958-11-01

    A method is presented for separating plutonium values from fission product values in aqueous acidic solution. This is accomplished by flowing the solutlon containing such values through a bed of zirconium orthophosphate. Any fission products adsorbed can subsequently be eluted by washing the column with a solution of 2N HNO/sub 3/ and O.lN H/sub 3/PO/sub 4/. Plutonium values may subsequently be desorbed by contacting the column with a solution of 7N HNO/sub 3/ .

  15. SEPARATING HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Lister, B.A.J.; Duncan, J.F.; Hutcheon, J.M.

    1956-08-21

    Substantially complete separation of zirconium from hafnium may be obtained by elution of ion exchange material, on which compounds of the elements are adsorbed, with an approximately normal solution of sulfuric acid. Preferably the acid concentration is between 0.8 N amd 1.2 N, amd should not exceed 1.5 N;. Increasing the concentration of sulfate ion in the eluting solution by addition of a soluble sulfate, such as sodium sulfate, has been found to be advantageous. The preferred ion exchange materials are sulfonated polystyrene resins such as Dowex 50,'' and are preferably arranged in a column through which the solutions are passed.

  16. Modification in band gap of zirconium complexes

    NASA Astrophysics Data System (ADS)

    Sharma, Mayank; Singh, J.; Chouhan, S.; Mishra, A.; Shrivastava, B. D.

    2016-05-01

    The optical properties of zirconium complexes with amino acid based Schiff bases are reported here. The zirconium complexes show interesting stereo chemical features, which are applicable in organometallic and organic synthesis as well as in catalysis. The band gaps of both Schiff bases and zirconium complexes were obtained by UV-Visible spectroscopy. It was found that the band gap of zirconium complexes has been modified after adding zirconium compound to the Schiff bases.

  17. SEPARATION OF HAFNIUM FROM ZIRCONIUM

    DOEpatents

    Overholser, L.B.; Barton, C.J. Sr.; Ramsey, J.W.

    1960-05-31

    The separation of hafnium impurities from zirconium can be accomplished by means of organic solvent extraction. The hafnium-containing zirconium feed material is dissolved in an aqueous chloride solution and the resulting solution is contacted with an organic hexone phase, with at least one of the phases containing thiocyanate. The hafnium is extracted into the organic phase while zirconium remains in the aqueous phase. Further recovery of zirconium is effected by stripping the onganic phase with a hydrochloric acid solution and commingling the resulting strip solution with the aqueous feed solution. Hexone is recovered and recycled by means of scrubbing the onganic phase with a sulfuric acid solution to remove the hafnium, and thiocyanate is recovered and recycled by means of neutralizing the effluent streams to obtain ammonium thiocyanate.

  18. Fine-grained zirconium-base material

    DOEpatents

    Van Houten, G.R.

    1974-01-01

    A method is described for making zirconium with inhibited grain growth characteristics, by the process of vacuum melting the zirconium, adding 0.3 to 0.5% carbon, stirring, homogenizing, and cooling. (Official Gazette)

  19. Ablation Resistant Zirconium and Hafnium Ceramics

    NASA Technical Reports Server (NTRS)

    Bull, Jeffrey (Inventor); White, Michael J. (Inventor); Kaufman, Larry (Inventor)

    1998-01-01

    High temperature ablation resistant ceramic composites have been made. These ceramics are composites of zirconium diboride and zirconium carbide with silicon carbide, hafnium diboride and hafnium carbide with silicon carbide and ceramic composites which contain mixed diborides and/or carbides of zirconium and hafnium. along with silicon carbide.

  20. Zirconium and hafnium in meteorites

    NASA Technical Reports Server (NTRS)

    Ehmann, W. D.; Chyi, L. L.

    1974-01-01

    The abundances of zirconium and hafnium have been determined in nine stony meteorites by a new, precise neutron-activation technique. The Zr/Hf abundance ratios for the chondrites vary in a rather narrow range, consistent with previously published observations from our group. Replicate analyses of new, carefully selected clean interior samples of the Cl chondrite Orgueil yield mean zirconium and hafnium abundances of 5.2 and 0.10 ppm, respectively. These abundances are lower than we reported earlier for two Cl chondrite samples which we now suspect may have suffered contamination. The new Cl zirconium and hafnium abundances are in closer agreement with predictions based on theories of nucleosynthesis than the earlier data.

  1. PROCESS OF DISSOLVING ZIRCONIUM ALLOYS

    DOEpatents

    Shor, R.S.; Vogler, S.

    1958-01-21

    A process is described for dissolving binary zirconium-uranium alloys where the uranium content is about 2%. In prior dissolution procedures for these alloys, an oxidizing agent was added to prevent the precipitation of uranium tetrafluoride. In the present method complete dissolution is accomplished without the use of the oxidizing agent by using only the stoichiometric amount or slight excess of HF required by the zirconium. The concentration of the acid may range from 2M to 10M and the dissolution is advatageously carried out at a temperature of 80 deg C.

  2. Electrochemical process for zirconium alloy recycling

    SciTech Connect

    Snyder, T.S.; Stoltz, R.A.; Zuckerbrod, D.

    1990-05-08

    This patent describes a method of separating nickel from zirconium for recycling nickel-containing zirconium alloy. It comprises: placing the nickel-containing zirconium in a molten alt bath at 500{degrees} to about 722{degrees} C. with the molten salt in the molten salt bath consisting essentially of a mixture of 0 to about 46.5 mole % lithium fluoride, about 11.5 to about 40 mole % sodium fluoride and potassium fluoride to produce a molten salt bath containing dissolved zirconium and dissolved nickel; electrochemically plating the nickel from the molten salt bath at a voltage sufficient to plate nickel but less than the voltage to plate zirconium to provide an essentially nickel-free molten salt bath; and electrochemically plating the zirconium from the essentially nickel-free molten salt bath to provide an essentially nickel-free zirconium.

  3. SEPARATION PROCESS FOR ZIRCONIUM AND COMPOUNDS THEREOF

    DOEpatents

    Crandall, H.W.; Thomas, J.R.

    1959-06-30

    The separation of zirconium from columbium, rare earths, yttrium and the alkaline earth metals, such mixtures of elements occurring in zirconium ores or neutron irradiated uranium is described. According to the invention a suitable separation of zirconium from a one normal acidic aqueous solution containing salts, nitrates for example, of tetravalent zirconium, pentavalent columbium, yttrium, rare earths in the trivalent state and alkaline earths can be obtained by contacting the aqueous solution with a fluorinated beta diketonc alone or in an organic solvent solution, such as benzene, to form a zirconium chelate compound. When the organic solvent is present the zirconium chelate compound is directly extracted; otherwise it is separated by filtration. The zirconium may be recovered from contacting the organic solvent solution containing the chelated compound by back extraction with either an aqueous hydrofluoric acid or an oxalic acid solution.

  4. Environmentally Friendly Zirconium Oxide Pretreatment

    DTIC Science & Technology

    2013-05-01

    functional carboxylic acid additives 52 Figure 37 Salt Spray Corrosion Resistance of zirconium Dried- In-Place treatment made from alternate sources...GMW14872 (40 cycles) Corrosion Performance of DIP formulations with metal salts and modified organic acids versus commercial controls on aluminum... corrosion , dried-in-place, depot, environment, hexafluorozirconic acid , hexavalent chromium, paint, pretreatment, primer, steel, TT-C-490E

  5. PROCESS OF PREPARING ZIRCONIUM OXYCHLORIDE

    DOEpatents

    Wilhelm, H.A.; Andrews, M.L.

    1960-06-28

    A process is given for preparing zirconyl chloride by mixing solid zirconyl chloride octahydrate and solid zirconium tetrachloride at room temperature whereby both chlorides are converted to zirconyl chloride trinydrate and hydrogen chloride is formed and volatilized by the reaction heat.

  6. Process for producing zirconium based granules

    SciTech Connect

    Jade, S.S.

    1990-05-22

    This patent describes a process for the production f amorphous zirconium based granules. It comprises: adding about 2--15 wt % of a suitable phase stabilizer to an aqueous solutio, based upon the total weight of ZrO{sub 2} in solution, to produce an aqueous solution having a pH in the range of about 4 to 7 comprising a zirconium based complex and phase stabilizer and thereafter; drying the aqueous solution comprising the zirconium based complex and the phase stabilizer at a temperature below about 180{degrees} C. for a time sufficient to evaporate the aqueous solution thereby forming amorphous zirconium based granules containing the phase stabilizer.

  7. Method for preparing hydrous zirconium oxide gels and spherules

    DOEpatents

    Collins, Jack L.

    2003-08-05

    Methods for preparing hydrous zirconium oxide spherules, hydrous zirconium oxide gels such as gel slabs, films, capillary and electrophoresis gels, zirconium monohydrogen phosphate spherules, hydrous zirconium oxide spherules having suspendable particles homogeneously embedded within to form a composite sorbent, zirconium monohydrogen phosphate spherules having suspendable particles of at least one different sorbent homogeneously embedded within to form a composite sorbent having a desired crystallinity, zirconium oxide spherules having suspendable particles homogeneously embedded within to form a composite, hydrous zirconium oxide fiber materials, zirconium oxide fiber materials, hydrous zirconium oxide fiber materials having suspendable particles homogeneously embedded within to form a composite, zirconium oxide fiber materials having suspendable particles homogeneously embedded within to form a composite and spherules of barium zirconate. The hydrous zirconium oxide spherules and gel forms prepared by the gel-sphere, internal gelation process are useful as inorganic ion exchangers, catalysts, getters and ceramics.

  8. DISSOLUTION OF ZIRCONIUM-CONTAINING FUEL ELEMENTS

    DOEpatents

    Horn, F.L.

    1961-12-12

    Uranium is recovered from spent uranium fuel elements containing or clad with zirconium. These fuel elements are placed in an anhydrous solution of hydrogen fluoride and nitrogen dioxide. Within this system uranium forms a soluble complex and zirconium forms an insoluble complex. The uranium can then be separated, treated, and removed from solution as uranium hexafluoride. (AEC)

  9. Method of making crack-free zirconium hydride

    DOEpatents

    Sullivan, Richard W.

    1980-01-01

    Crack-free hydrides of zirconium and zirconium-uranium alloys are produced by alloying the zirconium or zirconium-uranium alloy with beryllium, or nickel, or beryllium and scandium, or nickel and scandium, or beryllium and nickel, or beryllium, nickel and scandium and thereafter hydriding.

  10. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  11. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  12. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  13. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  14. 47 CFR 97.515-97.517 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false 97.515-97.517 Section 97.515-97.517 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems §§ 97.515-97.517...

  15. 34 CFR 97.104-97.106 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false 97.104-97.106 Section 97.104-97.106 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) §§ 97.104-97.106...

  16. 34 CFR 97.104-97.106 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false 97.104-97.106 Section 97.104-97.106 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) §§ 97.104-97.106...

  17. 34 CFR 97.104-97.106 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false 97.104-97.106 Section 97.104-97.106 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) §§ 97.104-97.106...

  18. 34 CFR 97.104-97.106 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false 97.104-97.106 Section 97.104-97.106 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) §§ 97.104-97.106...

  19. 34 CFR 97.104-97.106 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false 97.104-97.106 Section 97.104-97.106 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) §§ 97.104-97.106...

  20. Activated sintering of zirconium dioxide

    NASA Astrophysics Data System (ADS)

    Panin, V. E.; Slosman, A. I.; Matrenin, S. V.

    1996-02-01

    A new phenomenon has been observed — the activated sintering of a zirconium ceramic in the hydrogen-nitrogen plasma of a glow discharge. It is shown that the activation energy is considerably lower than the activation energy for sintering in a vacuum furnace. This makes it possible to reduce sintering temperature, refine the grains, and improve the mechanical properties of the ceramic. It is proposed that the mechanism by which sintering is activated is connected with the activating effect of hydrogen during a structural transformation involving the formation of oxynitride phases.

  1. Method of etching zirconium diboride

    SciTech Connect

    Heath, L.S.; Kwiatkowski, B.

    1988-03-31

    The invention described herein may be manufactured, used, and licensed by or for the Government for governmental purposes without the payment to us of any royalty thereon. This invention relates in general to a method of etching, zirconium diboride(ZrB/sub 2/) and, in particular, to a method of dry etching a thin film of ZrB/sub 2/ that has been deposited onto a substrate and patterned using photolithography. U.S. patent application S.N. 156, 124, filed 16 February, 1988, of Linda S. Heath for Method of Etching Titanium Diboride and assigned to a common assignee and with which this application is copending describes and claims a method of etching titanium diboride with a dry etch. Zirconium diboride, like titanium diboride, TiB/sub 2/, has become of interest in laboratory research because of its resistance to change or degradation at high temperatures. By adjusting the process parameters, one is able to attain etch rates of 67 to 140 A/min for ZrB/sub 2/. This is useful for patterning ZrB/sub 2/ as a diffusion barrier or a Schottky contact to semiconductors. The ZrB/sub 2/ film may be on a GaAs substrate.

  2. URANIUM DECONTAMINATION WITH RESPECT TO ZIRCONIUM

    DOEpatents

    Vogler, S.; Beederman, M.

    1961-05-01

    A process is given for separating uranium values from a nitric acid aqueous solution containing uranyl values, zirconium values and tetravalent plutonium values. The process comprises contacting said solution with a substantially water-immiscible liquid organic solvent containing alkyl phosphate, separating an organic extract phase containing the uranium, zirconium, and tetravalent plutonium values from an aqueous raffinate, contacting said organic extract phase with an aqueous solution 2M to 7M in nitric acid and also containing an oxalate ion-containing substance, and separating a uranium- containing organic raffinate from aqueous zirconium- and plutonium-containing extract phase.

  3. Production of nuclear grade zirconium: A review

    NASA Astrophysics Data System (ADS)

    Xu, L.; Xiao, Y.; van Sandwijk, A.; Xu, Q.; Yang, Y.

    2015-11-01

    Zirconium is an ideal material for nuclear reactors due to its low absorption cross-section for thermal neutrons, whereas the typically contained hafnium with strong neutron-absorption is very harmful for zirconium as a fuel cladding material. This paper provides an overview of the processes for nuclear grade zirconium production with emphasis on the methods of Zr-Hf separation. The separation processes are roughly classified into hydro- and pyrometallurgical routes. The known pyrometallurgical Zr-Hf separation methods are discussed based on the following reaction features: redox characteristics, volatility, electrochemical properties and molten salt-metal equilibrium. In the present paper, the available Zr-Hf separation technologies are compared. The advantages and disadvantages as well as future directions of research and development for nuclear grade zirconium production are discussed.

  4. Modelling of zirconium alloy hydrogenation

    NASA Astrophysics Data System (ADS)

    Zaika, Yury V.; Rodchenkova, Natalia I.

    2016-11-01

    Zirconium alloys are the construction materials for critical elements in active zones of nuclear power reactors. During the operation of reactors such materials are subject to hydrogenation. Hydrogenation results in a decrease of alloy plasticity and cracking resistance. The formation of brittle hydrides at crack tips can result in severe embrittlement. One of the most important requirements for the reactor's active zone materials is low hydrogen absorptivity. The mathematical model of hydride layer formation and growth is developed. The problem is to determine the dynamics of the free boundary of phase interface and the distributions of hydrogen concentration in hydride and in solution. Iterative computational algorithm for solving the nonlinear boundary-value problem with the Stefan condition based on implicit difference schemes is developed.

  5. METHOD OF IMPROVING CORROSION RESISTANCE OF ZIRCONIUM

    DOEpatents

    Shannon, D.W.

    1961-03-28

    An improved intermediate rinse for zirconium counteracts an anomalous deposit that often results in crevices and outof-the-way places when ordinary water is used to rinse away a strong fluoride etching solution designed to promote passivation of the metal. The intermediate rinse, which is used after the etching solution and before the water, is characterized by a complexing agent for fluoride ions such as aluminum or zirconium nitrates or chlorides.

  6. DISSOLUTION OF ZIRCONIUM AND ALLOYS THEREFOR

    DOEpatents

    Swanson, J.L.

    1961-07-11

    The dissolution of zirconium cladding in a water solution of ammonium fluoride and ammonium nitrate is described. The method finds particular utility in processing spent fuel elements for nuclear reactors. The zirconium cladding is first dissolved in a water solution of ammonium fluoride and ammonium nitrate; insoluble uranium and plutonium fiuorides formed by attack of the solvent on the fuel materiai of the fuel element are then separated from the solution, and the fuel materiai is dissolved in another solution.

  7. Stark broadening effect and zirconium conflict problem

    NASA Astrophysics Data System (ADS)

    Dimitrijević, Milan S.; Popović, Luka Č.; Milovanović, Nenad

    2001-04-01

    Using the Modified Semiempirical Method we have calculated the electron-impact widths for four singly and doubly ionized zirconium UV lines of astrophysical importance. Using the SYNTH and ATLAS9 codes for stellar atmospheres similar to that of the HgMn star χ Lupi we have synthesized the line profiles and found equivalent widths for these lines. The influence of the Stark broadening effect on abundance determination and its contribution to the so-called ``zirconium conflict'' are discussed. .

  8. Zirconium Oxide Nanostructures Prepared by Anodic Oxidation

    SciTech Connect

    Dang, Ying Yi; Bhuiyan, Md S; Paranthaman, Mariappan Parans

    2008-01-01

    Zirconium oxide is an advanced ceramic material highly useful for structural and electrical applications because of its high strength, fracture toughness, chemical and thermal stability, and biocompatibility. If highly-ordered porous zirconium oxide membranes can be successfully formed, this will expand its real-world applications, such as further enhancing solid-oxide fuel cell technology. Recent studies have achieved various morphologies of porous zirconium oxide via anodization, but they have yet to create a porous layer where nanoholes are formed in a highly ordered array. In this study, electrochemical methods were used for zirconium oxide synthesis due to its advantages over other coating techniques, and because the thickness and morphology of the ceramic films can be easily tuned by the electrochemical parameters, such as electrolyte solutions and processing conditions, such as pH, voltage, and duration. The effects of additional steps such as pre-annealing and post-annealing were also examined. Results demonstrate the formation of anodic porous zirconium oxide with diverse morphologies, such as sponge-like layers, porous arrays with nanoholes ranging from 40 to 75 nm, and nanotube layers. X-ray powder diffraction analysis indicates a cubic crystallographic structure in the zirconium oxide. It was noted that increased voltage improved the ability of the membrane to stay adhered to the zirconium substrate, whereas lower voltages caused a propensity for the oxide film to flake off. Further studies are needed to define the parameters windows that create these morphologies and to investigate other important characteristics such as ionic conductivity.

  9. ZIRCONIUM OXIDE NANOSTRUCTURES PREPARED BY ANODIC OXIDATION

    SciTech Connect

    Dang, Y. Y.; Bhuiyan, M.S.; Paranthaman, M. P.

    2008-01-01

    Zirconium oxide is an advanced ceramic material highly useful for structural and electrical applications because of its high strength, fracture toughness, chemical and thermal stability, and biocompatibility. If highly-ordered porous zirconium oxide membranes can be successfully formed, this will expand its real-world applications, such as further enhancing solid-oxide fuel cell technology. Recent studies have achieved various morphologies of porous zirconium oxide via anodization, but they have yet to create a porous layer where nanoholes are formed in a highly ordered array. In this study, electrochemical methods were used for zirconium oxide synthesis due to its advantages over other coating techniques, and because the thickness and morphology of the ceramic fi lms can be easily tuned by the electrochemical parameters, such as electrolyte solutions and processing conditions, such as pH, voltage, and duration. The effects of additional steps such as pre-annealing and post-annealing were also examined. Results demonstrate the formation of anodic porous zirconium oxide with diverse morphologies, such as sponge-like layers, porous arrays with nanoholes ranging from 40 to 75 nm, and nanotube layers. X-ray powder diffraction analysis indicates a cubic crystallographic structure in the zirconium oxide. It was noted that increased voltage improved the ability of the membrane to stay adhered to the zirconium substrate, whereas lower voltages caused a propensity for the oxide fi lm to fl ake off. Further studies are needed to defi ne the parameters windows that create these morphologies and to investigate other important characteristics such as ionic conductivity.

  10. Synthesis of zirconium oxide nanoparticle by sol-gel technique

    SciTech Connect

    Lim, H. S.; Ahmad, A.; Hamzah, H.

    2013-11-27

    Zirconium oxide nanoparticle is synthesized using sol-gel technique. Various mole ratio of ammonia solution and nitric acid relative to zirconium propoxide is added in the reaction to study the effect on the crystallinity and particle size on zirconium oxide particle. Zirconium oxide synthesized with nitric acid have the smallest particle size under FESEM image and show the increasing formation of crystalline tetragonal phase under XRD diffractogram.

  11. Zirconium: biomedical and nephrological applications.

    PubMed

    Lee, David B N; Roberts, Martin; Bluchel, Christian G; Odell, Ross A

    2010-01-01

    Recent years have witnessed a rapid increase in the use of zirconium (Zr)-containing compounds in artificial internal organs. Examples include dental implants and other restorative practices, total knee and hip replacement, and middle-ear ossicular chain reconstruction. In nephrological practice, Zr-containing sorbents have been used in hemofiltration, hemodialysis, peritoneal dialysis, and in the design and construction of wearable artificial kidneys. Zr compounds continue to be widely and extensively used in deodorant and antiperspirant preparations. In the public health arena, Zr compounds have been studied or used in controlling phosphorus pollution and in the reclamation of poison and bacteria-contaminated water. Experimental and clinical studies support the general consensus that Zr compounds are biocompatible and exhibit low toxicity. Reports on possible Zr-associated adverse reactions are rare and, in general, have not rigorously established a cause-and-effect relationship. Although publications on the use of Zr compounds have continued to increase in recent years, reports on Zr toxicity have virtually disappeared from the medical literature. Nevertheless, familiarity with, and continued vigilant monitoring of, the use of these compounds are warranted. This article provides an updated review on the biomedical use of Zr compounds.

  12. Processing fissile material mixtures containing zirconium and/or carbon

    DOEpatents

    Johnson, Michael Ernest; Maloney, Martin David

    2013-07-02

    A method of processing spent TRIZO-coated nuclear fuel may include adding fluoride to complex zirconium present in a dissolved TRIZO-coated fuel. Complexing the zirconium with fluoride may reduce or eliminate the potential for zirconium to interfere with the extraction of uranium and/or transuranics from fission materials in the spent nuclear fuel.

  13. 40 CFR 721.10708 - Zirconium substituted heteropolycyclic (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium substituted heteropolycyclic... Specific Chemical Substances § 721.10708 Zirconium substituted heteropolycyclic (generic). (a) Chemical... as zirconium substituted heteropolycyclic (PMN P-13-152) is subject to reporting under this...

  14. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 31 2011-07-01 2011-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  15. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  16. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  17. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  18. 40 CFR 721.10601 - Lanthanum lead titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lanthanum lead titanium zirconium... Specific Chemical Substances § 721.10601 Lanthanum lead titanium zirconium oxide. (a) Chemical substance... titanium zirconium oxide (PMN P-11-273; CAS No. 1227908-26-0) is subject to reporting under this...

  19. 40 CFR 721.10601 - Lanthanum lead titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lanthanum lead titanium zirconium... Specific Chemical Substances § 721.10601 Lanthanum lead titanium zirconium oxide. (a) Chemical substance... titanium zirconium oxide (PMN P-11-273; CAS No. 1227908-26-0) is subject to reporting under this...

  20. 40 CFR 721.9973 - Zirconium dichlorides (generic).

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Zirconium dichlorides (generic). 721... Substances § 721.9973 Zirconium dichlorides (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substances identified generically as zirconium dichlorides (PMNs...

  1. Zirconium granuloma resulting from an aluminum zirconium complex: a previously unrecognized agent in the development of hypersensitivity granulomas.

    PubMed

    Skelton, H G; Smith, K J; Johnson, F B; Cooper, C R; Tyler, W F; Lupton, G P

    1993-05-01

    Zirconium compounds have been associated with the development of hypersensitivity granulomas. However, aluminum zirconium complexes have not previously been shown to induce sensitization. We present the clinical and histologic findings of a case in which a patient developed an acute hypersensitivity reaction to an aluminum zirconium complex.

  2. Radiation effects on corrosion of zirconium alloys

    SciTech Connect

    Johnson, A.B. Jr.

    1989-06-01

    From the wide use of zirconium alloys as components in nuclear reactors, has come clear evidence that reactor radiation is a major corrosion parameter. The evidence emerges from comparisons of zirconium alloy corrosion behavior in different reactor types, for example, BWRs versus PWRs and in corresponding reactor loop chemistries; also, oxidation rates differ with location along components such as fuel rods and reactor pressure tubes. In most respects, oxidation effects on power reactor components are paralleled by oxidation behavior on specimens exposed to radiation in reactor loops.

  3. Steady State Creep of Zirconium at High and Intermediate Temperatures

    SciTech Connect

    Rosen, R.S.; Hayes, T.A.

    2000-04-08

    Creep of zirconium and zirconium alloys has been labeled ''anomalous.'' Researchers often report that zirconium and its alloys never reach true steady state creep and have stress exponents that continuously change with stress and temperature. Many varied interpretations have been offered explaining the creep behavior of zirconium. Some have suggested that creep is diffusion controlled, while others maintain that creep is dislocation glide controlled. Cumulative zirconium creep data will be presented based on an extensive literature review. An interpretation of results will be presented and compared to previous interpretations.

  4. Intercalation chemistry of zirconium 4-sulfophenylphosphonate

    SciTech Connect

    Svoboda, Jan; Zima, Vítězslav; Melánová, Klára; Beneš, Ludvík; Trchová, Miroslava

    2013-12-15

    Zirconium 4-sulfophenylphosphonate is a layered material which can be employed as a host for the intercalation reactions with basic molecules. A wide range of organic compounds were chosen to represent intercalation ability of zirconium 4-sulfophenylphosphonate. These were a series of alkylamines from methylamine to dodecylamine, 1,4-phenylenediamine, p-toluidine, 1,8-diaminonaphthalene, 1-aminopyrene, imidazole, pyridine, 4,4′-bipyridine, poly(ethylene imine), and a series of amino acids from glycine to 6-aminocaproic acid. The prepared compounds were characterized by powder X-ray diffraction, thermogravimetry analysis and IR spectroscopy and probable arrangement of the guest molecules in the interlayer space of the host is proposed based on the interlayer distance of the prepared intercalates and amount of the intercalated guest molecules. - Graphical abstract: Nitrogen-containing organic compounds can be intercalated into the interlayer space of zirconium 4-sulfophenylphosphonate. - Highlights: • Zirconium 4-sulfophenylphosphonate was examined as a host material in intercalation chemistry. • A wide range of nitrogen-containing organic compounds were intercalated. • Possible arrangement of the intercalated species is described.

  5. Ice-structuring mechanism for zirconium acetate.

    PubMed

    Deville, Sylvain; Viazzi, Céline; Guizard, Christian

    2012-10-23

    The control of ice nucleation and growth is critical in many natural and engineering situations. However, very few compounds are able to interact directly with the surface of ice crystals. Ice-structuring proteins, found in certain fish, plants, and insects, bind to the surface of ice, thereby controlling their growth. We recently revealed the ice-structuring properties of zirconium acetate, which are similar to those of ice-structuring proteins. Because zirconium acetate is a salt and therefore different from proteins having ice-structuring properties, its ice-structuring mechanism remains unelucidated. Here we investigate this ice-structuring mechanism through the role of the concentration of zirconium acetate and the ice crystal growth velocity. We then explore other compounds presenting similar functional groups (acetate, hydroxyl, or carboxylic groups). On the basis of these results, we propose that zirconium acetate adopts a hydroxy-bridged polymer structure that can bind to the surface of the ice crystals through hydrogen bonding, thereby slowing down the ice crystal growth.

  6. Superconductivity in zirconium-rhodium alloys

    NASA Technical Reports Server (NTRS)

    Zegler, S. T.

    1969-01-01

    Metallographic studies and transition temperature measurements were made with isothermally annealed and water-quenched zirconium-rhodium alloys. The results clarify both the solid-state phase relations at the Zr-rich end of the Zr-Rh alloy system and the influence upon the superconducting transition temperature of structure and composition.

  7. Zirconium modified nickel-copper alloy

    NASA Technical Reports Server (NTRS)

    Whittenberger, J. D. (Inventor)

    1977-01-01

    An improved material for use in a catalytic reactor which reduces nitrogen oxide from internal combustion engines is in the form of a zirconium-modified, precipitation-strengthened nickel-copper alloy. This material has a nominal composition of Ni-30 Cu-0.2 Zr and is characterized by improved high temperature mechanical properties.

  8. METHOD AND ALLOY FOR BONDING TO ZIRCONIUM

    DOEpatents

    McCuaig, F.D.; Misch, R.D.

    1960-04-19

    A brazing alloy can be used for bonding zirconium and its alloys to other metals, ceramics, and cermets, and consists of 6 to 9 wt.% Ni, 6 to 9 wn~.% Cr, Mo, or W, 0 to 7.5 wt.% Fe, and the balance Zr.

  9. Therapeutic antibody technology 97.

    PubMed

    Larrick, J W; Gavilondo, J

    1998-01-01

    Almost 200 antibody aficionados attended the Therapeutic Antibody Technology 97 meeting, held September 21-24, 1997 at the Holiday Inn, Union Square in the heart of San Francisco, CA. The meeting was sponsored by the Palo Alto Institute of Molecular Medicine and organized by James W. Larrick (PAIMM) and Dennis R. Burton (Scripps Research Institute). The meeting featured excellent discussions on many interesting talks and a number of poster presentations. It is likely that another meeting will be organized in 2 years, however in the meantime, an effort is underway to organize a 'Virtual Antibody Society' to be set up on the web server at Scripps Research Institute in La Jolla, CA (Questions and comments on this project can be sent to: Jwlarrick@aol.com or Burton@scripps.edu). Richard Lerner (Scripps) gave the keynote address on 'Catalytic Antibodies', describing recent work with Carlos Barbas on so-called reactive immunization to generate a high activity aldolase catalytic antibody. This antibody, soon to be described in an article in Science, is the first commercially available catalytic antibody.

  10. International strategic minerals inventory summary report; zirconium

    USGS Publications Warehouse

    Towner, R.R.

    1992-01-01

    Zircon, a zirconium silicate, is currently the most important commercial zirconium-bearing mineral. Baddeleyite, a natural form of zirconia, is less important but has some specific end uses. Both zircon and baddeleyite occur in hard-rock and placer deposits, but at present all zircon production is from placer deposits. Most baddeleyite production is from hard-rock deposits, principally as a byproduct of copper and phosphate-rock mining. World zirconium resources in identified, economically exploitable deposits are about 46 times current production rates. Of these resources, some 71 percent are in South Africa, Australia, and the United States. The principal end uses of zirconium minerals are in ceramic applications and as refractories, abrasives, and mold linings in foundries. A minor amount, mainly of zircon, is used for the production of hafnium-free zirconium metal, which is used principally for sheathing fuel elements in nuclear reactors and in the chemical-processing industry, aerospace engineering, and electronics. Australia and South Africa are the largest zircon producers and account for more than 70 percent of world output; the United States and the Soviet Union account for another 20 percent. South Africa accounts for almost all the world's production of baddeleyite, which is about 2 percent of world production of contained zirconia. Australia and South Africa are the largest exporters of zircon. Unless major new deposits are developed in countries that have not traditionally produced zircon, the pattern of world production is unlikely to change by 2020. The proportions, however, of production that come from existing producing countries may change somewhat.

  11. METHOD OF MAKING DELTA ZIRCONIUM HYDRIDE MONOLITHIC MODERATOR PIECES

    DOEpatents

    Vetrano, J.B.

    1962-01-23

    A method is given for preparing large, sound bodies of delta zirconium hydride. The method includes the steps of heating a zirconium body to a temperature of not less than l000 deg C, providing a hydrogen atmosphere for the zirconium body at a pressure not greater than one atmosphere, reducing the temperature slowly to 800 deg C at such a rate that cracks do not form while maintaining the hydrogen pressure substantially constant, and cooling in an atmosphere of hydrogen. (AEC)

  12. Effects of titanium and zirconium on iron aluminide weldments

    SciTech Connect

    Mulac, B.L.; Edwards, G.R.; Burt, R.P.; David, S.A.

    1997-12-01

    When gas-tungsten arc welded, iron aluminides form a coarse fusion zone microstructure which is susceptible to hydrogen embrittlement. Titanium inoculation effectively refined the fusion zone microstructure in iron aluminide weldments, but the inoculated weldments had a reduced fracture strength despite the presence of a finer microstructure. The weldments fractured by transgranular cleavage which nucleated at cracked second phase particles. With titanium inoculation, second phase particles in the fusion zone changed shape and also became more concentrated at the grain boundaries, which increased the particle spacing in the fusion zone. The observed decrease in fracture strength with titanium inoculation was attributed to increased spacing of second phase particles in the fusion zone. Current research has focused on the weldability of zirconium- and carbon-alloyed iron aluminides. Preliminary work performed at Oak Ridge National Laboratory has shown that zirconium and carbon additions affect the weldability of the alloy as well as the mechanical properties and fracture behavior of the weldments. A sigmajig hot cracking test apparatus has been constructed and tested at Colorado School of Mines. Preliminary characterization of hot cracking of three zirconium- and carbon-alloyed iron aluminides, each containing a different total concentration of zirconium at a constant zirconium/carbon ratio of ten, is in progress. Future testing will include low zirconium alloys at zirconium/carbon ratios of five and one, as well as high zirconium alloys (1.5 to 2.0 atomic percent) at zirconium/carbon ratios of ten to forty.

  13. Investigation of anodic oxide coatings on zirconium after heat treatment

    NASA Astrophysics Data System (ADS)

    Sowa, Maciej; Dercz, Grzegorz; Suchanek, Katarzyna; Simka, Wojciech

    2015-08-01

    Herein, results of heat treatment of zirconium anodised under plasma electrolytic oxidation (PEO) conditions at 500-800 °C are presented. The obtained oxide films were investigated by means of SEM, XRD and Raman spectroscopy. The corrosion resistance of the zirconium specimens was evaluated in Ringer's solution. A bilayer oxide coatings generated in the course of PEO of zirconium were not observed after the heat treatment. The resulting oxide layers contained a new sublayer located at the metal/oxide interface is suggested to originate from the thermal oxidation of zirconium. The corrosion resistance of the anodised metal was improved after the heat treatment.

  14. Manufacturing process to reduce large grain growth in zirconium alloys

    DOEpatents

    Rosecrans, P.M.

    1984-08-01

    It is an object of the present invention to provide a procedure for desensitizing zirconium-based alloys to large grain growth (LGG) during thermal treatment above the recrystallization temperature of the alloy. It is a further object of the present invention to provide a method for treating zirconium-based alloys which have been cold-worked in the range of 2 to 8% strain to reduce large grain growth. It is another object of the present invention to provide a method for fabricating a zirconium alloy clad nuclear fuel element wherein the zirconium clad is resistant to large grain growth.

  15. Corrosion Studies on Titanium and Zirconium Metals

    DTIC Science & Technology

    1951-12-01

    beryllium, and tin; in furfuryl alcohol with yh alloys containing chromium, beryllium, nickel, silicon, tungsten, copper , silver, molybdenum, antimony...furfryl alcohol with 35 alloys containing nickel, silicon, tungsten, copper , and tin; and in methyl a ethyl alcohol with 5 alloys containing tin...zirconium in synthetic ocean water indicates that these metals are electropositive (noble) with respect to certain comon metals. Copper , aluminum, tin

  16. ELECTROLYTIC CLADDING OF ZIRCONIUM ON URANIUM

    DOEpatents

    Wick, J.J.

    1959-09-22

    A method is presented for coating uranium with zircoalum by rendering the uranium surface smooth and oxidefree, immersing it in a molten electrolytic bath in NaCI, K/sub 2/ZrF/sub 6/, KF, and ZrO/sub 2/, and before the article reaches temperature equilibrium with the bath, applying an electrolyzing current of 60 amperes per square dectmeter at approximately 3 volts to form a layer of zirconium metal on the uranium.

  17. From Zirconium Nanograins to Zirconia Nanoneedles

    PubMed Central

    Zalnezhad, E.; Hamouda, A. M. S.; Jaworski, J.; Do Kim, Young

    2016-01-01

    Combinations of three simple techniques were utilized to gradually form zirconia nanoneedles from zirconium nanograins. First, a physical vapor deposition magnetron sputtering technique was used to deposit pure zirconium nanograins on top of a substrate. Second, an anodic oxidation was applied to fabricate zirconia nanotubular arrays. Finally, heat treatment was used at different annealing temperatures in order to change the structure and morphology from nanotubes to nanowires and subsequently to nanoneedles in the presence of argon gas. The size of the pure zirconium nanograins was estimated to be approximately 200–300 nm. ZrO2 nanotubular arrays with diameters of 70–120 nm were obtained. Both tetragonal and monoclinic ZrO2 were observed after annealing at 450 °C and 650 °C. Only a few tetragonal peaks appeared at 850 °C, while monoclinic ZrO2 was obtained at 900 °C and 950 °C. In assessing the biocompatibility of the ZrO2 surface, the human cell line MDA-MB-231 was found to attach and proliferate well on surfaces annealed at 850 °C and 450 °C; however, the amorphous ZrO2 surface, which was not heat treated, did not permit extensive cell growth, presumably due to remaining fluoride. PMID:27623486

  18. High temperature behavior of zirconium germanates

    SciTech Connect

    Utkin, A.V.; Baklanova, N.I.; Vasilyeva, I.G.

    2013-05-01

    The high temperature behavior of zirconium germanates ZrGeO₄ and Zr₃GeO₈ up to 2300 °C has been studied using the original photoemission thermal analysis technique with the comprehensive physicochemical study of solid and gaseous intermediate and final products. The two-stage process of incongruent sublimation of GeO₂ was established and the phase boundary of the homogeneity range for ZrGeO₄ and Zr₃GeO₈ were deduced from the thermal analysis, X-ray diffraction and Raman spectroscopy studies. A high tendency to sintering of the final ZrO₂ product is discussed. - Graphical abstract: The decomposition of zirconium germanates leads to the formation of gaseous GeO₂ and solid sintered ZrO₂ and occurs via two stages with the formation of intermediate ZrO₂-rich solid solution. Highlights: •Thermal behavior of ZrGeO₄ and Zr₃GeO₈ was studied using the original thermal analysis technique in wide temperature range. •The decomposition occurs via two stages with the formation of intermediate ZrO₂-rich solid solution. •The decomposition of zirconium germanates leads to the formation of gaseous GeO₂ and solid sintered ZrO₂. •The temperature of decomposition is strongly depended on the total gas pressure.

  19. Fluorometric determination of zirconium in minerals

    USGS Publications Warehouse

    Alford, W.C.; Shapiro, L.; White, C.E.

    1951-01-01

    The increasing use of zirconium in alloys and in the ceramics industry has created renewed interest in methods for its determination. It is a common constituent of many minerals, but is usually present in very small amounts. Published methods tend to be tedious, time-consuming, and uncertain as to accuracy. A new fluorometric procedure, which overcomes these objections to a large extent, is based on the blue fluorescence given by zirconium and flavonol in sulfuric acid solution. Hafnium is the only element that interferes. The sample is fused with borax glass and sodium carbonate and extracted with water. The residue is dissolved in sulfuric acid, made alkaline with sodium hydroxide to separate aluminum, and filtered. The precipitate is dissolved in sulfuric acid and electrolysed in a Melaven cell to remove iron. Flavonol is then added and the fluorescence intensity is measured with a photo-fluorometer. Analysis of seven standard mineral samples shows excellent results. The method is especially useful for minerals containing less than 0.25% zirconium oxide.

  20. Production optimization of 99Mo/99mTc zirconium molybate gel generators at semi-automatic device: DISIGEG.

    PubMed

    Monroy-Guzman, F; Rivero Gutiérrez, T; López Malpica, I Z; Hernández Cortes, S; Rojas Nava, P; Vazquez Maldonado, J C; Vazquez, A

    2012-01-01

    DISIGEG is a synthesis installation of zirconium (99)Mo-molybdate gels for (99)Mo/(99m)Tc generator production, which has been designed, built and installed at the ININ. The device consists of a synthesis reactor and five systems controlled via keyboard: (1) raw material access, (2) chemical air stirring, (3) gel dried by air and infrared heating, (4) moisture removal and (5) gel extraction. DISIGEG operation is described and dried condition effects of zirconium (99)Mo- molybdate gels on (99)Mo/(99m)Tc generator performance were evaluated as well as some physical-chemical properties of these gels. The results reveal that temperature, time and air flow applied during the drying process directly affects zirconium (99)Mo-molybdate gel generator performance. All gels prepared have a similar chemical structure probably constituted by three-dimensional network, based on zirconium pentagonal bipyramids and molybdenum octahedral. Basic structural variations cause a change in gel porosity and permeability, favouring or inhibiting (99m)TcO(4)(-) diffusion into the matrix. The (99m)TcO(4)(-) eluates produced by (99)Mo/(99m)Tc zirconium (99)Mo-molybdate gel generators prepared in DISIGEG, air dried at 80°C for 5h and using an air flow of 90mm, satisfied all the Pharmacopoeias regulations: (99m)Tc yield between 70-75%, (99)Mo breakthrough less than 3×10(-3)%, radiochemical purities about 97% sterile and pyrogen-free eluates with a pH of 6.

  1. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  2. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  3. 40 CFR 721.10250 - Zirconium lysine complex (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Zirconium lysine complex (generic... Specific Chemical Substances § 721.10250 Zirconium lysine complex (generic). (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified generically as...

  4. 40 CFR 721.10598 - Lead strontium titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Lead strontium titanium zirconium... Specific Chemical Substances § 721.10598 Lead strontium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead...

  5. 40 CFR 721.10598 - Lead strontium titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Lead strontium titanium zirconium... Specific Chemical Substances § 721.10598 Lead strontium titanium zirconium oxide. (a) Chemical substance and significant new uses subject to reporting. (1) The chemical substance identified as lead...

  6. [The clinical application of zirconium-dioxide-ceramics. Case report].

    PubMed

    Somfai, Dóra; Zsigmond, Ágnes; Károlyházy, Katalin; Kispély, Barbara; Hermann, Péter

    2015-12-01

    Due to its outstanding physical, mechanical and esthetic properties, zirconium-dioxide is one of the most popular non-metal denture, capable of surpassing PFM in most cases. The recent advances of CAD/CAM technology makes it a good alternitve. Here we show the usefulness of zirconium-dioxide in everyday dental practice through three case reports.

  7. NEUTRON REACTOR FUEL ELEMENT UTILIZING ZIRCONIUM-BASE ALLOYS

    DOEpatents

    Saller, H.A.; Keeler, J.R.; Szumachowski, E.R.

    1957-11-12

    This patent relates to clad fuel elements for use in neutronic reactors and is drawn to such a fuel element which consists of a core of fissionable material, comprised of an alloy of zirconium and U/sup 235/ enriched uranium, encased in a jacket of a binary zirconium-tin alloy in which the tin content ranges between 1 and 15% by weight.

  8. PROCESS FOR DISSOLVING BINARY URANIUM-ZIRCONIUM OR ZIRCONIUM-BASE ALLOYS

    DOEpatents

    Jonke, A.A.; Barghusen, J.J.; Levitz, N.M.

    1962-08-14

    A process of dissolving uranium-- zirconium and zircaloy alloys, e.g. jackets of fuel elements, with an anhydrous hydrogen fluoride containing from 10 to 32% by weight of hydrogen chloride at between 400 and 450 deg C., preferably while in contact with a fluidized inert powder, such as calcium fluoride is described. (AEC)

  9. Zirconium fluoride glass - Surface crystals formed by reaction with water

    NASA Technical Reports Server (NTRS)

    Doremus, R. H.; Bansal, N. P.; Bradner, T.; Murphy, D.

    1984-01-01

    The hydrated surfaces of a zirconium barium fluoride glass, which has potential for application in optical fibers and other optical elements, were observed by scanning electron microscopy. Crystalline zirconium fluoride was identified by analysis of X-ray diffraction patterns of the surface crystals and found to be the main constituent of the surface material. It was also found that hydrated zirconium fluorides form only in highly acidic fluoride solutions. It is possible that the zirconium fluoride crystals form directly on the glass surface as a result of its depletion of other ions. The solubility of zirconium fluoride is suggested to be probably much lower than that of barium fluoride (0.16 g/100 cu cm at 18 C). Dissolution was determined to be the predominant process in the initial stages of the reaction of the glass with water. Penetration of water into the glass has little effect.

  10. 21 CFR 700.16 - Use of aerosol cosmetic products containing zirconium.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... zirconium. 700.16 Section 700.16 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN... cosmetic products containing zirconium. (a) Zirconium-containing complexes have been used as an ingredient... indicates that certain zirconium compounds have caused human skin granulomas and toxic effects in the...

  11. Shell model description of zirconium isotopes

    SciTech Connect

    Sieja, K.; Nowacki, F.; Langanke, K.; Martinez-Pinedo, G.

    2009-06-15

    We calculate the low-lying spectra and several high-spin states of zirconium isotopes (Z=40) with neutron numbers from N=50 to N=58 using a large valence space with the {sup 78}Ni inert core, which a priori allows one to study the interplay between spherical and deformed configurations, necessary for the description of nuclides in this part of the nuclear chart. The effective interaction is derived by monopole corrections of the realistic G matrix. We reproduce essential nuclear properties, such as subshell closures in {sup 96}Zr and {sup 98}Zr. The spherical-to-deformed shape transition in {sup 100}Zr is addressed as well.

  12. Short-time oxidation of zirconium.

    NASA Technical Reports Server (NTRS)

    Srivastava, L. P.; Archbold, T. F.

    1972-01-01

    Study of zirconium oxidation kinetics for maximum exposure times of 3 min and in the temperature range 440 to 850 C. 'Discontinuous' oxidation runs were employed whereby a specimen was inserted into the gas stream for a predetermined time, removed and weighed, and reinserted into the oxidation atmosphere. It is considered that the increase in the observed activation energy for the early stage parabolic oxidation is a manifestation of a change from an n-type oxide to a predominantly p-type oxide, in agreement with the authors' earlier conclusion (1971) based on pressure effects.

  13. ZIRCONIUM-TITANIUM-BERYLLIUM BRAZING ALLOY

    DOEpatents

    Gilliland, R.G.; Patriarca, P.; Slaughter, G.M.; Williams, L.C.

    1962-06-12

    A new and improved ternary alloy is described which is of particular utility in braze-bonding parts made of a refractory metal selected from Group IV, V, and VI of the periodic table and alloys containing said metal as a predominating alloying ingredient. The brazing alloy contains, by weight, 40 to 50 per cent zirconium, 40 to 50 per cent titanium, and the balance beryllium in amounts ranging from 1 to 20 per cent, said alloy having a melting point in the range 950 to 1400 deg C. (AEC)

  14. The irradiation effects on zirconium alloys

    NASA Astrophysics Data System (ADS)

    Negut, Gh.; Ancuta, M.; Radu, V.; Ionescu, S.; Stefan, V.; Uta, O.; Prisecaru, I.; Danila, N.

    2007-05-01

    Pressure tube samples were irradiated under helium atmosphere in the TRIGA Steady State Research and Material Test Reactor of the Romanian Institute for Nuclear Research (INR). These samples are made of the Zr-2.5%Nb alloy used as structural material for the CANDU Romanian power reactors. After irradiation, mechanical tests were performed in the Post Irradiation Examination Laboratory (PIEL) to study the influence of irradiation on zirconium alloys mechanical behaviour. The tensile test results were used for structural integrity assessment. Results of the tests are presented. The paper presents, also, pressure tube structural integrity assessment.

  15. METHOD FOR DISSOLVING ZIRCONIUM-URANIUM COMPOSITIONS

    DOEpatents

    Gens, T.A.

    1961-07-18

    A method is descrioed for treating a zirconium-- uranium composition to form a stable solution from which uranium and other values may be extracted by contacting the composition with at least a 4 molar aqueous solution of ammonium fluoride at a temperature of about 100 deg C, adding a peroxide, in incremental amounts, to the heated solution throughout the period of dissolution until all of the uranium is converted to soluble uranyl salt, adding nitric acid to the resultant solution to form a solvent extraction feed solution to convert the uranyl salt to a solvent extractable state, and thereafter recovering the uranium and other desired values from the feed solution by solvent extraction.

  16. Cherenkov and Scintillation Properties of Cubic Zirconium

    NASA Technical Reports Server (NTRS)

    Christl, M.J.; Adams, J.H.; Parnell, T.A.; Kuznetsov, E.N.

    2008-01-01

    Cubic zirconium (CZ) is a high index of refraction (n =2.17) material that we have investigated for Cherenkov counter applications. Laboratory and proton accelerator tests of an 18cc sample of CZ show that the expected fast Cherenkov response is accompanied by a longer scintillation component that can be separated by pulse shaping. This presents the possibility of novel particle spectrometers which exploits both properties of CZ. Other high index materials being examined for Cherenkov applications will be discussed. Results from laboratory tests and an accelerator exposure will be presented and a potential application in solar energetic particle instruments will be discussed

  17. In situ hydrogen loading on zirconium powder

    PubMed Central

    Maimaitiyili, Tuerdi; Blomqvist, Jakob; Steuwer, Axel; Bjerkén, Christina; Zanellato, Olivier; Blackmur, Matthew S.; Andrieux, Jérôme; Ribeiro, Fabienne

    2015-01-01

    For the first time, various hydride phases in a zirconium–hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr–H phase diagram are obtained from a single experimental arrangement. PMID:26134803

  18. RECOVERY OF URANIUM FROM ZIRCONIUM-URANIUM NUCLEAR FUELS

    DOEpatents

    Gens, T.A.

    1962-07-10

    An improvement was made in a process of recovering uranium from a uranium-zirconium composition which was hydrochlorinated with gsseous hydrogen chloride at a temperature of from 350 to 800 deg C resulting in volatilization of the zirconium, as zirconium tetrachloride, and the formation of a uranium containing nitric acid insoluble residue. The improvement consists of reacting the nitric acid insoluble hydrochlorination residue with gaseous carbon tetrachloride at a temperature in the range 550 to 600 deg C, and thereafter recovering the resulting uranium chloride vapors. (AEC)

  19. METHOD OF PREPARING SINTERED ZIRCONIUM METAL FROM ITS HYDRIDES

    DOEpatents

    Angier, R.P.

    1958-02-11

    The invention relates to the preparation of metal shapes from zirconium hydride by powder metallurgical techniques. The zirconium hydride powder which is to be used for this purpose can be prepared by rendering massive pieces of crystal bar zirconium friable by heat treatment in purified hydrogen. This any then be ground into powder and powder can be handled in the air without danger of it igniting. It may then be compacted in the normal manner by being piaced in a die. The compact is sintered under vacuum conditions preferably at a temperature ranging from 1200 to 1300 deg C and for periods of one to three hours.

  20. SEPARATION OF URANIUM FROM ZIRCONIUM AND NIOBIUM BY SOLVENT EXTRACTION

    DOEpatents

    Voiland, E.E.

    1958-05-01

    A process for separation of the uranium from zirconium and/or niobium values contained in 3 to 7M aqueous nitric acid solutions is described. This is accomplished by adding phosphoric acid anions to the nitric acid solution containing the uranium, zirconium, and/or niobium in an amount sufficient to make the solution 0.05 to 0.2M in phosphate ion and contacting the solution with an organic water-immiscible solvent such as MEK, whereby the uranyl values are taken up by the extract phase while the zirconium and niobium preferentially remain in the aqueous raffinate.

  1. Amine-intercalated α-zirconium phosphates as lubricant additives

    NASA Astrophysics Data System (ADS)

    Xiao, Huaping; Dai, Wei; Kan, Yuwei; Clearfield, Abraham; Liang, Hong

    2015-02-01

    In this study, three types of amines intercalated α-zirconium phosphate nanosheets with different interspaces were synthesized and examined as lubricant additives to a mineral oil. Results from tribological experiments illustrated that these additives improved lubricating performance. Results of rheological experiments showed that the viscosity of the mineral oil was effectively reduced with the addition of α-zirconium phosphate nanosheets. The two-dimensional structure, with larger interspaces, resulting from amine intercalation, exhibited improved effectiveness in reducing viscosity. This study demonstrates that the nanosheet structure of α-zirconium phosphates is effective in friction reduction. The manufacture of lubricants with tailored viscosity is possible by using different intercalators.

  2. Crystal Structure of the ZrO Phase at Zirconium/Zirconium Oxide Interfaces**

    PubMed Central

    Nicholls, Rebecca J; Ni, Na; Lozano-Perez, Sergio; London, Andrew; McComb, David W; Nellist, Peter D; Grovenor, Chris RM; Pickard, Chris J; Yates, Jonathan R

    2015-01-01

    Zirconium-based alloys are used in water-cooled nuclear reactors for both nuclear fuel cladding and structural components. Under this harsh environment, the main factor limiting the service life of zirconium cladding, and hence fuel burn-up efficiency, is water corrosion. This oxidation process has recently been linked to the presence of a sub-oxide phase with well-defined composition but unknown structure at the metal–oxide interface. In this paper, the combination of first-principles materials modeling and high-resolution electron microscopy is used to identify the structure of this sub-oxide phase, bringing us a step closer to developing strategies to mitigate aqueous oxidation in Zr alloys and prolong the operational lifetime of commercial fuel cladding alloys. PMID:25892957

  3. EPDL97: the evaluated photo data library `97 version

    SciTech Connect

    Cullen, D.E.; Hubbell, J.H.; Kissel, L.

    1997-09-19

    The Evaluated Photon Data Library, 1997 version (EPLD97), is designed for use in photon transport calculations at Lawrence Livermore National Laboratory. This library includes photon interaction data for all elements with atomic number between Z = 1 (hydrogne) and 100 (fermium), including: photoionization, photoexcitation, coherent and incoherent scattering, and pair and triplet porduction cross sections. For use in applications data is provided for all elements over the energy range 1 eV to 100 GeV. This report documents the sources and treatment of the data included inthis library. EPDL97 completely supersedes the earlier 1989 version of EPDL and it is highly recommended that useres only use the most recent version of this library.

  4. Investigation of Electrochemical Recovery of Zirconium from Spent Nuclear Fuels

    SciTech Connect

    Simpson, Michael; Hwang, II-Soon

    2014-06-01

    This project uses both modeling and experimental studies to design optimal electrochemical technology methods for recovery of zirconium from used nuclear fuel rods for more effective waste management. The objectives are to provide a means of efficiently separating zirconium into metallic high-level waste forms and to support development of a process for decontamination of zircaloy hulls to enable their disposal as low- and intermediate-level waste. Modeling work includes extension of a 3D model previously developed by Seoul National University for uranium electrorefining by adding the ability to predict zirconium behavior. Experimental validation activities include tests for recovery of zirconium from molten salt solutions and aqueous tests using surrogate materials. *This is a summary of the FY 2013 progress for I-NERI project # 2010-001-K provided to the I-NERI office.

  5. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... the following substances: Lead strontium titanium zirconium oxide (PMN P-11-270; CAS No. 61461-40-3... strontium titanium tungsten oxide (PMN P-11-272; CAS No. 1262279-30-0); Lanthanum lead titanium...

  6. 40 CFR 721.10602 - Lead niobium titanium zirconium oxide.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... the following substances: Lead strontium titanium zirconium oxide (PMN P-11-270; CAS No. 61461-40-3... strontium titanium tungsten oxide (PMN P-11-272; CAS No. 1262279-30-0); Lanthanum lead titanium...

  7. Hydrogenation of zirconium film by implantation of hydrogen ions

    NASA Astrophysics Data System (ADS)

    Yang, LIU; Kaihong, FANG; Huiyi, LV; Jiwei, LIU; Boyu, WANG

    2017-03-01

    In order to understand the drive-in target in a D–D type neutron generator, it is essential to study the mechanism of the interaction between hydrogen ion beams and the hydrogen-absorbing metal film. The present research concerns the nucleation of hydride within zirconium film implanted with hydrogen ions. Doses of 30 keV hydrogen ions ranging from 4.30 × 1017 to 1.43 × 1018 ions cm‑2 were loaded into the zirconium film through the ion beam implantation technique. Features of the surface morphology and transformation of phase structures were investigated with scanning electron microscopy, atomic force microscopy and x-ray diffraction. Confirmation of the formation of δ phase zirconium hydride in the implanted samples was first made by x-ray diffraction, and the different stages in the gradual nucleation and growth of zirconium hydride were then observed by atomic force microscope and scanning electron microscopy.

  8. Nucleation Pathways For Freezing Of Two Grades Of Zirconium

    NASA Technical Reports Server (NTRS)

    Rhim, Won-Kyu; Rulison, Aaron; Bayuzick, Robert; Hofmeister, William; Morton, Craig

    1996-01-01

    Report discusses classical nucleation theory of freezing and describes experimental study of nucleation mechanisms that predominate during freezing of spherical specimens of initially molten zirconium levitated electrostatically in vacuum.

  9. Process for massively hydriding zirconium--uranium fuel elements

    DOEpatents

    Katz, N.H.

    1973-12-01

    A method is described of hydriding uranium-zirconium alloy by heating the alloy in a vacuum, introducing hydrogen and maintaining an elevated temperature until occurrence of the beta--delta phase transformation and isobarically cooling the composition. (Official Gazette)

  10. PRECIPITATION OF ZIRCONIUM AND FLUORIDE IONS FROM SOLUTIONS

    DOEpatents

    Newby, B.J.

    1963-06-11

    A process is given for removing zirconium and fluorine ions from aqueous solutions also containing uranium(VI). The precipitation is carried out with sodium formate, and the uranium remains in solution. (AEC)

  11. Collinear laser spectroscopy of radioisotopes of zirconium

    NASA Astrophysics Data System (ADS)

    Thayer, H. L.; Billowes, J.; Campbell, P.; Dendooven, P.; Flanagan, K. T.; Forest, D. H.; Griffith, J. A. R.; Huikari, J.; Jokinen, A.; Moore, R.; Nieminen, A.; Tungate, G.; Zemlyanoi, S.; Äystö, J.

    2003-09-01

    Isotope shifts and hyperfine structures have been measured for radioisotopes of ionic zirconium using on-line laser spectroscopy at the IGISOL facility in Jyväskylä, where the installation of an ion beam cooler/buncher has significantly improved the experimental sensitivity. Measurements have been made on all the neutron-deficient isotopes from 87Zr to 90Zr, including the isomers 87m,89mZr, and the neutron-rich isotopes from 96Zr to 102Zr. The change in mean square charge radii between the isotopes and the nuclear moments of the odd isotopes have been extracted. The data show a sudden increase in the mean square charge radius at mass A = 100, consistent with an onset of nuclear deformation which has been observed in the gamma ray spectroscopy of isotope chains in this region of the nuclear chart.

  12. Plastic deformation of polycrystalline zirconium carbide

    NASA Technical Reports Server (NTRS)

    Darolia, R.; Archbold, T. F.

    1976-01-01

    The compressive yield strength of arc-melted polycrystalline zirconium carbide has been found to vary from 77 kg per sq mm at 1200 C to 19 kg per sq mm at 1800 C. Yield drops were observed with plastic strain-rates greater than 0.003/sec but not with slower strain rates. Strain-rate change experiments yielded values for the strain-rate sensitivity parameter m which range from 6.5 at 1500 C to 3.8 at 1800 C, and the product dislocation velocity stress exponent times T was found to decrease linearly with increasing temperature. The deformation rate results are consistent with the Kelly-Rowcliffe model in which the diffusion of carbon assists the motion of dislocations.

  13. Zirconium Hydride Space Power Reactor design.

    NASA Technical Reports Server (NTRS)

    Asquith, J. G.; Mason, D. G.; Stamp, S.

    1972-01-01

    The Zirconium Hydride Space Power Reactor being designed and fabricated at Atomics International is intended for a wide range of potential applications. Throughout the program a series of reactor designs have been evaluated to establish the unique requirements imposed by coupling with various power conversion systems and for specific applications. Current design and development emphasis is upon a 100 kilowatt thermal reactor for application in a 5 kwe thermoelectric space power generating system, which is scheduled to be fabricated and ground tested in the mid 70s. The reactor design considerations reviewed in this paper will be discussed in the context of this 100 kwt reactor and a 300 kwt reactor previously designed for larger power demand applications.

  14. Mid-term survivorship and clinical outcomes of cobalt-chrome and oxidized zirconium on highly crosslinked polyethylene

    PubMed Central

    Petis, Stephen M.; Vasarhelyi, Edward M.; Lanting, Brent A.; Howard, James L.; Naudie, Douglas D.R.; Somerville, Lyndsay E.; McCalden, Richard W.

    2016-01-01

    Background The choice of bearing articulation for total hip arthroplasty in younger patients is amenable to debate. We compared mid-term patient-reported outcomes and survivorship across 2 different bearing articulations in a young patient cohort. Methods We reviewed patients with cobalt-chrome or oxidized zirconium on highly crosslinked polyethylene who were followed prospectively between 2004 and 2012. Kaplan–Meier analysis was used to determine predicted cumulative survivorship at 5 years with all-cause and aseptic revisions as the outcome. We compared patient-reported outcomes, including the Harris hip score (HHS), Western Ontario and McMaster University Osteoarthritis Index (WOMAC) and Short-form 12 (SF-12) scores. Results A total of 622 patients were followed during the study period. Mean follow-up was 8.2 (range 2.0–10.6) years for cobalt-chrome and 7.8 (range 2.1–10.7) years for oxidized zirconium. Mean age was 54.9 ± 10.6 years for cobalt-chrome and 54.8 ± 10.7 years for oxidized zirconium. Implant survivorship was 96.0% (95% confidence interval [CI] 94.9%–97.1%) for cobalt-chrome and 98.7% (95% CI 98.0%–99.4%) for oxidized zirconium on highly crosslinked polyethylene for all-cause revisions, and 97.2% (95% CI 96.2%–98.2%) for cobalt-chrome and 99.0% (95% CI 98.4%–99.6%) for oxidized zirconium for aseptic revisions. An age-, sex- and diagnosis-matched comparison of the HHS, WOMAC and SF-12 scores demonstrated no significant changes in clinical outcomes across the groups. Conclusion Both bearing surface couples demonstrated excellent mid-term survivorship and outcomes in young patient cohorts. Future analyses on wear and costs are warranted to elicit differences between the groups at long-term follow-up. PMID:26812409

  15. Electrical Relaxation in Calcium Fluoride Doped with Thorium and Zirconium.

    DTIC Science & Technology

    1986-09-01

    9, 1055 (1976). 4. M. Ouwerkerk , F. F. Veldkamp, N. H. Andersen, and J . Schoonman, Solid State Ionics, 16, 125 (1985). 5. S. F. Matar, J . M. Reau, P...AD-Al?2 366 ELECTRICAL RELAXATION IN CALCIUM FLUORIDE DOPED WITH L1/ THORIUM AND ZIRCONIUM(U) NAYRL ACADEMY ANNAPOLIS MD DEPT OF PHYSICS J J ...Fluoride Doped with Thorium and Zirconium by John J . Fontanella & Mary C. Wintersgill Prepared for Publication in Crystal Lattice Defects and Amorphous

  16. Critical role of nitrogen during high temperature scaling of zirconium

    NASA Technical Reports Server (NTRS)

    Evans, E. B.; Tsangarakis, N.; Probst, H. B.; Garibotti, N. J.

    1973-01-01

    The mechanisms of scale cracking, scale color changes, and scale growth, and their interrelations, were studied in zirconium specimens at elevated temperatures in air, oxygen and nitrogen. Nitrogen was found to be responsible for monoclinic-to-cubic ZrO2 conversion, for scale cracking and breakaway on zirconium nitride, and for the formation of ZrN on the metal interface underneath an outer oxide layer.

  17. STS-97 Prelaunch Press Conference

    NASA Technical Reports Server (NTRS)

    2000-01-01

    Bruce Buckingham, NASA Public Affairs, introduces Ron Dittemore, NASA Shuttle Program Manager, Bob Cabana, International Space Station (ISS) Manager, International Operations, NASA, Michael Vachon, Canadian Space Agency, David King, NASA Director of Shuttle Processing, and Lieutenant Ken Ferland, 45th Weather Squadron, US Air Force. They each give a brief statement on the STS-97 Endeavour mission, launch, and weather status and answer questions from the press.

  18. Zirconium alkoxide interfaces for adhesion enhancement and electrocatalysis

    NASA Astrophysics Data System (ADS)

    Vanderkam, Susan Killian

    Tetra(tert-butoxy)zirconium was chemisorbed onto the native oxide layers of aluminum, iron, copper, and porous silicon, forming surface bound di- or tri-alkoxy zirconium species. Poly(ethylene- co-acrylic acid) was subsequently reacted with the surface forming chemically bound copolymer through carboxyzirconium linkages. Copolymer bound through the zirconium complex adhered to the metal oxide surfaces better than without the zirconium alkoxide intermediate, as determined by FTIR spectroscopy. Copper substrates were subjected to a variety of stability tests, including exposure to ambient conditions, base washing, and chronocoulometry. The copper-zirconium-copolymer ensemble was shown to be very stable in all of these tests. Indium tin oxide (ITO) powder was titrated to determine surface hydroxyl content per unit area. ITO-coated glass slides were reacted with tetra( tert-butoxy)zirconium, and subsequently with both carboxylic acid and phenol derivatives. Ferrocene-carboxyzirconium-coated ITO was characterized electrochemically, and the surface loading of ferrocene was found to be approximately one monolayer. Phenoxyzirconium-coated ITO was also characterized electrochemically and tested for electrocatalytic properties for the oxidation of several compounds in solution. Phenoxyzirconium-coated ITO was found to improve the oxidation kinetics for ferrocene and tetramethylphenylenediamine in acetonitrile.

  19. Quercetin as colorimetric reagent for determination of zirconium

    USGS Publications Warehouse

    Grimaldi, F.S.; White, C.E.

    1953-01-01

    Methods described in the literature for the determination of zirconium are generally designed for relatively large amounts of this element. A good procedure using colorimetric reagent for the determination of trace amounts is desirable. Quercetin has been found to yield a sensitive color reaction with zirconium suitable for the determination of from 0.1 to 50?? of zirconium dioxide. The procedure developed involves the separation of zirconium from interfering elements by precipitation with p-dimethylaminoazophenylarsonic acid prior to its estimation with quercetin. The quercetin reaction is carried out in 0.5N hydrochloric acid solution. Under the operating conditions it is indicated that quercetin forms a 2 to 1 complex with zirconium; however, a 2 to 1 and a 1 to 1 complex can coexist under special conditions. Approximate values for the equilibrium constants of the complexes are K1 = 0.33 ?? 10-5 and K2 = 1.3 ?? 10-9. Seven Bureau of Standards samples of glass sands and refractories were analyzed with excellent results. The method described should find considerable application in the analysis of minerals and other materials for macro as well as micro amounts of zirconium.

  20. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Definitions. 97.402 Section 97.402 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to...

  1. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Definitions. 97.402 Section 97.402 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to...

  2. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Definitions. 97.402 Section 97.402 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to...

  3. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Definitions. 97.402 Section 97.402 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to...

  4. Understanding the Irradiation Behavior of Zirconium Carbide

    SciTech Connect

    Motta, Arthur; Sridharan, Kumar; Morgan, Dane; Szlufarska, Izabela

    2013-10-11

    Zirconium carbide (ZrC) is being considered for utilization in high-temperature gas-cooled reactor fuels in deep-burn TRISO fuel. Zirconium carbide possesses a cubic B1-type crystal structure with a high melting point, exceptional hardness, and good thermal and electrical conductivities. The use of ZrC as part of the TRISO fuel requires a thorough understanding of its irradiation response. However, the radiation effects on ZrC are still poorly understood. The majority of the existing research is focused on the radiation damage phenomena at higher temperatures (>450{degree}C) where many fundamental aspects of defect production and kinetics cannot be easily distinguished. Little is known about basic defect formation, clustering, and evolution of ZrC under irradiation, although some atomistic simulation and phenomenological studies have been performed. Such detailed information is needed to construct a model describing the microstructural evolution in fast-neutron irradiated materials that will be of great technological importance for the development of ZrC-based fuel. The goal of the proposed project is to gain fundamental understanding of the radiation-induced defect formation in zirconium carbide and irradiation response by using a combination of state-of-the-art experimental methods and atomistic modeling. This project will combine (1) in situ ion irradiation at a specialized facility at a national laboratory, (2) controlled temperature proton irradiation on bulk samples, and (3) atomistic modeling to gain a fundamental understanding of defect formation in ZrC. The proposed project will cover the irradiation temperatures from cryogenic temperature to as high as 800{degree}C, and dose ranges from 0.1 to 100 dpa. The examination of this wide range of temperatures and doses allows us to obtain an experimental data set that can be effectively used to exercise and benchmark the computer calculations of defect properties. Combining the examination of radiation

  5. High-speed deformation and fracture of the dioxide-zirconium ceramics and zirconium alumina concrete

    NASA Astrophysics Data System (ADS)

    Bragov, A.; Kruszka, L.; Lomunov, A.; Konstantinov, A.; Lamzin, D.; Filippov, A.

    2012-08-01

    The results of dynamic tests of two refractory materials based on zirconium dioxide: three types of ceramics and barium-aluminate concrete. The ceramic specimens had various initial density and porosity and also differed by technology of manufacturing. Compression tests were carried out using the Kolsky technique and its updating - specimen in a rigid jacket. The dynamic stress-strain curves were obtained. The strong influence of sample's initial grain composition, mode of stressed-strained state and technologies of manufacturing of specimens onto ceramics mechanical properties is marked.

  6. PROCESS OF RECOVERING ZIRCONIUM VALUES FROM HAFNIUM VALUES BY SOLVENT EXTRACTION WITH AN ALKYL PHOSPHATE

    DOEpatents

    Peppard, D.F.

    1960-02-01

    A process of separating hafnium nitrate from zirconium nitrate contained in a nitric acid solution by selectively. extracting the zirconium nitrate with a water-immiscible alkyl phosphate is reported.

  7. Elimination of phosphate and zirconium in the high-activity fraction resulting from TRUEX partitioning of ICPP zirconium calcines

    SciTech Connect

    Brewer, K.N.; Tillotson, R.D.; Tullock, P.A.

    1997-07-01

    Laboratory testing was undertaken with the aim of developing a TRUEX flowsheet that would efficiently remove actinides from solutions of dissolved zirconium calcine and minimize the glass volume produced from the ensuing high-activity fraction. A TRUEX flowsheet is recommended for testing in the 2-cm centrifugal contactor pilot-plant based on the results from this testing. These laboratory tests show that zirconium recovery in the high activity fraction is minimized by scrubbing with an optimized NHF concentration of 0.2 M. This NH4F concentration in the scrub allowed the HEDPA strip concentration to be reduced from 0.04 M to 0.004 M because HEDPA is not consumed by zirconium. Complete TRU stripping was also achieved in these laboratory tests with 0.004 M HEDPA. Data from the small-scale laboratory batch contact tests were used in the Generic TRUEX Model (GTM) to evaluate the proposed flowsheet under counter-current conditions. GTM results indicate the raffinate will meet the Class A non-TRU limit of < 10 nCi/g in six extraction stages (O/A = 1), and quantitative actinide recovery will be achieved with the 0.004 M HEDPA in six strip stages (O/A = 1). Only 6.6 % of the initial zirconium concentration is anticipated to be recovered with the actinides, indicating the four scrub stages (O/A = 3) efficiently removes zirconium from the TRUEX solvent. In addition to recommending an improved TRUEX flowsheet for testing in the 2-cm centrifugal contactor pilot-plant, this work has shown that small reductions in zirconium extraction drastically improves flowsheet performance. These small changes in zirconium extraction can be accomplished by modifying the calcine dissolution parameters. Therefore, further calcine dissolution testing followed by TRUEX testing with the resulting feed solutions is also recommended.

  8. Mechanical properties of zirconium alloys and zirconium hydrides predicted from density functional perturbation theory

    DOE PAGES

    Weck, Philippe F.; Kim, Eunja; Tikare, Veena; ...

    2015-10-13

    Here, the elastic properties and mechanical stability of zirconium alloys and zirconium hydrides have been investigated within the framework of density functional perturbation theory. Results show that the lowest-energy cubic Pn-3m with combining macron]m polymorph of δ-ZrH1.5 does not satisfy all the Born requirements for mechanical stability, unlike its nearly degenerate tetragonal P42/mcm polymorph. Elastic moduli predicted with the Voigt–Reuss–Hill approximations suggest that mechanical stability of α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates is limited by the shear modulus. According to both Pugh's and Poisson's ratios, α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates can be considered ductile. The Debye temperatures predicted formore » γ-ZrH, δ-ZrH1.5 and ε-ZrH2 are θD = 299.7, 415.6 and 356.9 K, respectively, while θD = 273.6, 284.2, 264.1 and 257.1 K for the α-Zr, Zry-4, ZIRLO and M5 matrices, i.e. suggesting that Zry-4 possesses the highest micro-hardness among Zr matrices.« less

  9. Mechanical properties of zirconium alloys and zirconium hydrides predicted from density functional perturbation theory

    SciTech Connect

    Weck, Philippe F.; Kim, Eunja; Tikare, Veena; Mitchell, John A.

    2015-10-13

    Here, the elastic properties and mechanical stability of zirconium alloys and zirconium hydrides have been investigated within the framework of density functional perturbation theory. Results show that the lowest-energy cubic Pn-3m with combining macron]m polymorph of δ-ZrH1.5 does not satisfy all the Born requirements for mechanical stability, unlike its nearly degenerate tetragonal P42/mcm polymorph. Elastic moduli predicted with the Voigt–Reuss–Hill approximations suggest that mechanical stability of α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates is limited by the shear modulus. According to both Pugh's and Poisson's ratios, α-Zr, Zr-alloy and Zr-hydride polycrystalline aggregates can be considered ductile. The Debye temperatures predicted for γ-ZrH, δ-ZrH1.5 and ε-ZrH2 are θD = 299.7, 415.6 and 356.9 K, respectively, while θD = 273.6, 284.2, 264.1 and 257.1 K for the α-Zr, Zry-4, ZIRLO and M5 matrices, i.e. suggesting that Zry-4 possesses the highest micro-hardness among Zr matrices.

  10. Inhibition of ice growth and recrystallization by zirconium acetate and zirconium acetate hydroxide.

    PubMed

    Mizrahy, Ortal; Bar-Dolev, Maya; Guy, Shlomit; Braslavsky, Ido

    2013-01-01

    The control over ice crystal growth, melting, and shaping is important in a variety of fields, including cell and food preservation and ice templating for the production of composite materials. Control over ice growth remains a challenge in industry, and the demand for new cryoprotectants is high. Naturally occurring cryoprotectants, such as antifreeze proteins (AFPs), present one solution for modulating ice crystal growth; however, the production of AFPs is expensive and inefficient. These obstacles can be overcome by identifying synthetic substitutes with similar AFP properties. Zirconium acetate (ZRA) was recently found to induce the formation of hexagonal cavities in materials prepared by ice templating. Here, we continue this line of study and examine the effects of ZRA and a related compound, zirconium acetate hydroxide (ZRAH), on ice growth, shaping, and recrystallization. We found that the growth rate of ice crystals was significantly reduced in the presence of ZRA and ZRAH, and that solutions containing these compounds display a small degree of thermal hysteresis, depending on the solution pH. The compounds were found to inhibit recrystallization in a manner similar to that observed in the presence of AFPs. The favorable properties of ZRA and ZRAH suggest tremendous potential utility in industrial applications.

  11. Synthesis and characterization of a mesoporous hydrous zirconium oxide used for arsenic removal from drinking water

    SciTech Connect

    Bortun, Anatoly; Bortun, Mila; Pardini, James; Khainakov, Sergei A.; Garcia, Jose R.

    2010-02-15

    Powder (20-50 {mu}m) mesoporous hydrous zirconium oxide was prepared from a zirconium salt granular precursor. The effect of some process parameters on product morphology, porous structure and adsorption performance has been studied. The use of hydrous zirconium oxide for selective arsenic removal from drinking water is discussed.

  12. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 32 2013-07-01 2013-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  13. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 32 2012-07-01 2012-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  14. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 31 2011-07-01 2011-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  15. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 31 2014-07-01 2014-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  16. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  17. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants to waters of...

  18. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  19. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  20. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  1. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  2. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... METAL POWDERS POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants...

  3. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  4. 40 CFR 471.90 - Applicability; description of the zirconium-hafnium forming subcategory.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... zirconium-hafnium forming subcategory. 471.90 Section 471.90 Protection of Environment ENVIRONMENTAL... POINT SOURCE CATEGORY Zirconium-Hafnium Forming Subcategory § 471.90 Applicability; description of the zirconium-hafnium forming subcategory. This subpart applies to discharges of pollutants to waters of...

  5. 40 CFR 721.10089 - Modified salicylic acid, zirconium complex (generic).

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 30 2010-07-01 2010-07-01 false Modified salicylic acid, zirconium... Specific Chemical Substances § 721.10089 Modified salicylic acid, zirconium complex (generic). (a) Chemical... as modified salicylic acid, zirconium complex (PMN P-00-552) is subject to reporting under...

  6. 40 CFR 421.330 - Applicability: Description of the primary zirconium and hafnium subcategory.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... primary zirconium and hafnium subcategory. 421.330 Section 421.330 Protection of Environment ENVIRONMENTAL... CATEGORY Primary Zirconium and Hafnium Subcategory § 421.330 Applicability: Description of the primary zirconium and hafnium subcategory. The provisions of this subpart are applicable to discharges...

  7. Process for electrolytic deposition of metals on zirconium materials

    DOEpatents

    Donaghy, Robert E.

    1979-01-30

    A process for the electrolytic deposition of a metal layer on an article comprised of zirconium or a zirconium alloy is disclosed. The article is activated in an aged aqueous solution comprising from about 10 to about 20 grams per liter ammonium bifluoride and from about 0.75 to about 2 grams per liter of sulfuric acid. The solution is aged by immersion of pickled zirconium in the solution for at least about 10 minutes. The loosely adhering film formed on the article in the activating step is removed and the article is contacted with an electrolytic plating solution containing the metal to be deposited on the article in the presence of an electrode receiving current.

  8. METHOD OF FABRICATING A URANIUM-ZIRCONIUM HYDRIDE REACTOR CORE

    DOEpatents

    Weeks, I.F.; Goeddel, W.V.

    1960-03-22

    A method is described of evenly dispersing uranlum metal in a zirconium hydride moderator to produce a fuel element for nuclear reactors. According to the invention enriched uranium hydride and zirconium hydride powders of 200 mesh particle size are thoroughly admixed to form a mixture containing 0.1 to 3% by weight of U/sup 235/ hydride. The mixed powders are placed in a die and pressed at 100 tons per square inch at room temperature. The resultant compacts are heated in a vacuum to 300 deg C, whereby the uranium hydride deoomposes into uranium metal and hydrogen gas. The escaping hydrogen gas forms a porous matrix of zirconium hydride, with uramum metal evenly dispersed therethrough. The advantage of the invention is that the porosity and uranium distribution of the final fuel element can be more closely determined and controlled than was possible using prior methods of producing such fuel ele- ments.

  9. Process for electroless deposition of metals on zirconium materials

    DOEpatents

    Donaghy, Robert E.

    1978-01-01

    A process for the electroless deposition of a metal layer on an article comprised of zirconium or a zirconium alloy is disclosed. The article is activated in an aged aqueous solution comprising from about 10 to about 20 grams per liter ammonium bifluoride and from about 0.75 to about 2 grams per liter of sulfuric acid. The solution is aged by immersion of pickled zirconium in the solution for at least about 10 minutes. The loosely adhering film formed on the article in the activating step is removed and the article is contacted with an electroless plating solution containing the metal to be deposited on the article upon sufficient contact with the article.

  10. Studies on synthesis esterified zirconium glyphosates and their hydrophobic properties

    NASA Astrophysics Data System (ADS)

    Zhang, Yaqing; Li, Minglei; Ji, Xuemei; Xu, Qinghong

    2010-03-01

    A series of new organic-modified zirconium glyphosate compounds were synthesized based on the reactions between esterified glyphosates and ZrOCl 2. FT-IR spectra, solid-state 31P MAS NMR and elementary analysis proved the formation of these new compounds. Powder X-ray diffraction (PXRD) patterns and transmission electron microscope (TEM) images proved these compounds had lamellar structures. Scanning electronic microscope (SEM) images showed that solvents used in synthesis had great influence on the morphologies of products. Water contact angle measurements showed that the hydrophobic property of the products was a function of the number of carbon in esterified glyphosates, increased from 0° of zirconium glyphosate to 133° of dodecyl zirconium glyphosate. The present study offered a new route to synthesize organic-modified α-Zr(HPO 4) 2·H 2O (α-ZrP) materials with various morphology and controllable hydrophobic property.

  11. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Question pools. 97.523 Section 97.523 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining...

  12. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  13. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  14. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  15. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Question pools. 97.523 Section 97.523 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining...

  16. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Question pools. 97.523 Section 97.523 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining...

  17. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  18. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  19. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  20. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Question pools. 97.523 Section 97.523 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining...

  1. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  2. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  3. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  4. 47 CFR 97.217 - Telemetry.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Telemetry. 97.217 Section 97.217 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.217 Telemetry. Telemetry transmitted by an amateur station on or within...

  5. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  6. 47 CFR 97.523 - Question pools.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Question pools. 97.523 Section 97.523 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.523 Question pools. All VECs must cooperate in maintaining...

  7. 47 CFR 97.25 - License term.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false License term. 97.25 Section 97.25 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE General Provisions § 97.25 License term. An amateur service license is normally granted for a...

  8. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Station control. 97.109 Section 97.109 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at...

  9. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  10. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  11. 47 CFR 97.511 - Examinee conduct.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Examinee conduct. 97.511 Section 97.511 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Qualifying Examination Systems § 97.511 Examinee conduct. Each examinee must comply with...

  12. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2010-04-01 2010-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  13. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  14. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  15. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  16. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  17. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  18. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 1 2013-07-01 2013-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  19. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 1 2012-07-01 2012-07-01 false Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  20. 29 CFR 97.34 - Copyrights.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 1 2014-07-01 2013-07-01 true Copyrights. 97.34 Section 97.34 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.34 Copyrights. The... copyright in any work developed under a grant, subgrant, or contract under a grant or subgrant; and (b)...

  1. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2011-04-01 2011-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  2. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2014-04-01 2014-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  3. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2012-04-01 2011-04-01 true Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  4. 27 CFR 71.97 - Powers.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 2 2013-04-01 2013-04-01 false Powers. 71.97 Section 71.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE... Judges § 71.97 Powers. Administrative law judges shall have authority to (a) administer oaths...

  5. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 4 2011-10-01 2011-10-01 false Crank pins. 230.97 Section 230.97 Transportation... § 230.97 Crank pins. (a) General provisions. Crank pins shall be securely applied. Securing the fit of a loose crank pin by shimming, prick punching, or welding is not permitted. (b) Maintenance. Crank...

  6. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 49 Transportation 4 2012-10-01 2012-10-01 false Crank pins. 230.97 Section 230.97 Transportation... § 230.97 Crank pins. (a) General provisions. Crank pins shall be securely applied. Securing the fit of a loose crank pin by shimming, prick punching, or welding is not permitted. (b) Maintenance. Crank...

  7. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 4 2010-10-01 2010-10-01 false Crank pins. 230.97 Section 230.97 Transportation... § 230.97 Crank pins. (a) General provisions. Crank pins shall be securely applied. Securing the fit of a loose crank pin by shimming, prick punching, or welding is not permitted. (b) Maintenance. Crank...

  8. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 49 Transportation 4 2013-10-01 2013-10-01 false Crank pins. 230.97 Section 230.97 Transportation... § 230.97 Crank pins. (a) General provisions. Crank pins shall be securely applied. Securing the fit of a loose crank pin by shimming, prick punching, or welding is not permitted. (b) Maintenance. Crank...

  9. 40 CFR 97.101 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.101 Section 97.101 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Provisions § 97.101 Purpose. This subpart and subparts BB through II set forth the general provisions and...

  10. 40 CFR 97.1 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.1 Section 97.1 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Provisions § 97.1 Purpose. This part establishes general provisions and the applicability,...

  11. 40 CFR 97.301 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.301 Section 97.301 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... General Provisions § 97.301 Purpose. This subpart and subparts BBBB through IIII set forth the...

  12. 40 CFR 97.201 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.201 Section 97.201 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.201 Purpose. This subpart and subparts BBB through III set forth the general provisions and...

  13. 50 CFR 300.97 - Inseason orders.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 50 Wildlife and Fisheries 11 2014-10-01 2014-10-01 false Inseason orders. 300.97 Section 300.97 Wildlife and Fisheries INTERNATIONAL FISHING AND RELATED ACTIVITIES INTERNATIONAL FISHERIES REGULATIONS Fraser River Sockeye and Pink Salmon Fisheries § 300.97 Inseason orders. (a) During the fishing...

  14. 50 CFR 300.97 - Inseason orders.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 50 Wildlife and Fisheries 9 2011-10-01 2011-10-01 false Inseason orders. 300.97 Section 300.97 Wildlife and Fisheries INTERNATIONAL FISHING AND RELATED ACTIVITIES INTERNATIONAL FISHERIES REGULATIONS Fraser River Sockeye and Pink Salmon Fisheries § 300.97 Inseason orders. (a) During the fishing...

  15. 50 CFR 300.97 - Inseason orders.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 50 Wildlife and Fisheries 11 2013-10-01 2013-10-01 false Inseason orders. 300.97 Section 300.97 Wildlife and Fisheries INTERNATIONAL FISHING AND RELATED ACTIVITIES INTERNATIONAL FISHERIES REGULATIONS Fraser River Sockeye and Pink Salmon Fisheries § 300.97 Inseason orders. (a) During the fishing...

  16. 50 CFR 300.97 - Inseason orders.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 50 Wildlife and Fisheries 11 2012-10-01 2012-10-01 false Inseason orders. 300.97 Section 300.97 Wildlife and Fisheries INTERNATIONAL FISHING AND RELATED ACTIVITIES INTERNATIONAL FISHERIES REGULATIONS Fraser River Sockeye and Pink Salmon Fisheries § 300.97 Inseason orders. (a) During the fishing...

  17. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 32 National Defense 3 2012-07-01 2009-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  18. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 3 2013-07-01 2013-07-01 false Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  19. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 32 National Defense 3 2014-07-01 2014-07-01 false Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  20. 29 CFR 97.25 - Program income.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Program income. 97.25 Section 97.25 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Financial Administration § 97.25 Program income. (a) General. Grantees are encouraged to earn income to defray program costs. Program income includes income from...

  1. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  2. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  3. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  4. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  5. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  6. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  7. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... Not applicable Elements 3 and 4. (2) Advanced; General; or Technician granted before March 21,...

  8. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  9. 47 CFR 97.503 - Element standards.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Element standards. 97.503 Section 97.503... SERVICE Qualifying Examination Systems § 97.503 Element standards. A written examination must be such as... question set as follows: (a) Element 2: 35 questions concerning the privileges of a Technician...

  10. 47 CFR 97.505 - Element credit.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Element credit. 97.505 Section 97.505... SERVICE Qualifying Examination Systems § 97.505 Element credit. (a) The administering VEs must give credit... operator license grant: Elements 2 and 3. (2) An unexpired (or expired but within the grace period...

  11. 9 CFR 201.97 - Annual reports.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 9 Animals and Animal Products 2 2010-01-01 2010-01-01 false Annual reports. 201.97 Section 201.97... § 201.97 Annual reports. Every packer, live poultry dealer, stockyard owner, market agency, and dealer... Administration a report on prescribed forms not later than April 15 following the calendar year end or, if...

  12. 49 CFR 585.97 - Records.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 7 2014-10-01 2014-10-01 false Records. 585.97 Section 585.97 Transportation Other Regulations Relating to Transportation (Continued) NATIONAL HIGHWAY TRAFFIC SAFETY ADMINISTRATION... Requirements § 585.97 Records. Each manufacturer must maintain records of the Vehicle Identification Number...

  13. 49 CFR 585.97 - Records.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 49 Transportation 7 2010-10-01 2010-10-01 false Records. 585.97 Section 585.97 Transportation Other Regulations Relating to Transportation (Continued) NATIONAL HIGHWAY TRAFFIC SAFETY ADMINISTRATION... Requirements § 585.97 Records. Each manufacturer must maintain records of the Vehicle Identification Number...

  14. 49 CFR 585.97 - Records.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 49 Transportation 7 2011-10-01 2011-10-01 false Records. 585.97 Section 585.97 Transportation Other Regulations Relating to Transportation (Continued) NATIONAL HIGHWAY TRAFFIC SAFETY ADMINISTRATION... Requirements § 585.97 Records. Each manufacturer must maintain records of the Vehicle Identification Number...

  15. 49 CFR 585.97 - Records.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 49 Transportation 7 2013-10-01 2013-10-01 false Records. 585.97 Section 585.97 Transportation Other Regulations Relating to Transportation (Continued) NATIONAL HIGHWAY TRAFFIC SAFETY ADMINISTRATION... Requirements § 585.97 Records. Each manufacturer must maintain records of the Vehicle Identification Number...

  16. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  17. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  18. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  19. 29 CFR 452.97 - Secret ballot.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 2 2011-07-01 2011-07-01 false Secret ballot. 452.97 Section 452.97 Labor Regulations... OF 1959 Election Procedures; Rights of Members § 452.97 Secret ballot. (a) A prime requisite of elections regulated by title IV is that they be held by secret ballot among the members or in...

  20. 29 CFR 452.97 - Secret ballot.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 2 2014-07-01 2014-07-01 false Secret ballot. 452.97 Section 452.97 Labor Regulations... OF 1959 Election Procedures; Rights of Members § 452.97 Secret ballot. (a) A prime requisite of elections regulated by title IV is that they be held by secret ballot among the members or in...

  1. 29 CFR 452.97 - Secret ballot.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 2 2010-07-01 2010-07-01 false Secret ballot. 452.97 Section 452.97 Labor Regulations... OF 1959 Election Procedures; Rights of Members § 452.97 Secret ballot. (a) A prime requisite of elections regulated by title IV is that they be held by secret ballot among the members or in...

  2. 29 CFR 452.97 - Secret ballot.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 2 2012-07-01 2012-07-01 false Secret ballot. 452.97 Section 452.97 Labor Regulations... OF 1959 Election Procedures; Rights of Members § 452.97 Secret ballot. (a) A prime requisite of elections regulated by title IV is that they be held by secret ballot among the members or in...

  3. 29 CFR 452.97 - Secret ballot.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 2 2013-07-01 2013-07-01 false Secret ballot. 452.97 Section 452.97 Labor Regulations... OF 1959 Election Procedures; Rights of Members § 452.97 Secret ballot. (a) A prime requisite of elections regulated by title IV is that they be held by secret ballot among the members or in...

  4. 47 CFR 97.117 - International communications.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false International communications. 97.117 Section 97.117 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.117 International communications. Transmissions...

  5. 27 CFR 9.97 - Sonoita.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2014-04-01 2014-04-01 false Sonoita. 9.97 Section 9.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY ALCOHOL AMERICAN VITICULTURAL AREAS Approved American Viticultural Areas § 9.97 Sonoita. (a)...

  6. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  7. 34 CFR 97.409 - Wards.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Wards. 97.409 Section 97.409 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.409 Wards. (a) Children who are wards of the State or any other...

  8. 34 CFR 97.403 - IRB duties.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false IRB duties. 97.403 Section 97.403 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.403 IRB duties. In addition to other responsibilities...

  9. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Conditions. 97.124 Section 97.124 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124...

  10. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  11. 34 CFR 97.409 - Wards.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Wards. 97.409 Section 97.409 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.409 Wards. (a) Children who are wards of the State or any other...

  12. 34 CFR 97.403 - IRB duties.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false IRB duties. 97.403 Section 97.403 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.403 IRB duties. In addition to other responsibilities...

  13. 34 CFR 97.403 - IRB duties.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false IRB duties. 97.403 Section 97.403 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.403 IRB duties. In addition to other responsibilities...

  14. 34 CFR 97.121 - [Reserved

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false 97.121 Section 97.121 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.121...

  15. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Conditions. 97.124 Section 97.124 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124...

  16. 34 CFR 97.403 - IRB duties.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false IRB duties. 97.403 Section 97.403 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.403 IRB duties. In addition to other responsibilities...

  17. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Conditions. 97.124 Section 97.124 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124...

  18. 34 CFR 97.121 - [Reserved

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false 97.121 Section 97.121 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.121...

  19. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Conditions. 97.124 Section 97.124 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124...

  20. 34 CFR 97.409 - Wards.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Wards. 97.409 Section 97.409 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.409 Wards. (a) Children who are wards of the State or any other...

  1. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  2. 34 CFR 97.121 - [Reserved

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false 97.121 Section 97.121 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.121...

  3. 34 CFR 97.121 - [Reserved

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false 97.121 Section 97.121 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.121...

  4. 34 CFR 97.121 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false 97.121 Section 97.121 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.121...

  5. 34 CFR 97.403 - IRB duties.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false IRB duties. 97.403 Section 97.403 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.403 IRB duties. In addition to other responsibilities...

  6. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  7. 34 CFR 97.124 - Conditions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Conditions. 97.124 Section 97.124 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.124...

  8. 34 CFR 97.115 - IRB records.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false IRB records. 97.115 Section 97.115 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.115 IRB...

  9. 34 CFR 97.409 - Wards.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Wards. 97.409 Section 97.409 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Additional ED Protections for Children Who Are Subjects in Research § 97.409 Wards. (a) Children who are wards of the State or any other...

  10. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  11. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  12. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 34 Education 1 2012-07-01 2012-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  13. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  14. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  15. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  16. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  17. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  18. 7 CFR 97.154 - Government employees.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Government employees. 97.154 Section 97.154... PLANT VARIETY AND PROTECTION Attorneys and Agents § 97.154 Government employees. Officers and employees... attorneys or agents in proceedings or other matters before government departments or agencies, shall not...

  19. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... STANDARDS FOR NAVAL STORES Proceedings in Case of Violation § 160.97 Publication. Composite data...

  20. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... STANDARDS FOR NAVAL STORES Proceedings in Case of Violation § 160.97 Publication. Composite data...

  1. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... STANDARDS FOR NAVAL STORES Proceedings in Case of Violation § 160.97 Publication. Composite data...

  2. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... STANDARDS FOR NAVAL STORES Proceedings in Case of Violation § 160.97 Publication. Composite data...

  3. 7 CFR 160.97 - Publication.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Publication. 160.97 Section 160.97 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards... STANDARDS FOR NAVAL STORES Proceedings in Case of Violation § 160.97 Publication. Composite data...

  4. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  5. 46 CFR 97.34-1 - Application.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Application. 97.34-1 Section 97.34-1 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Work Vests § 97.34-1 Application. (a) Provisions of this subpart shall apply to all vessels inspected...

  6. 29 CFR 97.31 - Real property.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Real property. 97.31 Section 97.31 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Changes, Property, and Subawards § 97.31 Real property. (a) Title. Subject to the obligations and conditions set forth in this section, title to real...

  7. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  8. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  9. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  10. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  11. 46 CFR 111.97-7 - Distribution.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Distribution. 111.97-7 Section 111.97-7 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) ELECTRICAL ENGINEERING ELECTRIC SYSTEMS-GENERAL REQUIREMENTS Electric Power-Operated Watertight Door Systems § 111.97-7 Distribution. (a) Each...

  12. 34 CFR 97.114 - Cooperative research.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false Cooperative research. 97.114 Section 97.114 Education... Protection of Human Subjects (Basic ED Policy for Protection of Human Research Subjects) § 97.114 Cooperative research. Cooperative research projects are those projects covered by this policy which involve more...

  13. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  14. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  15. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  16. 47 CFR 97.209 - Earth station.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Earth station. 97.209 Section 97.209... SERVICE Special Operations § 97.209 Earth station. (a) Any amateur station may be an Earth station. A holder of any class operator license may be the control operator of an Earth station, subject to...

  17. 50 CFR 27.97 - Private operations.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 50 Wildlife and Fisheries 6 2010-10-01 2010-10-01 false Private operations. 27.97 Section 27.97 Wildlife and Fisheries UNITED STATES FISH AND WILDLIFE SERVICE, DEPARTMENT OF THE INTERIOR (CONTINUED) THE NATIONAL WILDLIFE REFUGE SYSTEM PROHIBITED ACTS Other Disturbing Violations § 27.97 Private...

  18. 29 CFR 97.11 - State plans.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true State plans. 97.11 Section 97.11 Labor Office of the... LOCAL GOVERNMENTS Pre-Award Requirements § 97.11 State plans. (a) Scope. The statutes for some programs require States to submit plans before receiving grants. Under regulations implementing Executive...

  19. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 3 2010-07-01 2010-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  20. 29 CFR 97.11 - State plans.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 1 2014-07-01 2013-07-01 true State plans. 97.11 Section 97.11 Labor Office of the... LOCAL GOVERNMENTS Pre-Award Requirements § 97.11 State plans. (a) Scope. The statutes for some programs require States to submit plans before receiving grants. Under regulations implementing Executive...

  1. 40 CFR 97.61 - EPA recordation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false EPA recordation. 97.61 Section 97.61 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Transfers § 97.61...

  2. 40 CFR 97.361 - EPA recordation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false EPA recordation. 97.361 Section 97.361 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.361 EPA recordation. (a) Within 5 business days (except as provided in paragraph (b) of...

  3. 40 CFR 97.161 - EPA recordation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false EPA recordation. 97.161 Section 97.161 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR NOX Allowance Transfers § 97.161...

  4. 40 CFR 97.61 - EPA recordation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false EPA recordation. 97.61 Section 97.61 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Transfers § 97.61...

  5. 40 CFR 97.361 - EPA recordation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false EPA recordation. 97.361 Section 97.361 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.361 EPA recordation. (a) Within 5 business days (except as provided in paragraph (b) of...

  6. 40 CFR 97.361 - EPA recordation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false EPA recordation. 97.361 Section 97.361 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.361 EPA recordation. (a) Within 5 business days (except as provided in paragraph (b) of...

  7. 40 CFR 97.161 - EPA recordation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false EPA recordation. 97.161 Section 97.161 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR NOX Allowance Transfers § 97.161...

  8. 40 CFR 97.261 - EPA recordation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false EPA recordation. 97.261 Section 97.261 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.261...

  9. 40 CFR 97.261 - EPA recordation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false EPA recordation. 97.261 Section 97.261 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.261...

  10. 40 CFR 97.261 - EPA recordation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false EPA recordation. 97.261 Section 97.261 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.261...

  11. 40 CFR 97.161 - EPA recordation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 40 Protection of Environment 22 2012-07-01 2012-07-01 false EPA recordation. 97.161 Section 97.161 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR NOX Allowance Transfers § 97.161...

  12. 40 CFR 97.361 - EPA recordation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false EPA recordation. 97.361 Section 97.361 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.361 EPA recordation. (a) Within 5 business days (except as provided in paragraph (b) of...

  13. 40 CFR 97.61 - EPA recordation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false EPA recordation. 97.61 Section 97.61 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Transfers § 97.61...

  14. 40 CFR 97.261 - EPA recordation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false EPA recordation. 97.261 Section 97.261 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.261...

  15. 40 CFR 97.261 - EPA recordation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false EPA recordation. 97.261 Section 97.261 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR SO2 Allowance Transfers § 97.261...

  16. 40 CFR 97.161 - EPA recordation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false EPA recordation. 97.161 Section 97.161 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR NOX Allowance Transfers § 97.161...

  17. 40 CFR 97.61 - EPA recordation.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 40 Protection of Environment 20 2010-07-01 2010-07-01 false EPA recordation. 97.61 Section 97.61 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Transfers § 97.61...

  18. 40 CFR 97.361 - EPA recordation.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 40 Protection of Environment 21 2011-07-01 2011-07-01 false EPA recordation. 97.361 Section 97.361 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... § 97.361 EPA recordation. (a) Within 5 business days (except as provided in paragraph (b) of...

  19. 40 CFR 97.61 - EPA recordation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 21 2014-07-01 2014-07-01 false EPA recordation. 97.61 Section 97.61 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS NOX Allowance Transfers § 97.61...

  20. 40 CFR 97.161 - EPA recordation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false EPA recordation. 97.161 Section 97.161 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX BUDGET TRADING PROGRAM AND CAIR NOX AND SO2 TRADING PROGRAMS CAIR NOX Allowance Transfers § 97.161...

  1. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    1997-10-01

    ... 48 Federal Acquisition Regulations System 5 1997-10-01 1997-10-01 false Title. 1352.217-97 Section... Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97 ) (Jan 1987) Unless title to materials and equipment acquired or produced for, or allocated...

  2. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    1998-10-01

    ... 48 Federal Acquisition Regulations System 5 1998-10-01 1998-10-01 false Title. 1352.217-97 Section... Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title to materials and equipment acquired or produced for, or allocated to,...

  3. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2007-10-01

    ... 48 Federal Acquisition Regulations System 5 2007-10-01 2007-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  4. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2009-10-01

    ... 48 Federal Acquisition Regulations System 5 2009-10-01 2009-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  5. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2001-10-01

    ... 48 Federal Acquisition Regulations System 5 2001-10-01 2001-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  6. 48 CFR 1352.217-97 - Title.

    Code of Federal Regulations, 2010 CFR

    2005-10-01

    ... 48 Federal Acquisition Regulations System 5 2005-10-01 2005-10-01 false Title. 1352.217-97 Section... SOLICITATION PROVISIONS AND CONTRACT CLAUSES Texts of Provisions and Clauses 1352.217-97 Title. As prescribed in 1317.7001(a), insert the following clause: Title (CAR 1352.217-97) (JAN 1987) Unless title...

  7. 14 CFR 97.1 - Applicability.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 14 Aeronautics and Space 2 2010-01-01 2010-01-01 false Applicability. 97.1 Section 97.1... AND GENERAL OPERATING RULES STANDARD INSTRUMENT PROCEDURES General § 97.1 Applicability. (a) This part prescribes standard instrument approach procedures to civil airports in the United States and the...

  8. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  9. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  10. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  11. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  12. 7 CFR 97.14 - Joint applicants.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Joint applicants. 97.14 Section 97.14 Agriculture... PLANT VARIETY AND PROTECTION The Application § 97.14 Joint applicants. (a) Joint owners shall file a joint application by signing as joint applicants. (b) If an application for certificate is made by...

  13. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  14. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  15. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  16. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  17. 47 CFR 97.111 - Authorized transmissions.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Authorized transmissions. 97.111 Section 97.111... SERVICE Station Operation Standards § 97.111 Authorized transmissions. (a) An amateur station may transmit the following types of two-way communications: (1) Transmissions necessary to exchange messages...

  18. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  19. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 1 2010-07-01 2010-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  20. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 32 National Defense 1 2012-07-01 2012-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  1. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 32 National Defense 1 2014-07-01 2014-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  2. 32 CFR 9.7 - Regulations.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Regulations. 9.7 Section 9.7 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE MILITARY COMMISSIONS PROCEDURES FOR TRIALS BY MILITARY COMMISSIONS OF CERTAIN NON-UNITED STATES CITIZENS IN THE WAR AGAINST TERRORISM § 9.7...

  3. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 1 2011-10-01 2011-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  4. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 1 2012-10-01 2012-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  5. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 42 Public Health 1 2010-10-01 2010-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  6. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 1 2014-10-01 2014-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  7. 42 CFR 9.7 - Reproduction.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 1 2013-10-01 2013-10-01 false Reproduction. 9.7 Section 9.7 Public Health PUBLIC HEALTH SERVICE, DEPARTMENT OF HEALTH AND HUMAN SERVICES GENERAL PROVISIONS STANDARDS OF CARE FOR CHIMPANZEES HELD IN THE FEDERALLY SUPPORTED SANCTUARY SYSTEM § 9.7 Reproduction. Chimpanzee reproduction...

  8. 47 CFR 97.109 - Station control.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Station control. 97.109 Section 97.109... SERVICE Station Operation Standards § 97.109 Station control. (a) Each amateur station must have at least one control point. (b) When a station is being locally controlled, the control operator must be at...

  9. 14 CFR 33.97 - Thrust reversers.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 14 Aeronautics and Space 1 2011-01-01 2011-01-01 false Thrust reversers. 33.97 Section 33.97 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Block Tests; Turbine Aircraft Engines § 33.97 Thrust reversers. (a) If...

  10. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 2 2012-10-01 2012-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING MARINE PORTABLE TANKS AND CARGO HANDLING SYSTEMS Cargo Handling System § 64.97 Cargo hose. Each hose assembly, consisting of couplings and a...

  11. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 2 2010-10-01 2010-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING MARINE PORTABLE TANKS AND CARGO HANDLING SYSTEMS Cargo Handling System § 64.97 Cargo hose. Each hose assembly, consisting of couplings and a...

  12. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 2 2014-10-01 2014-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING MARINE PORTABLE TANKS AND CARGO HANDLING SYSTEMS Cargo Handling System § 64.97 Cargo hose. Each hose assembly, consisting of couplings and a...

  13. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 2 2013-10-01 2013-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING MARINE PORTABLE TANKS AND CARGO HANDLING SYSTEMS Cargo Handling System § 64.97 Cargo hose. Each hose assembly, consisting of couplings and a...

  14. 46 CFR 64.97 - Cargo hose.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 2 2011-10-01 2011-10-01 false Cargo hose. 64.97 Section 64.97 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) MARINE ENGINEERING MARINE PORTABLE TANKS AND CARGO HANDLING SYSTEMS Cargo Handling System § 64.97 Cargo hose. Each hose assembly, consisting of couplings and a...

  15. 29 CFR 97.41 - Financial reporting.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 29 Labor 1 2010-07-01 2010-07-01 true Financial reporting. 97.41 Section 97.41 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Reports, Records Retention, and Enforcement § 97.41 Financial reporting. (a) General. (1) Except as provided in paragraphs (a)(2) and (5) of this section, grantees...

  16. 46 CFR 97.34-10 - Use.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Use. 97.34-10 Section 97.34-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Work Vests § 97.34-10 Use. (a) Approved buoyant work vests are considered to be items of safety apparel and may be...

  17. 32 CFR 552.97 - Communications.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 3 2011-07-01 2009-07-01 true Communications. 552.97 Section 552.97 National Defense Department of Defense (Continued) DEPARTMENT OF THE ARMY MILITARY RESERVATIONS AND NATIONAL CEMETERIES REGULATIONS AFFECTING MILITARY RESERVATIONS Fort Lewis Land Use Policy § 552.97...

  18. 12 CFR 313.97 - Financial hardship.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 12 Banks and Banking 4 2011-01-01 2011-01-01 false Financial hardship. 313.97 Section 313.97 Banks... CORPORATE DEBT COLLECTION Administrative Wage Garnishment § 313.97 Financial hardship. (a) A debtor whose..., divorce, or catastrophic illness which result in financial hardship. (b) A debtor requesting a...

  19. 12 CFR 313.97 - Financial hardship.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 12 Banks and Banking 5 2012-01-01 2012-01-01 false Financial hardship. 313.97 Section 313.97 Banks... CORPORATE DEBT COLLECTION Administrative Wage Garnishment § 313.97 Financial hardship. (a) A debtor whose..., divorce, or catastrophic illness which result in financial hardship. (b) A debtor requesting a...

  20. 29 CFR 97.41 - Financial reporting.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 1 2014-07-01 2013-07-01 true Financial reporting. 97.41 Section 97.41 Labor Office of the... LOCAL GOVERNMENTS Post-Award Requirements Reports, Records Retention, and Enforcement § 97.41 Financial... other forms as may from time to time be authorized by OMB, for: (i) Submitting financial reports...

  1. 12 CFR 313.97 - Financial hardship.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 12 Banks and Banking 5 2013-01-01 2013-01-01 false Financial hardship. 313.97 Section 313.97 Banks... CORPORATE DEBT COLLECTION Administrative Wage Garnishment § 313.97 Financial hardship. (a) A debtor whose..., divorce, or catastrophic illness which result in financial hardship. (b) A debtor requesting a...

  2. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 46 Shipping 4 2014-10-01 2014-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  3. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 46 Shipping 4 2012-10-01 2012-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  4. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 46 Shipping 4 2013-10-01 2013-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  5. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  6. 46 CFR 97.15-10 - Sanitation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 46 Shipping 4 2011-10-01 2011-10-01 false Sanitation. 97.15-10 Section 97.15-10 Shipping COAST GUARD, DEPARTMENT OF HOMELAND SECURITY (CONTINUED) CARGO AND MISCELLANEOUS VESSELS OPERATIONS Tests, Drills, and Inspections § 97.15-10 Sanitation. (a) It shall be the duty of the master and chief...

  7. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  8. 47 CFR 97.207 - Space station.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Space station. 97.207 Section 97.207... SERVICE Special Operations § 97.207 Space station. (a) Any amateur station may be a space station. A holder of any class operator license may be the control operator of a space station, subject to...

  9. 28 CFR 97.12 - Employee training.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 28 Judicial Administration 2 2010-07-01 2010-07-01 false Employee training. 97.12 Section 97.12... OR DETAINEE SERVICES § 97.12 Employee training. Private prisoner transport companies must require the completion of a minimum of 100 hours of employee training before an employee may transport violent...

  10. Separation of zirconium by thin-layer chromatography.

    PubMed

    Oguma, K

    1969-03-01

    The thin-layer Chromatographie separation of a number of metal ions [Sc, Y, Zr, La, Sm, Th, U(VI), etc.] with solvent mixtures of mesityl oxide, ethanol and 5M nitric acid on silica gel-cellulose (5:1) thin-layer plates is reported. Zirconium remains stationary whilst the other metal ions move with the solvent, thus allowing a selective separation of zirconium from about 20 metal ions in ratios ranging from 100:1 to 1:100. Mixtures of various metal ions can also be separated.

  11. In-situ stabilization of radioactive zirconium swarf

    SciTech Connect

    Hess, Clay C.

    1997-12-01

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes.

  12. Radiochemical separation of zirconium and hafnium from other radionuclides.

    PubMed

    Hahn, R B

    1972-11-01

    Radiozirconium and radiohafnium may be separated from all other radionuclides except scandium and protactinium by precipitation with mandelic acid from 5-10 M hydrochloric acid, using commercial zirconyl chloride as carrier. Scandium and protactinium are removed by dissolving the precipitate in sodium carbonate, then adding barium nitrate to precipitate barium carbonate which acts as a scavenger. Zirconium mandelate is finally reprecipitated and the sample weighed and counted in this form. The method was checked by analysing commercial zirconyl chloride and standard rock samples for zirconium and hafnium by neutron-activation analysis.

  13. Isotopic zirconium as a probe of AGB nucleosynthesis theory

    NASA Astrophysics Data System (ADS)

    Malaney, R. A.

    Nuclear reaction network calculations of the zirconium relative isotope abundances in AGB stars are presented. It is shown how these isotopic abundances depend on the AGB stellar mass and on the uncertain neutron absorption cross section for Zr-96. With regard to observations of the zirconium isotopes in S stars, it is shown how the many neutron exposure mechanisms associated with AGB thermal pulses cannot be operating in these stars. A less predictable scheme in which only a few neutron exposures take place appears to be more consistent with the reported S star observations.

  14. In-situ stabilization of radioactive zirconium swarf

    DOEpatents

    Hess, C.C.

    1999-08-31

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes. 6 figs.

  15. Oxidized Zirconium Bearing Surfaces in Total Knee Arthroplasty: Lessons Learned.

    PubMed

    Schüttler, Karl Friedrich; Efe, Turgay; Heyse, Thomas J; Haas, Steven B

    2015-10-01

    Polyethylene wear in total knee arthroplasty is a still unsolved problem resulting in osteolysis and long-term failure of knee joint replacement. To address the problem of polyethylene wear, research aimed for an optimal implant design and for an optimal combination of bearing surfaces. Oxidized zirconium was introduced to minimize surface wear and thus potentially increase long-term implant survival. This review comprises the current literature related to in vitro and in vivo studies evaluating performance of oxidized zirconium total knee arthroplasty and results from retrieval analyses.

  16. In-situ stabilization of radioactive zirconium swarf

    DOEpatents

    Hess, Clay C.

    1999-01-01

    The method for treating ignitable cutting swarf in accordance with the present invention involves collecting cutting swarf in a casting mold underwater and injecting a binder mixture comprising vinyl ester styrene into the vessel to fill void volume; and form a mixture comprising swarf and vinyl ester styrene; and curing the mixture. The method is especially useful for stabilizing the ignitable characteristics of radioactive zirconium cutting swarf, and can be used to solidify zirconium swarf, or other ignitable finely divided material, underwater. The process could also be performed out of water with other particulate wastes.

  17. Hydrogen pickup mechanism of zirconium alloys

    NASA Astrophysics Data System (ADS)

    Couet, Adrien

    Although the optimization of zirconium based alloys has led to significant improvements in hydrogen pickup and corrosion resistance, the mechanisms by which such alloy improvements occur are still not well understood. In an effort to understand such mechanisms, a systematic study of the alloy effect on hydrogen pickup is conducted, using advanced characterization techniques to rationalize precise measurements of hydrogen pickup. The hydrogen pick-up fraction is accurately measured for a specially designed set of commercial and model alloys to investigate the effects of alloying elements, microstructure and corrosion kinetics on hydrogen uptake. Two different techniques to measure hydrogen concentrations were used: a destructive technique, Vacuum Hot Extraction, and a non-destructive one, Cold Neutron Prompt Gamma Activation Analysis. The results indicate that hydrogen pickup varies not only from alloy to alloy but also during the corrosion process for a given alloy. For instance Zircaloy type alloys show high hydrogen pickup fraction and sub-parabolic oxidation kinetics whereas ZrNb alloys show lower hydrogen pickup fraction and close to parabolic oxidation kinetics. Hypothesis is made that hydrogen pickup result from the need to balance charge during the corrosion reaction, such that the pickup of hydrogen is directly related to (and indivisible of) the corrosion mechanism and decreases when the rate of electron transport or oxide electronic conductivity sigmao xe through the protective oxide increases. According to this hypothesis, alloying elements (either in solid solution or in precipitates) embedded in the oxide as well as space charge variations in the oxide would impact the hydrogen pick-up fraction by modifying sigmaox e, which drives oxidation and hydriding kinetics. Dedicated experiments and modelling were performed to assess and validate these hypotheses. In-situ electrochemical impedance spectroscopy (EIS) experiments were performed on Zircaloy-4 tubes

  18. Preliminary investigation of zirconium boride ceramals for gas-turbine blade applications

    NASA Technical Reports Server (NTRS)

    Hoffman, Charles A

    1953-01-01

    Zirconium boride ZrB2 ceramals were investigated for possible gas-turbine-blade application. Included in the study were thermal shock evaluations of disks, preliminary turbine-blade operation, and observations of oxidation resistance. Thermal shock disks of the following three compositions were studied: (a) 97.5 percent ZrB2 plus 2.5 percent B by weight; (b) 92.5 percent ZrB2 plus 7.5 percent B by weight; and (c) 100 percent ZrB2. Thermal shock disks were quenched from temperatures of 1800 degrees, 2000 degrees, 2200 degrees, and 2400 degrees F. The life of turbine blades containing 93 percent ZrB2 plus 7 percent B by weight was determined in gas-turbine tests. The blades were run at approximately 1600 degrees F and 15,000 to 26,000 rpm. The thermal shock resistance of the 97.5 percent ZrB2 plus 2.5 percent boron ceramals compares favorably with that of TiC plus Co and TiC plus Ni ceramals. Oxidation of the disks during the thermal shock evaluation was slight for the comparatively short time (8.3 hr) up through 2000 degrees F. Oxidation of a specimen was severe, however, after 100 hours at 2000 degrees F. The turbine blade performance evaluation of the 93 percent ZrB2 plus 7 percent B composition was preliminary in scope ; no conclusions can be drawn.

  19. Antimicrobial effects of silver zeolite, silver zirconium phosphate silicate and silver zirconium phosphate against oral microorganisms

    PubMed Central

    Saengmee-anupharb, Sirikamon; Srikhirin, Toemsak; Thaweboon, Boonyanit; Thaweboon, Sroisiri; Amornsakchai, Taweechai; Dechkunakorn, Surachai; Suddhasthira, Theeralaksna; Kamaguchi, Arihide

    2013-01-01

    Objective To evaluate the antimicrobial activities of silver inorganic materials, including silver zeolite (AgZ), silver zirconium phosphate silicate (AgZrPSi) and silver zirconium phosphate (AgZrP), against oral microorganisms. In line with this objective, the morphology and structure of each type of silver based powders were also investigated. Methods The antimicrobial activities of AgZ, AgZrPSi and AgZrP were tested against Streptococcus mutans, Lactobacillus casei, Candida albicans and Staphylococcus aureus using disk diffusion assay as a screening test. The minimum inhibitory concentration (MIC) and minimum lethal concentration (MLC) were determined using the modified membrane method. Scanning electron microscope and X-ray diffraction were used to investigate the morphology and structure of these silver materials. Results All forms of silver inorganic materials could inhibit the growth of all test microorganisms. The MIC of AgZ, AgZrPSi and AgZrP was 10.0 g/L whereas MLC ranged between 10.0–60.0 g/L. In terms of morphology and structure, AgZrPSi and AgZrP had smaller sized particles (1.5–3.0 µm) and more uniformly shaped than AgZ. Conclusions Silver inorganic materials in the form of AgZ, AgZrPSi and AgZrP had antimicrobial effects against all test oral microorganisms and those activities may be influenced by the crystal structure of carriers. These results suggest that these silver materials may be useful metals applied to oral hygiene products to provide antimicrobial activity against oral infection. PMID:23570016

  20. Mineral resource of the month: zirconium and hafnium

    USGS Publications Warehouse

    Gambogi, Joseph

    2007-01-01

    Zirconium and hafnium are corrosion-resistant metals that are grouped in the same family as titanium on the periodic table. The two elements commonly occur in oxide and silicate minerals and have significant economic importance in everything from ink, ceramics and golf shoes to nuclear fuel rods.

  1. Bronchopulmonary Cellular Response to Aluminum and Zirconium Salts

    PubMed Central

    Stankus, Richard P.; Schuyler, Mark R.; D'Amato, Robert A.; Salvaggio, John E.

    1978-01-01

    The bronchopulmonary cellular immunological response to repeated intratracheal inoculation of aluminum chlorhydrate, sodium zirconium lactate, and zirconium aluminum glycine was examined in rabbits. Results of a dose-response experiment using 0.1, 1.0, and 10.0-mg intratracheal inoculations of each metallic salt demonstrated significant bronchopulmonary histopathology in the 10.0-mg dose-response groups only. Acute lesions were histologically characterized by an inflammatory response centered around respiratory bronchioles. Although epithelioid cell formation was evident in 10.0 mg of aluminum salt (aluminum chlorhydrate and zirconium aluminum glycine) -injected animals, no well-defined granulomas characterized by an orderly arrangement of epithelioid cells, lymphocytes, and giant cells were evident in any of the experimental groups employed. All three metallic salts induced “activated” bronchopulmonary macrophages as determined by an in vitro phagocytic assay. This activation was likely nonimmunological since no measurable differences were observed in metallic salt-induced delayed skin reactivity or migration inhibition factor production between inoculated and uninoculated rabbits. The above observations suggest that aluminum and zirconium salts administered in comparatively high dosage via the respiratory tract route can induce respiratory bronchiolitis and activation of alveolar macrophages in the absence of demonstrable delayed hypersensitivity. Images PMID:352963

  2. Mechanistic Elucidation of Zirconium-Catalyzed Direct Amidation.

    PubMed

    Lundberg, Helena; Tinnis, Fredrik; Zhang, Jiji; Algarra, Andrés G; Himo, Fahmi; Adolfsson, Hans

    2017-02-15

    The mechanism of the zirconium-catalyzed condensation of carboxylic acids and amines for direct formation of amides was studied using kinetics, NMR spectroscopy, and DFT calculations. The reaction is found to be first order with respect to the catalyst and has a positive rate dependence on amine concentration. A negative rate dependence on carboxylic acid concentration is observed along with S-shaped kinetic profiles under certain conditions, which is consistent with the formation of reversible off-cycle species. Kinetic experiments using reaction progress kinetic analysis protocols demonstrate that inhibition of the catalyst by the amide product can be avoided using a high amine concentration. These insights led to the design of a reaction protocol with improved yields and a decrease in catalyst loading. NMR spectroscopy provides important details of the nature of the zirconium catalyst and serves as the starting point for a theoretical study of the catalytic cycle using DFT calculations. These studies indicate that a dinuclear zirconium species can catalyze the reaction with feasible energy barriers. The amine is proposed to perform a nucleophilic attack at a terminal η(2)-carboxylate ligand of the zirconium catalyst, followed by a C-O bond cleavage step, with an intermediate proton transfer from nitrogen to oxygen facilitated by an additional equivalent of amine. In addition, the DFT calculations reproduce experimentally observed effects on reaction rate, induced by electronically different substituents on the carboxylic acid.

  3. Electrochemical Deoxidation of Solid Zirconium Dioxide in Molten Calcium Chloride

    NASA Astrophysics Data System (ADS)

    Mohandas, K. S.; Fray, D. J.

    2009-10-01

    The reduction of zirconium dioxide pellets by electro-deoxidation in molten calcium chloride-calcium oxide (900 °C) has been studied. In this technique, the solid oxide is cathodically polarized against a graphite counter electrode under a constant applied potential. Unlike other metal oxides that have been reduced by this technique, only a small area around the cathodic current-collector wire was reduced to zirconium metal with zirconia pellets sintered at ~1100 °C; the rest of the sample was largely calcium zirconate. Pellets sintered above 1200 °C showed better reduction near the cathode wire and the reduction extended to the entire surface of the pellet with the passage of time. However, reduction of the inner core was found to be increasingly difficult, because the surface metal layer thickened on continuous electro-deoxidation. An analysis of the experimental results showed that the poor electrical conductivity of the intermediate compound, CaZrO3 and its blocky morphology inhibited the electro-deoxidation process. The increase in the sintering temperature of the pellet made it better conducting. However, the pores formed in the thick zirconium metal layer in such samples were too small for an ideal contact between the inner core and the molten electrolyte and hence the reduction of the inner core remained incomplete. Within the scope of this study, it is concluded that preforms with good grain growth and porosity are necessary for the electro-deoxidation of solid zirconium oxide.

  4. Phosphorus Recovery Using Zirconium-Loaded Saponified Orange Juice Residue

    NASA Astrophysics Data System (ADS)

    Harada, Hiroyuki; Kondo, Mitsunori; Biswas, Biplob K.; Ohura, Seichirou; Inoue, Katsutoshi; Ishikawa, Susumu; Kawakita, Hidetaka; Ohto, Keisuke

    Zirconium was immobilized to orange juice residue, to investigate the feasibility of using zirconium-loaded saponified orange juice residue (Zr-SOJR) for phosphorus recovery from secondary effluent and the extraction solution from incinerated sewage sludge ash by using H2SO4 and HCl. These had phosphorus concentrations of 68.2 mg/dm3 and 5.9 mg/dm3, respectively. The phosphorus removal rate secondary effluent increased with an increasing solid/liquid ratio in batch experiments. The adsorption capacity of Zr-SOJR was also compared with those obtained using a synthetic phosphorus solution and using zirconium-loaded ferrite. The prepared absorbent was effective for phosphorus removal and exhibited a reasonably high sorption capacity, twice that of zirconium ferrite. Secondary effluent was treated by packed column, and this reached break-through after 300 bed volumes. The results from phosphorous extraction from the ash indicate that can be treated with acid to efficiently recover phosphorous and thus can be absorbed by Zr-SOJR.

  5. Uranyl tungstate and zirconium tungstate in salt melts

    SciTech Connect

    Kryukova, A.I.; Bragina, R.A.; Kazantsev, G.N.; Korshunov, I.A.

    1988-05-01

    The article discusses the preparation, properties, and behavior of uranyl tungstate and zirconium tungstate in salt melts. Procedures for their preparation are presented. The radiographic and IR spectroscopic characteristics, the thermal stability, and solubility and stability in chloride-tungstate melts of different composition have been studied.

  6. On The Creep Behavior Of Niobium-Modified Zirconium Alloys

    SciTech Connect

    Charit, I.; Murty, K.L.

    2006-07-01

    Zr alloys remain the main cladding materials in most water reactors. Historically, a series of Zircaloys were developed, and two versions, Zircaloy-2 and -4, are still employed in many reactors. The recent trend is to use the Nb-modified zirconium alloys where it has been shown that Nb addition improves cladding performance in various ways, most significant being superior long-term corrosion resistance. Hence, new alloys with Nb additions have recently been developed, such as Zirlo{sup TM(i)} and M5TM{sup (ii)}. Although it is known that creep properties improve, there have been very few data available to precisely evaluate the creep characteristics of new commercial alloys. However, the creep behavior of many Nb-modified zirconium alloys has been studied in several occasions. In this study, we have collected the creep data of these Nb-modified alloys from the open literature as well as our own study over a wide range of stresses and temperatures. The data have been compared with those of conventional Zr and Zircaloys to determine the exact role Nb plays. It has been argued that Nb-modified zirconium alloys would behave as a Class-A alloy (stress exponent of 3) with the Nb atoms forming solute atmospheres around dislocations and thus, impeding dislocation glide under suitable conditions. On the other hand, zirconium and Zircaloys behave as Class-M alloys with a stress exponent of {>=} 4, attesting to the dislocation climb-controlled deformation mode. (authors)

  7. Studies on the Characteristic of Zirconium-Tritium Reaction

    NASA Astrophysics Data System (ADS)

    Huang, Gang; Long, Xing-Gui; Peng, Shu-Ming; Liang, Jian-Hua; Yang, Ben-Fu

    2011-02-01

    The p- c-T curves of tritium absorption and desorption of zirconium were measured using the method of step equilibrium by stepping up the tritium quantity on an experimental apparatus of metal hydride. The p- c-T curves for tritium have one plateau at temperature range from 450 to 500°C and two plateaus at temperature above 600°C. The thermodynamic parameters of the different phases were determined according to the van't Hoff equation. The hysteresis effect was observed in reversible process of tritium absorption and desorption of zirconium on our experimental condition. The tritium absorption behavior by zirconium in the temperature range from 450 to 620°C and desorption behavior of zirconium in the temperature range from 775 to 875°C have been investigated. A method of the reaction rate analysis was proposed and examined for determining the rate constant. The apparent activation energy obtained by this analysis for the absorption and the desorption were (-16.8 ± 0.8) kJ·mol-1 and (57.7 ± 1.6) kJ·mol-1, respectively.

  8. Manufacturing process to reduce large grain growth in zirconium alloys

    DOEpatents

    Rosecrans, Peter M.

    1987-01-01

    A method of treating cold-worked zirconium alloys to reduce large grain gth during thermal treatment at temperatures above the recrystallization temperature of the alloy comprising heating the cold-worked alloy between about 1300.degree.-1350.degree. F. for 1 to 3 hours prior to treatment above its recrystallization temperature.

  9. Method for calcining nuclear waste solutions containing zirconium and halides

    DOEpatents

    Newby, Billie J.

    1979-01-01

    A reduction in the quantity of gelatinous solids which are formed in aqueous zirconium-fluoride nuclear reprocessing waste solutions by calcium nitrate added to suppress halide volatility during calcination of the solution while further suppressing chloride volatility is achieved by increasing the aluminum to fluoride mole ratio in the waste solution prior to adding the calcium nitrate.

  10. Nanophase Nickel-Zirconium Alloys for Fuel Cells

    NASA Technical Reports Server (NTRS)

    Narayanan, Sekharipuram; Whitacre, jay; Valdez, Thomas

    2008-01-01

    Nanophase nickel-zirconium alloys have been investigated for use as electrically conductive coatings and catalyst supports in fuel cells. Heretofore, noble metals have been used because they resist corrosion in the harsh, acidic fuel cell interior environments. However, the high cost of noble metals has prompted a search for less-costly substitutes. Nickel-zirconium alloys belong to a class of base metal alloys formed from transition elements of widely different d-electron configurations. These alloys generally exhibit unique physical, chemical, and metallurgical properties that can include corrosion resistance. Inasmuch as corrosion is accelerated by free-energy differences between bulk material and grain boundaries, it was conjectured that amorphous (glassy) and nanophase forms of these alloys could offer the desired corrosion resistance. For experiments to test the conjecture, thin alloy films containing various proportions of nickel and zirconium were deposited by magnetron and radiofrequency co-sputtering of nickel and zirconium. The results of x-ray diffraction studies of the deposited films suggested that the films had a nanophase and nearly amorphous character.

  11. Surface modification of layered zirconium phosphate with PNIPAM.

    PubMed

    Wang, Xuezhen; Zhao, Di; Medina, Ilse B Nava; Diaz, Agustin; Wang, Huiliang; Clearfield, Abraham; Mannan, M Sam; Cheng, Zhengdong

    2016-04-04

    A new method was reported to modify layered zirconium phosphate (ZrP) with thermoresponsive polymer PNIPAM (poly N-isopropylacrylamide). PNIPAM was proved to be covalently grafted onto ZrP. (60)Co γ-rays irradiation produced peroxide groups on the surface which, upon heating, initiated free radical polymerization and subsequent attachment of PNIPAM.

  12. 46 CFR 97.12-5 - Manual.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 46 Shipping 4 2010-10-01 2010-10-01 false Manual. 97.12-5 Section 97.12-5 Shipping COAST GUARD...-5 Manual. The manual on the “Stowage of Bulk Cargoes Such as Ore, Ore Concentrates, and Similar... compliance with the requirements of § 97.12-1(a). 1 Copies of this manual are on file at Coast...

  13. Layered zirconium phosphonate with inorganic–organic hybrid structure: Preparation and its assembly with DNA

    SciTech Connect

    Liu, Li-Min; Lu, Guo-Yuan; Jiang, Li-Ping; Zhu, Jun-Jie

    2014-07-01

    An aminoethoxy-functionalized zirconium phosphonate (Zr(O{sub 3}POCH{sub 2}CH{sub 2}NH{sub 2}){sub 2}·3H{sub 2}O), abbreviated as ZrRP (R=OCH{sub 2}CH{sub 2}NH{sub 2}), with layered structure has been synthesized. This layered compound possesses the characteristic of inorganic–organic hybrid, due to the covalently linked aminoethoxy in the host layer. The anion exchanged property of this zirconium phosphonate is suitable for the direct intercalation of negatively charged DNA, which is different from these reported zirconium phosphates or zirconium phosphonates. As a precursor, this prepared zirconium phosphonate was utilized to fabricate a novel DNA/ZrRP binary hybrid via a delamination-reassembly procedure. The release behavior of DNA from the DNA/ZrRP composite was investigated at different medium pH, because the combination between zirconium phosphonate sheets and DNA was pH-dependent sensitively. Moreover, the helical conformation of DNA was almost retained after the intercalation and release process. These properties of the DNA/ZrRP composite suggested the potential application of layered zirconium phosphonate as a non-viral vector in gene delivery. - Graphical abstract: The intercalation of DNA into zirconium phosphonate and the release of DNA from the interlayer of zirconium phosphonate. - Highlights: ●A layered aminoethoxy-functionalized zirconium phosphonate has been synthesized. ●DNA was intercalated directly into the prepared zirconium phosphonate. ●A novel zirconium phosphonate/DNA binary hybrid was fabricated. ●DNA can be reversibly released from the interlayer of zirconium phosphonate. ●The intercalation/release processes do not induce the denaturalization of DNA.

  14. 50 CFR 17.97 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ..., TRANSPORTATION, SALE, PURCHASE, BARTER, EXPORTATION, AND IMPORTATION OF WILDLIFE AND PLANTS (CONTINUED) ENDANGERED AND THREATENED WILDLIFE AND PLANTS (CONTINUED) Interagency Cooperation (Continued) § 17.97...

  15. Syntheses and structural characterization of zirconium-tin and zirconium-lead binary and ternary systems

    SciTech Connect

    Kwon, Y.U.

    1991-01-28

    The binary zirconium-tin system was reinvestigated. The A15 phase appears to be a line phase with a Zr{sub 4}Sn composition. The Zr{sub 5}Sn{sub 3} (Mn{sub 5}Si{sub 3}-type) and Zr{sub 5}Sn{sub 4} (Ti{sub 5}Ga{sub 4}-type) compounds are line phases below 1000{degree}C, the latter being a self-interstitial phase of the former. ZrSn{sub 2} is the tin-richest phase. There is an one-phase region between these phases with partial self-interstitials at high temperatures. The zirconium-lead system behaves similarly: there are an A15 phase with a Zr{sub {approximately}5.8}Pb composition, Zr{sub 5}Pb{sub 3} (Mn{sub 5}Si{sub 3}-type) and Zr{sub 5}Pb{sub 4} (Ti{sub 5}Ga{sub 4-type}) compounds, and a high temperature solid solution between Zr{sub 5}Pb{sub >3.5} and Zr{sub 5}Pb{sub 4} from below 1000{degree}C; however, the ZrSn{sub 2} analogue is not formed. The Mn{sub 5}Si{sub 3}-type phases in these systems can accommodate third elements interstitially to form stoichiometric compounds Zr{sub 5}Sn{sub 3}Z (Z = B, C, N, O, Al, Si, P, S, Cu, Zn, Ga, Ge, and As and Se) and Zr{sub 5}Pb{sub 3}Z (Z = Al, Si, P, S, Fe, Co, Ni, Cu, Zn, Ga, Ge, As, Se, Ag, Cd, In, Sn, Sb and Te) as well as their self-interstitial derivatives. The systems Zr-Sn-T, T = Fe, Co and Ni, did not produce stoichiometric interstitial phases Zr{sub 5}Sn{sub 3}T. Instead, the interstitial phases for these elements are formed only with excess tin that partially occupies the interstitial site together with a T element. Reducing the amount of tin in these systems yields two new phases; Zr{sub 5}Sn{sub 2+x}Fe{sub 1-x} (0 {le} {times} {le} 0.28) (W{sub 5}Si{sub 3}-type) and Zr{sub 6}Sn{sub 2}Fe (Zr{sub 6}Al{sub 2}Co-type) as characterized by X-ray single crystal analyses. A cobalt analogue for the latter was also synthesized.

  16. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 29 Labor 5 2014-07-01 2014-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor... radiation. (a) Electromagnetic radiation—(1) Definitions applicable to this paragraph. (i) The term electromagnetic radiation is restricted to that portion of the spectrum commonly defined as the radio...

  17. 29 CFR 1910.97 - Nonionizing radiation.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 5 2012-07-01 2012-07-01 false Nonionizing radiation. 1910.97 Section 1910.97 Labor... radiation. (a) Electromagnetic radiation—(1) Definitions applicable to this paragraph. (i) The term electromagnetic radiation is restricted to that portion of the spectrum commonly defined as the radio...

  18. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 47 Telecommunication 5 2012-10-01 2012-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  19. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 47 Telecommunication 5 2013-10-01 2013-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  20. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 47 Telecommunication 5 2014-10-01 2014-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  1. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 47 Telecommunication 5 2011-10-01 2011-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  2. 47 CFR 97.23 - Mailing address.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 47 Telecommunication 5 2010-10-01 2010-10-01 false Mailing address. 97.23 Section 97.23 Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO... name and mailing address. The mailing address must be in an area where the amateur service is...

  3. 7 CFR 97.8 - Specimen requirements.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Specimen requirements. 97.8 Section 97.8 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS PLANT VARIETY AND PROTECTION...

  4. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 14 Aeronautics and Space 2 2010-01-01 2010-01-01 false Aeronautical knowledge. 61.97 Section 61.97 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION (CONTINUED) AIRMEN... ground training from an authorized instructor or complete a home-study course on the...

  5. 14 CFR 61.97 - Aeronautical knowledge.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 14 Aeronautics and Space 2 2014-01-01 2014-01-01 false Aeronautical knowledge. 61.97 Section 61.97 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION (CONTINUED) AIRMEN... ground training from an authorized instructor or complete a home-study course on the...

  6. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2010-10-01 2010-10-01 false Station identification. 97.119 Section...

  7. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2012-10-01 2012-10-01 false Station identification. 97.119 Section...

  8. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2014-10-01 2014-10-01 false Station identification. 97.119 Section...

  9. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2011-10-01 2011-10-01 false Station identification. 97.119 Section...

  10. 47 CFR 97.119 - Station identification.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... SERVICE Station Operation Standards § 97.119 Station identification. (a) Each amateur station, except a space station or telecommand station, must transmit its assigned call sign on its transmitting channel... 47 Telecommunication 5 2013-10-01 2013-10-01 false Station identification. 97.119 Section...

  11. 40 CFR 97.401 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.401 Section 97.401 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Purpose. This subpart sets forth the general, designated representative, allowance, and...

  12. 40 CFR 97.501 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.501 Section 97.501 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Purpose. This subpart sets forth the general, designated representative, allowance, and...

  13. 40 CFR 97.701 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.701 Section 97.701 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Purpose. This subpart sets forth the general, designated representative, allowance, and...

  14. 40 CFR 97.601 - Purpose.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 40 Protection of Environment 22 2013-07-01 2013-07-01 false Purpose. 97.601 Section 97.601 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL NOX... Purpose. This subpart sets forth the general, designated representative, allowance, and...

  15. 9 CFR 201.97 - Annual reports.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 9 Animals and Animal Products 2 2012-01-01 2012-01-01 false Annual reports. 201.97 Section 201.97 Animals and Animal Products GRAIN INSPECTION, PACKERS AND STOCKYARDS ADMINISTRATION (PACKERS AND... (except a packer buyer registered to purchase livestock for slaughter only) shall file annually with...

  16. 9 CFR 201.97 - Annual reports.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 9 Animals and Animal Products 2 2014-01-01 2014-01-01 false Annual reports. 201.97 Section 201.97 Animals and Animal Products GRAIN INSPECTION, PACKERS AND STOCKYARDS ADMINISTRATION (PACKERS AND... (except a packer buyer registered to purchase livestock for slaughter only) shall file annually with...

  17. 9 CFR 201.97 - Annual reports.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 9 Animals and Animal Products 2 2011-01-01 2011-01-01 false Annual reports. 201.97 Section 201.97 Animals and Animal Products GRAIN INSPECTION, PACKERS AND STOCKYARDS ADMINISTRATION (PACKERS AND... (except a packer buyer registered to purchase livestock for slaughter only) shall file annually with...

  18. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2011-04-01 2011-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  19. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2012-04-01 2012-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  20. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false Benzene. 21.97 Section 21... TREASURY LIQUORS FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  1. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2013-04-01 2013-04-01 false Benzene. 21.97 Section 21... TREASURY ALCOHOL FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  2. 27 CFR 21.97 - Benzene.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2014-04-01 2014-04-01 false Benzene. 21.97 Section 21... TREASURY ALCOHOL FORMULAS FOR DENATURED ALCOHOL AND RUM Specifications for Denaturants § 21.97 Benzene. (a..., Standard No. D 836-77; for incorporation by reference, see § 21.6(b).) When 100 ml of benzene are...

  3. 29 CFR 97.3 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 1 2012-07-01 2012-07-01 false Definitions. 97.3 Section 97.3 Labor Office of the Secretary of Labor UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND COOPERATIVE AGREEMENTS TO STATE AND... and Indian housing agency under the United States Housing Act of 1937) school district,...

  4. 29 CFR 97.3 - Definitions.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Definitions. 97.3 Section 97.3 Labor Office of the Secretary of Labor UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND COOPERATIVE AGREEMENTS TO STATE AND... and Indian housing agency under the United States Housing Act of 1937) school district,...

  5. 29 CFR 97.3 - Definitions.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 29 Labor 1 2013-07-01 2013-07-01 false Definitions. 97.3 Section 97.3 Labor Office of the Secretary of Labor UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND COOPERATIVE AGREEMENTS TO STATE AND... and Indian housing agency under the United States Housing Act of 1937) school district,...

  6. 7 CFR 97.178 - Refunds.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 3 2010-01-01 2010-01-01 false Refunds. 97.178 Section 97.178 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS...

  7. 7 CFR 97.178 - Refunds.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ... 7 Agriculture 3 2011-01-01 2011-01-01 false Refunds. 97.178 Section 97.178 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS...

  8. 7 CFR 97.178 - Refunds.

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 7 Agriculture 3 2014-01-01 2014-01-01 false Refunds. 97.178 Section 97.178 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS...

  9. 7 CFR 97.178 - Refunds.

    Code of Federal Regulations, 2012 CFR

    2012-01-01

    ... 7 Agriculture 3 2012-01-01 2012-01-01 false Refunds. 97.178 Section 97.178 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS...

  10. 7 CFR 97.178 - Refunds.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 7 Agriculture 3 2013-01-01 2013-01-01 false Refunds. 97.178 Section 97.178 Agriculture Regulations of the Department of Agriculture (Continued) AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS...

  11. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 36 Parks, Forests, and Public Property 1 2012-07-01 2012-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  12. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 36 Parks, Forests, and Public Property 1 2014-07-01 2014-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  13. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 36 Parks, Forests, and Public Property 1 2010-07-01 2010-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  14. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 36 Parks, Forests, and Public Property 1 2011-07-01 2011-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  15. 36 CFR 9.7 - Assessment work.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 36 Parks, Forests, and Public Property 1 2013-07-01 2013-07-01 false Assessment work. 9.7 Section 9.7 Parks, Forests, and Public Property NATIONAL PARK SERVICE, DEPARTMENT OF THE INTERIOR MINERALS..., 1976. The Secretary expressly reserves, however, the existing right to contest claims for failure to...

  16. 32 CFR 97.5 - Responsibilities.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 32 National Defense 1 2011-07-01 2011-07-01 false Responsibilities. 97.5 Section 97.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN RELEASE... Responsibilities. (a) The General Counsel, Department of Defense, shall provide general policy and...

  17. 32 CFR 97.5 - Responsibilities.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 32 National Defense 1 2013-07-01 2013-07-01 false Responsibilities. 97.5 Section 97.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN RELEASE... Responsibilities. (a) The General Counsel, Department of Defense, shall provide general policy and...

  18. 40 CFR 97.301 - Purpose.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... provisions and the designated representative, permitting, allowance, monitoring, and opt-in provisions for... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Purpose. 97.301 Section 97.301 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  19. 40 CFR 97.101 - Purpose.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... designated representative, permitting, allowance, monitoring, and opt-in provisions for the Federal Clean Air... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Purpose. 97.101 Section 97.101 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  20. 40 CFR 97.1 - Purpose.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ..., allowance, excess emissions, monitoring, and opt-in provisions for the federal NOX Budget Trading Program... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Purpose. 97.1 Section 97.1 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  1. 40 CFR 97.1 - Purpose.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ..., allowance, excess emissions, monitoring, and opt-in provisions for the federal NOX Budget Trading Program... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Purpose. 97.1 Section 97.1 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  2. 40 CFR 97.101 - Purpose.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... designated representative, permitting, allowance, monitoring, and opt-in provisions for the Federal Clean Air... 40 Protection of Environment 21 2011-07-01 2011-07-01 false Purpose. 97.101 Section 97.101 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  3. 40 CFR 97.301 - Purpose.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... provisions and the designated representative, permitting, allowance, monitoring, and opt-in provisions for... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Purpose. 97.301 Section 97.301 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR PROGRAMS (CONTINUED) FEDERAL...

  4. 34 CFR 97.107 - IRB membership.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 34 Education 1 2013-07-01 2013-07-01 false IRB membership. 97.107 Section 97.107 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the... membership. (a) Each IRB shall have at least five members, with varying backgrounds to promote complete...

  5. 34 CFR 97.107 - IRB membership.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 34 Education 1 2014-07-01 2014-07-01 false IRB membership. 97.107 Section 97.107 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the... membership. (a) Each IRB shall have at least five members, with varying backgrounds to promote complete...

  6. 34 CFR 97.107 - IRB membership.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 34 Education 1 2010-07-01 2010-07-01 false IRB membership. 97.107 Section 97.107 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the... membership. (a) Each IRB shall have at least five members, with varying backgrounds to promote complete...

  7. 34 CFR 97.107 - IRB membership.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 34 Education 1 2011-07-01 2011-07-01 false IRB membership. 97.107 Section 97.107 Education Office of the Secretary, Department of Education PROTECTION OF HUMAN SUBJECTS Federal Policy for the... membership. (a) Each IRB shall have at least five members, with varying backgrounds to promote complete...

  8. 32 CFR 97.5 - Responsibilities.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 32 National Defense 1 2010-07-01 2010-07-01 false Responsibilities. 97.5 Section 97.5 National Defense Department of Defense OFFICE OF THE SECRETARY OF DEFENSE PERSONNEL, MILITARY AND CIVILIAN RELEASE... Responsibilities. (a) The General Counsel, Department of Defense, shall provide general policy and...

  9. 49 CFR 230.97 - Crank pins.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 49 Transportation 4 2014-10-01 2014-10-01 false Crank pins. 230.97 Section 230.97 Transportation Other Regulations Relating to Transportation (Continued) FEDERAL RAILROAD ADMINISTRATION, DEPARTMENT OF TRANSPORTATION STEAM LOCOMOTIVE INSPECTION AND MAINTENANCE STANDARDS Steam Locomotives and Tenders Driving...

  10. 14 CFR 97.20 - General.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 14 Aeronautics and Space 2 2010-01-01 2010-01-01 false General. 97.20 Section 97.20 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION (CONTINUED) AIR TRAFFIC AND...). For information on the availability of this material at NARA, call 202-741-6030, or go to...

  11. 27 CFR 6.97 - [Reserved

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... 27 Alcohol, Tobacco Products and Firearms 1 2010-04-01 2010-04-01 false 6.97 Section 6.97 Alcohol, Tobacco Products and Firearms ALCOHOL AND TOBACCO TAX AND TRADE BUREAU, DEPARTMENT OF THE TREASURY LIQUORS âTIED-HOUSEâ Exceptions §...

  12. 29 CFR 97.43 - Enforcement.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 29 Labor 1 2011-07-01 2011-07-01 false Enforcement. 97.43 Section 97.43 Labor Office of the Secretary of Labor UNIFORM ADMINISTRATIVE REQUIREMENTS FOR GRANTS AND COOPERATIVE AGREEMENTS TO STATE AND LOCAL GOVERNMENTS Post-Award Requirements Reports, Records Retention, and Enforcement §...

  13. 29 CFR 97.41 - Financial reporting.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 29 Labor 1 2012-07-01 2012-07-01 false Financial reporting. 97.41 Section 97.41 Labor Office of... Financial reporting. (a) General. (1) Except as provided in paragraphs (a)(2) and (5) of this section... supplementary or other forms as may from time to time be authorized by OMB, for: (i) Submitting...

  14. 34 CFR 97.402 - Definitions.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... Children Who Are Subjects in Research § 97.402 Definitions. The definitions in § 97.102 apply to this... have not attained the legal age for consent to treatments or procedures involved in the research, under the applicable law of the jurisdiction in which the research will be conducted. (b) Assent means...

  15. Nuclear-grade zirconium prepared by combining combustion synthesis with molten-salt electrorefining technique

    NASA Astrophysics Data System (ADS)

    Li, Hui; Nersisyan, Hayk H.; Park, Kyung-Tae; Park, Sung-Bin; Kim, Jeong-Guk; Lee, Jeong-Min; Lee, Jong-Hyeon

    2011-06-01

    Zirconium has a low absorption cross-section for neutrons, which makes it an ideal material for use in nuclear reactor applications. However, hafnium typically contained in zirconium causes it to be far less useful for nuclear reactor materials because of its high neutron-absorbing properties. In the present study, a novel effective method has been developed for the production of hafnium-free zirconium. The process includes two main stages: magnesio-thermic reduction of ZrSiO 4 under a combustion mode, to produce zirconium silicide (ZrSi), and recovery of hafnium-free zirconium by molten-salt electrorefining. It was found that, depending on the electrorefining procedure, it is possible to produce zirconium powder with a low hafnium content: 70 ppm, determined by ICP-AES analysis.

  16. Hydrogen content in titanium and a titanium-zirconium alloy after acid etching.

    PubMed

    Frank, Matthias J; Walter, Martin S; Lyngstadaas, S Petter; Wintermantel, Erich; Haugen, Håvard J

    2013-04-01

    Dental implant alloys made from titanium and zirconium are known for their high mechanical strength, fracture toughness and corrosion resistance in comparison with commercially pure titanium. The aim of the study was to investigate possible differences in the surface chemistry and/or surface topography of titanium and titanium-zirconium surfaces after sand blasting and acid etching. The two surfaces were compared by X-ray photoelectron spectroscopy, secondary ion mass spectroscopy, scanning electron microscopy and profilometry. The 1.9 times greater surface hydrogen concentration of titanium zirconium compared to titanium was found to be the major difference between the two materials. Zirconium appeared to enhance hydride formation on titanium alloys when etched in acid. Surface topography revealed significant differences on the micro and nanoscale. Surface roughness was increased significantly (p<0.01) on the titanium-zirconium alloy. High-resolution images showed nanostructures only present on titanium zirconium.

  17. Experiments on interactions between zirconium-containing melt and water (ZREX): Hydrogen generation and chemical augmentation of energetics

    SciTech Connect

    Cho, D.H.; Armstrong, D.R.; Gunther, W.H.; Basu, S.

    1997-08-01

    The results of the first data series of experiments on interactions between zirconium-containing melt and water are described. These experiments involved dropping 1-kg batches of pure zirconium or zirconium-zirconium dioxide mixture melt into a column of water. A total of nine tests were conducted, including four with pure zirconium melt and five with Zr-ZrO{sub 2} mixture melt. Explosions took place only in those tests which were externally triggered. While the extent of zirconium oxidation in the triggered experiments was quite extensive, the estimated explosion energetics were found to be very small compared to the combined thermal and chemical energy available.

  18. The effect of zirconium on the cyclic oxidation of NiCrAl alloys

    NASA Technical Reports Server (NTRS)

    Barrett, C. A.; Khan, A. S.; Lowell, C. E.

    1981-01-01

    This paper examines results with cyclic oxidation tests of Ni(9-20) Cr(15-30) Al-(x)Zr alloys carried out at 1100 C and 1200 C in static air. The concentration of zirconium varies from 0 to 0.63 atomic percent. Significant aluminum penetration is found in metallographic and electron microscopic examination of oxidized surfaces. Small amounts of zirconium lead to minimal penetration, and with increased zirconium content pronounced oxide penetration is observed.

  19. Corrosion behavior of stainless steel-zirconium alloy waste forms.

    SciTech Connect

    Abraham, D. P.

    1999-01-13

    Stainless steel-zirconium (SS-Zr) alloys are being considered as waste forms for the disposal of metallic waste generated during the electrometallurgical treatment of spent nuclear fuel. The baseline waste form for spent fuels from the EBR-II reactor is a stainless steel-15 wt.% zirconium (SS-15Zr) alloy. This article briefly reviews the microstructure of various SS-Zr waste form alloys and presents results of immersion corrosion and electrochemical corrosion tests performed on these alloys. The electrochemical tests show that the corrosion behavior of SS-Zr alloys is comparable to those of other alloys being considered for the Yucca Mountain geologic repository. The immersion tests demonstrate that the SS-Zr alloys are resistant to selective leaching of fission product elements and, hence, suitable as candidates for high-level nuclear waste forms.

  20. Corrosion testing of stainless steel-zirconium metal waste form.

    SciTech Connect

    Abraham, D. P.

    1998-12-14

    Stainless steel-zirconium (SS-Zr) alloys are being considered as waste forms for the disposition of metallic waste generated during the electrometallurgical treatment of spent nuclear fuel. The waste forms contain irradiated cladding hulls, components of the alloy fuel, noble metal fission products, and actinide elements. The baseline waste form is a stainless steel-15 wt% zirconium (SS-15Zr) alloy. This article presents microstructure and some of the corrosion studies being conducted on the waste form alloys. Electrochemical corrosion, immersion corrosion, and vapor hydration tests have been performed on various alloy compositions to evaluate corrosion behavior and resistance to selective leaching of simulated fission products. The SS-Zr waste forms are successful at the immobilization and retention of fission products and show potential for acceptance as high-level nuclear waste forms.

  1. Effects of solutes on damage production and recovery in zirconium

    SciTech Connect

    Zee, R.H.; Birtcher, R.C.; MacEwen, S.R.; Abromeit, C.

    1986-04-01

    Dilute zirconium-based alloys and pure zirconium were irradiated at 10 K with spallation neutrons at IPNS. Four types of alloys - Zr-Ti, Zr-Sn, Zr-Dy and Zr-Au - each with three concentration levels, were used. Low-temperature resistivity damage rates are enhanced by the presence of any of the four solutes. The greatest enhancement was produced by Au while the least by Dy. Within each alloy group, damage production also increased but at a decreasing rate, with increasing concentration. Post-irradiation annealing experiments, up to 400 K, showed that all four solutes suppress recovery due to interstitial migration, indicative of interstitial trapping by the solutes. Vacancy recovery is also suppressed by the presence of Sn, Dy or Au. The effect of Ti is to shift this stage to lower temperature. No clear correlation between the results with solute size was detected.

  2. Asymmetric induction in the zirconium catalyzed ethylmagnesiation reaction

    SciTech Connect

    Bell, J.L.; Whitby, R.J.; Jones, R.V.H.

    1995-12-31

    In 1985 Dzhemilev reported the zirconium catalysed ethylmagnesiation of terminal alkenes. A chiral centre is formed during the reaction which occurs under mild conditions. The authors have applied this reaction to a number of substrates and a mechanism has been elucidated. In order to induce asymmetry into the reaction, several chiral literature catalysts were synthesised including Ethylenebis(tetrahydroindenyl)zirconium dichloride and two more hindered complexes reported by Erker. All of these catalysts displayed low activity and poor asymmetric induction with terminal alkenes. The synthesis and properties of two novel catalysts will be described. Results show high activity furnishing carbomagnesiated products in excellent yields with as little as 2 mol% catalyst. The enantiomeric excesses induced by the complexes are as high as 79% with terminal alkenes but are >95% with cyclic ethers. The catalyst has proved recoverable. Ethylmagnesiation of an amine followed by an acidic workup furnishes the chiral complex in a quantitative return.

  3. Alternative Processing of High Temperature Hafnium and Zirconium Based Materials

    NASA Technical Reports Server (NTRS)

    Gasch, Matthew; Gusman, Michael; Ellerby, Don; Irby, Edward; Johnson, Sylvia M.

    2003-01-01

    The behavior of refractory hafnium and zirconium based materials are being investigated at NASA Ames as part of ongoing research aimed at developing superior heat resistant materials for aerospace applications. Hafnium and zirconium diboride based materials have shown high temperature capabilities in simulated reentry environments indicating that these materials may successfully operate as reusable oxidation resistant components for leading edge applications. Due to the refractory nature of these materials, processing of fine-grained uniform microstructures poses a number of challenges. To better understand the process-property-microstructure relationship, processing of these materials has been carried out with conventional hot pressing in addition to the novel approach of Spark Plasma Sintering (SPS). The two processing methods are compared and contrasted in an evaluation of the sintering behavior of high temperature diboride based materials and preliminary physical and mechanical properties are presented.

  4. Properties of Alloys of Zirconium and Niobium Carbides in Their Homogeneity Domain,

    DTIC Science & Technology

    ZIRCONIUM COMPOUNDS, ELECTRICAL PROPERTIES), (*NIOBIUM COMPOUNDS, ELECTRICAL PROPERTIES), (*REFRACTORY MATERIALS, CARBIDES), ELECTRICAL RESISTANCE, HALL EFFECT, MAGNETIC PROPERTIES, THERMAL PROPERTIES, SEEBECK EFFECT , USSR

  5. SEPARATION OF PLUTONIUM IONS FROM SOLUTION BY ADSORPTION ON ZIRCONIUM PYROPHOSPHATE

    DOEpatents

    Stoughton, R.W.

    1961-01-31

    A method is given for separating plutonium in its reduced, phosphate- insoluble state from other substances. It involves contacting a solution containing the plutonium with granular zirconium pyrophosphate.

  6. Removal of zirconium from aqueous solution by modified clinoptilolite.

    PubMed

    Faghihian, H; Kabiri-Tadi, M

    2010-06-15

    Adsorptive behavior of natural clinoptilolite was assessed for the removal of zirconium from aqueous solutions. Natural zeolite was characterized by X-ray diffraction, X-ray fluorescence, thermal methods of analysis and FTIR. The zeolite sample composed mainly of clinoptilolite and presented a cation exchange capacity of 1.46 meq g(-1). K, Na and Ca-exchanged forms of zeolite were prepared and their sorption capacities for removal of zirconium from aqueous solutions were determined. The effects of relevant parameters, including initial concentration, contact time, temperature and initial pH on the removal efficiency were investigated in batch studies. The pH strongly influenced zirconium adsorption capacity and maximal capacity was obtained at pH 1.0. The maximum removal efficiency obtained at 40 degrees C and equilibration time of 24h on the Ca-exchanged form. Kinetics and isotherm of adsorption were also studied. The pseudo-first-order, pseudo-second-order, Elovich and intra-particle diffusion models were used to describe the kinetic data. The pseudo-second-order kinetic model provided excellent kinetic data fitting (R(2)>0.998) with rate constant of 1.60x10(-1), 1.96x10(-1), 2.45x10(-1) and 2.02x10(-1)g mmol(-1)min(-1) respectively for Na, K, Ca-exchanged forms and natural clinoptilolite. The Langmuir and Freundlich models were applied to describe the equilibrium isotherms for zirconium uptake and the Langmuir model agrees very well with experimental data. Thermodynamic parameters were determined and are discussed.

  7. Zirconium as a Structural Material for Naval Systems

    DTIC Science & Technology

    2010-08-12

    structural metals with the exception of titanium , vandium, and niobium . Fabrication of all zirconiumi structures or the lining of other metals with...molten magnesium or sodium to yield a spongy form of the free metal containing up to three percent hafnium. It resembles titanium and hafnium...including some comparisons with other common structural metals. From the table we learn that the density of zirconium is intermediate between titanium and

  8. Distribution coefficients of rare earth ions in cubic zirconium dioxide

    NASA Astrophysics Data System (ADS)

    Romer, H.; Luther, K.-D.; Assmus, W.

    1994-08-01

    Cubic zirconium dioxide crystals are grown with the skull melting technique. The effective distribution coefficients for Nd(exp 3+), Sm(exp 3+) and Er(sup 3+) as dopants are determined experimentally as a function of the crystal growth velocity. With the Burton-Prim-Slichter theory, the equilibrium distribution coefficients can be calculated. The distribution coefficients of all other trivalent rare earth ions can be estimated by applying the correlation towards the ionic radii.

  9. Electrochemical Study of Corrosion Phenomena in Zirconium Alloys

    DTIC Science & Technology

    2005-06-01

    determined that there are large ECP differences associated with Inconel and zirconium alloys that correlate to increased galvanic current density when the...Pt-Pt, Zircaloy 2 (Zr-2)-Pt, Inconel (X-750)-Pt, and Zr- 2-X-750. To determine the changes in the coolant water conductivity due to the presence of...of fuel cladding integrity during accident scenarios. The limitation on acceptance criteria, in accordance with 10 CFR 50.46(b) is that the maximum

  10. Oxidation characteristics of molybdenum-zirconium oxide cermets

    NASA Technical Reports Server (NTRS)

    Heitzinger, B.

    1984-01-01

    The oxidation of molybdenum is affected by the factors of temperature, the oxygen pressure in the oxidizing atmosphere, and the time of exposure. Studies of the oxidation characteristics of Mo show that the oxidation rate increases strongly when the temperature exceeds 600 C. Investigations of the behavior of cermets with various percentages of zirconium oxide are discussed, taking into account oxidation conditions at temperatures under and above the melting point of molybdenum trioxide.

  11. Polyimide nanocomposites based on cubic zirconium tungstate

    NASA Astrophysics Data System (ADS)

    Ramasubramanian Sharma, Gayathri

    2009-12-01

    In this research, cubic zirconium tungstate (ZrW2O8) was used as a filler to reduce the CTE of polyimides (PI), and the effect of ZrW2O8 nanoparticles on the bulk polymer properties was studied. Polyimides are high performance polymers with exceptional thermal stability, and there is a need for PIs with low CTEs for high temperature applications. The nanofiller, cubic ZrW2O8, is well known for its isotropic negative thermal expansion (NTE) over a wide temperature range from -272.7 to 777°C. The preparation of nanocomposites involved the synthesis of ZrW 2O8 nanofiller, engineering the polymer-filler interface using linker groups and optimization of processing strategies to prepare free-standing PI nanocomposite films. A hydrothermal method was used to synthesize ZrW 2O8 nanoparticles. Polyimide-ZrW2O8 interface interaction was enhanced by covalently bonding linker moieties to the surface of ZrW2O8 nanoparticles. Specifically, ZrW 2O8 nanoparticles were functionalized with two different linker groups: (1) a short aliphatic silane, and (2) low molecular weight PI. The surface functionalization was confirmed using X-ray photoelectron spectroscopy and thermal gravimetric analysis (TGA). Reprecipitation blending was used to prepare the freestanding PI-ZrW2O8 nanocomposite films with up to 15 volume% filler loading. SEM images showed the improvements in polymer-filler wetting behavior achieved using interface engineering. SEM images indicated that there was better filler dispersion in the PI matrix using reprecipitation blending, compared to the filler dispersion achieved in the nanocomposites prepared using conventional blending technique. The structure-property relationships in PI-ZrW2O8 nanocomposites were investigated by studying the thermal degradation, glass transition, tensile and thermal expansion properties of the nanocomposites. The properties were studied as a function of filler loading and interface linker groups. Addition of ZrW2O8 nanoparticles did not

  12. Continuous ion exchange separation of zirconium and hafnium

    SciTech Connect

    Begovich, J.M.; Sisson, W.G.

    1981-01-01

    A pressurized continuous annular chromatograph (CAC) has been developed for truly continuous ion exchange preparative separations. This device utilizes a slowly rotating annular bed of sorbent material, fixed multiple feed points, and fixed withdrawal locations. Most of our investigations have been performed with a 28-cm-diam by 60-cm-long CAC, but a larger model has recently been designed and constructed. A detailed study has been made of the separation of copper, nickel, and cobalt components from a simulated carbonate leach liquor of the Caron process for recovering nickel and cobalt from laterite ores. Recent studies have investigated the ion exchange separation of zirconium and hafnium from a sulfate feed solution. Nuclear reactor-grade zirconium, containing < 0.01 wt % hafnium, and hafnium, containing < 1% zirconium, have been continuously prepared using cation exchange resin in the pressurized CAC. This device, because of its continuous feed and product withdrawal, its adaptability to largescale operations, and its ability to separate many components, is expected to make chromatography a more competitive process in the industrial sector.

  13. Laves intermetallics in stainless steel-zirconium alloys

    SciTech Connect

    Abraham, D.P.; McDeavitt, S.M.; Richardson, J.W. Jr.

    1997-05-01

    Laves intermetallics have a significant effect on properties of metal waste forms being developed at Argonne National Laboratory. These waste forms are stainless steel-zirconium alloys that will contain radioactive metal isotopes isolated from spent nuclear fuel by electrometallurgical treatment. The baseline waste form composition for stainless steel-clad fuels is stainless steel-15 wt.% zirconium (SS-15Zr). This article presents results of neutron diffraction measurements, heat-treatment studies and mechanical testing on SS-15Zr alloys. The Laves intermetallics in these alloys, labeled Zr(Fe,Cr,Ni){sub 2+x}, have both C36 and C15 crystal structures. A fraction of these intermetallics transform into (Fe,Cr,Ni){sub 23}Zr{sub 6} during high-temperature annealing; the authors have proposed a mechanism for this transformation. The SS-15Zr alloys show virtually no elongation in uniaxial tension, but exhibit good strength and ductility in compression tests. This article also presents neutron diffraction and microstructural data for a stainless steel-42 wt.% zirconium (SS-42Zr) alloy.

  14. Ferrier rearrangement promoted by an electrochemically generated zirconium catalyst.

    PubMed

    Stevanović, Dragana; Pejović, Anka; Damljanović, Ivan; Minić, Aleksandra; Bogdanović, Goran A; Vukićević, Mirjana; Radulović, Niko S; Vukićević, Rastko D

    2015-04-30

    In situ generated zirconium catalyst from a sacrificial zirconium anode was successfully applied to promote Ferrier rearrangement of 3,4,5-tri-O-acetyl-D-glucal and 6-deoxy-3,4-di-O-acetyl-L-glucal (3,4-di-O-acetyl-L-rhamnal) in the presence of three thiols and eleven thiophenols as nucleophiles. A simple constant current electrolysis (20 mA, 0.4 F mol(-1)) of an acetonitrile solution of lithium perchlorate (0.1 M) containing the corresponding glycal and S-nucleophiles, using a zirconium anode and a platinum cathode resulted in the successful synthesis of the corresponding 2,3-unsaturated peracetylated thioglycosides (with an average anomer ratio α/β=4.129 in the case of peracetylated D-glucal and 8.740 in the case of L-rhamnal). The same procedure proved to be appropriate in synthesizing dihydropyran derivatives ('C-glycosides') using allyltrimethylsilane as the nucleophile (only 'α-anomers' were obtained). All new compounds were fully characterized by spectral data, whereas single-crystal X-ray analysis was performed for two thioglycosides.

  15. Thermodynamic and kinetic studies of As(V) removal from water by zirconium oxide-coated marine sand.

    PubMed

    Khan, Tabrez Alam; Chaudhry, Saif Ali; Ali, Imran

    2013-08-01

    Arsenic contamination of groundwater is a major threat to human beings globally. Among various methods available for arsenic removal, adsorption is fast, inexpensive, selective, accurate, reproducible and eco-friendly in nature. The present paper describes removal of arsenate from water on zirconium oxide-coated sand (novel adsorbent). In the present work, zirconium oxide-coated sand was prepared and characterised by infrared and X-ray diffraction techniques. Batch experiments were performed to optimise different adsorption parameters such as initial arsenate concentration (100-1,000 μg/L), dose (1-8 g/L), pH of the solution (2-14), contact time (15-150 min.), and temperature (20, 30, 35 and 40 °C). The experimental data were analysed by Langmuir, Freundlich, Temkin and Dubinin-Radushkevich isotherm models. Furthermore, thermodynamic and kinetic parameters were evaluated to know the mode of adsorption between ZrOCMS and As(V). The maximum removal of arsenic, 97 %, was achieved at initial arsenic concentration of 200 μg/L, after 75 min at dosage of 5.0 g/L, pH 7.0 and 27 ± 2 °C. For 600 μg/L concentration, the maximum Langmuir monolayer adsorption capacity was found to be 270 μg/g at 35 °C. Kinetic modelling data indicated that adsorption process followed pseudo-second-order kinetics. The mechanism is controlled by liquid film diffusion model. Thermodynamic parameter, ΔH°, was -57.782, while the values of ΔG° were -9.460, -12.183, -13.343 and -13.905 kJ/mol at 20, 30, 35 and 40 °C, respectively, suggesting exothermic and spontaneous nature of the process. The change in entropy, ΔS°= -0.23 kJ/mol indicated that the entropy decreased due to adsorption of arsenate ion onto the solid adsorbent. The results indicated that the reported zirconium oxide-coated marine sand (ZrOCMS) was good adsorbent with 97 % removal capacity at 200 μg/L concentration. It is interesting to note that the permissible limit of arsenic as per World Health Organization is 10

  16. A zirconium-based nanoparticle: essential factors for sustainable application in treatment of fluoride containing water.

    PubMed

    He, Jinsong; Chen, J Paul

    2014-02-15

    Excessive intake of fluoride can cause a severe threat on human beings. In this study, a zirconium-based nano-particles (NPs) was synthesized for effective defluoridation from aqueous solution. The pH effect, adsorption kinetics, adsorption isotherms, and effect of co-existing substances on the fluoride uptake were investigated. The results showed that the sorbent had a high adsorption capacity for fluoride within a wide pH ranging from 3 to 10. The optimal pH for the adsorption was around 4. The study of adsorption kinetics revealed that most uptake of fluoride occurred in the first 1h, and the adsorption equilibrium was established within 4h. Langmuir equation well described the adsorption isotherm data; the maximum adsorption capacities of 97.48 and 78.56 mg/g were found at optimal pH and neutral pH, respectively. The presence of PO4(3-), NO3(-) and natural organic matters did not significantly inhibit the fluoride removal. However, both HCO3(-) and SiO2(3-) retarded the removal. The regeneration revealed that the sorbent possessed a high reusability for defluoridation. The intraparticle surface diffusion model well described the adsorption kinetics. The FTIR and XPS analysis demonstrated that the adsorption of fluoride was mainly associated with the ion-exchange between sulfate and fluoride ions.

  17. 27 CFR 25.97 - Continuation certificate.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ..., DEPARTMENT OF THE TREASURY LIQUORS BEER Bonds and Consents of Surety § 25.97 Continuation certificate. If the... of law and regulations applicable to bonds on Form 5130.22 given under this part, including...

  18. 27 CFR 25.97 - Continuation certificate.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ..., DEPARTMENT OF THE TREASURY LIQUORS BEER Bonds and Consents of Surety § 25.97 Continuation certificate. If the... of law and regulations applicable to bonds on Form 5130.22 given under this part, including...

  19. 27 CFR 25.97 - Continuation certificate.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ..., DEPARTMENT OF THE TREASURY LIQUORS BEER Bonds and Consents of Surety § 25.97 Continuation certificate. If the... of law and regulations applicable to bonds on Form 5130.22 given under this part, including...

  20. 27 CFR 25.97 - Continuation certificate.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ..., DEPARTMENT OF THE TREASURY ALCOHOL BEER Bonds and Consents of Surety § 25.97 Continuation certificate. If the... of law and regulations applicable to bonds on Form 5130.22 given under this part, including...

  1. 27 CFR 25.97 - Continuation certificate.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ..., DEPARTMENT OF THE TREASURY ALCOHOL BEER Bonds and Consents of Surety § 25.97 Continuation certificate. If the... of law and regulations applicable to bonds on Form 5130.22 given under this part, including...

  2. 7 CFR 97.153 - Persons recognized.

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ..., Inspections, Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS... authorized as provided in § 97.151, no person shall be permitted to file or advance applications before...

  3. 14 CFR 33.97 - Thrust reversers.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Block Tests; Turbine Aircraft Engines § 33.97 Thrust reversers. (a) If the engine incorporates a reverser, the endurance calibration, operation, and vibration tests prescribed...

  4. Graphs for Isotopes of 97-Bk (Berkelium)

    NASA Astrophysics Data System (ADS)

    Sukhoruchkin, S. I.; Soroko, Z. N.

    This document is part of the Supplement containing the complete sets of data of Subvolume B `Nuclei with Z = 55 - 100' of Volume 22 `Nuclear Binding Energies and Atomic Masses' of Landolt-Börnstein - Group I `Elementary Particles, Nuclei and Atoms', and additionally including data for nuclei with Z = 101 - 130. It provides a graphic representation of nucleon separation energies and residual interaction parameters for isotopes of the chemical element 97-Bk (Berkelium, atomic number Z = 97).

  5. 40 CFR 721.10152 - Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica...

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ...-, hydrolysis products with alkanol zirconium(4+) salt and silica, acetates (generic). 721.10152 Section 721... Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica... zirconium(4+) salt and silica, acetates (PMN P-07-674) is subject to reporting under this section for...

  6. 40 CFR 721.10152 - Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica...

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ...-, hydrolysis products with alkanol zirconium(4+) salt and silica, acetates (generic). 721.10152 Section 721... Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica... zirconium(4+) salt and silica, acetates (PMN P-07-674) is subject to reporting under this section for...

  7. 40 CFR 721.10152 - Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica...

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ...-, hydrolysis products with alkanol zirconium(4+) salt and silica, acetates (generic). 721.10152 Section 721... Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica... zirconium(4+) salt and silica, acetates (PMN P-07-674) is subject to reporting under this section for...

  8. 40 CFR 721.10152 - Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica...

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ...-, hydrolysis products with alkanol zirconium(4+) salt and silica, acetates (generic). 721.10152 Section 721... Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica... zirconium(4+) salt and silica, acetates (PMN P-07-674) is subject to reporting under this section for...

  9. 40 CFR 721.10152 - Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica...

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ...-, hydrolysis products with alkanol zirconium(4+) salt and silica, acetates (generic). 721.10152 Section 721... Oxirane, substituted silylmethyl-, hydrolysis products with alkanol zirconium(4+) salt and silica... zirconium(4+) salt and silica, acetates (PMN P-07-674) is subject to reporting under this section for...

  10. Lithium aluminate/zirconium material useful in the production of tritium

    DOEpatents

    Cawley, William E.; Trapp, Turner J.

    1984-10-09

    A composition is described useful in the production of tritium in a nuclear eactor. Lithium aluminate particles are dispersed in a matrix of zirconium. Tritium produced by the reactor of neutrons with the lithium are absorbed by the zirconium, thereby decreasing gas pressure within capsules carrying the material.

  11. Lithium aluminate/zirconium material useful in the production of tritium

    DOEpatents

    Cawley, W.E.; Trapp, T.J.

    1984-10-09

    A composition is described useful in the production of tritium in a nuclear reactor. Lithium aluminate particles are dispersed in a matrix of zirconium. Tritium produced by the reactor of neutrons with the lithium are absorbed by the zirconium, thereby decreasing gas pressure within capsules carrying the material.

  12. Lithium aluminate/zirconium material useful in the production of tritium

    DOEpatents

    Cawley, W.E.; Trapp, T.J.

    A composition is described useful in the production of tritium in a nuclear reactor. Lithium aluminate particles are dispersed in a matrix of zirconium. Tritium produced by the reactor of neutrons with the lithium are absorbed by the zirconium, thereby decreasing gas pressure within capsules carrying the material.

  13. Zirconium carbide as an electrocatalyst for the chromous-chromic redox couple

    NASA Technical Reports Server (NTRS)

    Gahn, R. F.; Reid, M. A.; Yang, C. Y. (Inventor)

    1981-01-01

    Zirconium carbide is used as a catalyst in a REDOX cell for the oxidation of chromous ions to chromic ions and for the reduction of chromic ions to chromous ions. The zirconium carbide is coated on an inert electronically conductive electrode which is present in the anode fluid of the cell.

  14. Fused salt process for purifying zirconium and/or hafnium tetrachlorides

    SciTech Connect

    Lee, E.D.

    1991-04-23

    This patent describes a fused salt process for continuously purifying zirconium and/or hafnium tetrachloride dissolved in a molten bath in a vessel. It comprises: maintaining a mass of a suitable mixture of salts, including zirconium and/or hafnium tetrachloride; heating the mixture of salts to a temperature at or immediately below the vaporization temperature of the zirconium and/or hafnium tetrachloride at which temperature the mixture of salts is fused to form a molten, tetrachloride-dissolving bath; continuously introducing into the dissolving bath a zirconium and/or hafnium tetrachloride powder; heating a portion of the dissolving bath in situ to a temperature higher than the vaporization temperature of the zirconium and/or hafnium tetrachloride so as to vaporize the tetrachloride; internally circulating the dissolving bath whereby the portion of the dissolving bath at the high temperature circulate with the bath at the lower temperature.

  15. A simple spectrophotometric method for determination of zirconium or hafnium in selected molybdenum-base alloys

    NASA Technical Reports Server (NTRS)

    Dupraw, W. A.

    1972-01-01

    A simple analytical procedure is described for accurately and precisely determining the zirconium or hafnium content of molybdenum-base alloys. The procedure is based on the reaction of the reagent Arsenazo III with zirconium or hafnium in strong hydrochloric acid solution. The colored complexes of zirconium or hafnium are formed in the presence of molybdenum. Titanium or rhenium in the alloy have no adverse effect on the zirconium or hafnium complex at the following levels in the selected aliquot: Mo, 10 mg; Re, 10 mg; Ti, 1 mg. The spectrophotometric measurement of the zirconium or hafnium complex is accomplished without prior separation with a relative standard deviation of 1.3 to 2.7 percent.

  16. Preparation and properties of uniform mixed and coated colloidal particles. Part 5. Zirconium compounds

    SciTech Connect

    Alken, B.; Hsu, W.P.; Matijevic, E.

    1990-01-01

    Colloidal dispersions of uniform spherical particles by zirconium basic sulphate and zirconium oxy-basic carbonate were prepared by ageing zirconium sulphate solutions at elevated temperatures in the presence of urea. Different chemical compositions of the above products resulted when the ageing temperature was altered. Depending on the nature of the original solids, calcination at 800 C resulted in the formation of tetragonal or monoclinic zirconia. Under certain conditions a mixed phase, including cubic zirconia, has also been identified. The particle morphology was retained during these transformations. Coprecipitation in mixed solutions of zirconium and yttrium salts aged at 80 C yielded composite spherical particles of basic carbonate with a zirconium to yttrium ratio of the solid similar to that used in the initial solution.

  17. Efficient One-Pot Synthesis of Colloidal Zirconium Oxide Nanoparticles for High-Refractive-Index Nanocomposites.

    PubMed

    Liu, Chao; Hajagos, Tibor Jacob; Chen, Dustin; Chen, Yi; Kishpaugh, David; Pei, Qibing

    2016-02-01

    Zirconium oxide nanoparticles are promising candidates for optical engineering, photocatalysis, and high-κ dielectrics. However, reported synthetic methods for the colloidal zirconium oxide nanoparticles use unstable alkoxide precursors and have various other drawbacks, limiting their wide application. Here, we report a facile one-pot method for the synthesis of colloidally stable zirconium oxide nanoparticles. Using a simple solution of zirconium trifluoroacetate in oleylamine, highly stable zirconium oxide nanoparticles have been synthesized with high yield, following a proposed amidization-assisted sol-gel mechanism. The nanoparticles can be readily dispersed in nonpolar solvents, forming a long-term stable transparent solution, which can be further used to fabricate high-refractive-index nanocomposites in both monolith and thin-film forms. In addition, the same method has also been extended to the synthesis of titanium oxide nanoparticles, demonstrating its general applicability to all group IVB metal oxide nanoparticles.

  18. Inhibitors of the AAA+ Chaperone p97

    PubMed Central

    Chapman, Eli; Maksim, Nick; de la Cruz, Fabian; La Clair, James J.

    2015-01-01

    It is remarkable that a pathway as ubiquitous as protein quality control can be targeted to treat cancer. Bortezomib, an inhibitor of the proteasome, was first approved by the US Food and Drug Administration (FDA) more than 10 years ago to treat refractory myeloma and later extended to lymphoma. Its use has increased the survival rate of myeloma patients by as much as three years. This success was followed with the recent accelerated approval of the natural product derived proteasome inhibitor carfilzomib (Kyprolis®), which is used to treat patients with bortezomib-resistant multiple myeloma. The success of these two drugs has validated protein quality control as a viable target to fight select cancers, but begs the question why are proteasome inhibitors limited to lymphoma and myeloma? More recently, these limitations have encouraged the search for additional targets within the protein quality control system that might offer heightened cancer cell specificity, enhanced clinical utility, a lower rate of resistance, reduced toxicity, and mitigated side effects. One promising target is p97, an ATPase associated with various cellular activities (AAA+) chaperone. p97 figures prominently in protein quality control as well as serving a variety of other cellular functions associated with cancer. More than a decade ago, it was determined that up-regulation of p97 in many forms of cancer correlates with a poor clinical outcome. Since these initial discoveries, a mechanistic explanation for this observation has been partially illuminated, but details are lacking. Understandably, given this clinical correlation, myriad roles within the cell, and its importance in protein quality control, p97 has emerged as a potential therapeutic target. This review provides an overview of efforts towards the discovery of small molecule inhibitors of p97, offering a synopsis of efforts that parallel the excellent reviews that currently exist on p97 structure, function, and physiology. PMID

  19. Zirconium(IV) dilanthanum(III) penta­sulfide

    PubMed Central

    Raw, Adam D.; Ibers, James A.

    2011-01-01

    Zirconium(IV) dilanthanum(III) penta­sulfide, ZrLa2S5, crystallizes with four formula units in the space group Pnma in the U3S5 structure type. The asymmetric unit comprises one Zr, one La and four S atoms. The Zr and three S atoms are situated on mirror planes. The structure consists of LaS8 face-sharing bicapped distorted trigonal prisms and ZrS7 edge-sharing monocapped octa­hedra. PMID:22199468

  20. The abundances of zirconium and hafnium in the solar system

    NASA Technical Reports Server (NTRS)

    Ganapathy, R.; Papia, G. M.; Grossman, L.

    1976-01-01

    The concentrations of zirconium and hafnium have been determined in the Orgueil, Murchison, Allende, Bruderheim, and Alais meteorites by radiochemical neutron activation analysis. The mean Zr/Hf weight ratio in the first four of these meteorites is 31.3 (plus or minus 2.2), indicating no major fractionation of Zr from Hf. Alais contains anomalously high amounts of many refractory lithophile elements, including Zr and Hf. Orgueil contains 3.1 ppm Zr and 0.11 ppm Hf, corresponding to 9.0 and 0.16 atoms, respectively, relative to 1 million Si atoms.

  1. Plasma sprayed and electrospark deposited zirconium metal diffusion barrier coatings

    SciTech Connect

    Hollis, Kendall J; Pena, Maria I

    2010-01-01

    Zirconium metal coatings applied by plasma spraying and electrospark deposition (ESD) have been investigated for use as diffusion barrier coatings on low enrichment uranium fuel for research nuclear reactors. The coatings have been applied to both stainless steel as a surrogate and to simulated nuclear fuel uranium-molybdenum alloy substrates. Deposition parameter development accompanied by coating characterization has been performed. The structure of the plasma sprayed coating was shown to vary with transferred arc current during deposition. The structure of ESD coatings was shown to vary with the capacitance of the deposition equipment.

  2. METHOD FOR ANNEALING AND ROLLING ZIRCONIUM-BASE ALLOYS

    DOEpatents

    Picklesimer, M.L.

    1959-07-14

    A fabrication procedure is presented for alpha-stabilized zirconium-base alloys, and in particular Zircaloy-2. The alloy is initially worked at a temperature outside the alpha-plus-beta range (810 to 970 deg ), held at a temperature above 970 deg C for 30 minutes and cooled rapidly. The alloy is then cold-worked to reduce the size at least 20% and annealed at a temperature from 700 to 810 deg C. This procedure serves both to prevent the formation of stringers and to provide a randomly oriented crystal structure.

  3. Mechanical Properties of Continuous Fiber Reinforced Zirconium Diboride Matrix Composites

    NASA Technical Reports Server (NTRS)

    Stuffle, Kevin; Creegan, Peter; Nowell, Steven; Bull, Jeffrey D.; Rasky, Daniel J. (Technical Monitor)

    1995-01-01

    Continuous fiber reinforced zirconium diboride matrix composites, SCS-9a-(RBSiCZrB2)matrix, are being developed for leading edge, rocket nozzle and turbine engine applications. Recently, the composite materials have been characterized for tensile properties to 1250 C, the highest temperature tested. The tensile properties are fiber dominated as the matrix is microcracked on fabrication, but favorable failure characteristic are observed. Compression and shear mechanical testing results will be reported if completed. The effects of fiber volume fraction and matrix density on mechanical properties will be discussed. The target applications of the materials will be discussed. Specific testing being performed towards qualification for these applications will be included.

  4. Unexpected wear of an unicompartimental knee arthroplasty in oxidized zirconium.

    PubMed

    Luyet, Anais; Fischer, Jean-François; Jolles, Brigitte M; Lunebourg, Alexandre

    2015-12-01

    Unicompartimental knee arthroplasty is a successful procedure for the treatment of localized osteoarthritis to one compartment of the knee with good long-term results. However, several modes of failure of unicompartimental knee arthroplasty have been described, namely aseptic or septic loosening, progression of disease, wear, and instability. Metallosis after unicompartimental knee arthroplasty is rarely reported and is most often related with polyethylene wear or break. We report on a case of rapid failure of unicompartimental knee arthroplasty in oxidized zirconium associated with metallosis secondary to the dislocation of the polyethylene.

  5. 47 CFR 97.121 - Restricted operation.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.121 Restricted operation. (a) If the operation of an amateur... characteristics, are used to receive such transmissions, and this fact is made known to the amateur...

  6. 47 CFR 97.121 - Restricted operation.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.121 Restricted operation. (a) If the operation of an amateur... characteristics, are used to receive such transmissions, and this fact is made known to the amateur...

  7. 47 CFR 97.201 - Auxiliary station.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.201 Auxiliary station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be an auxiliary station. A...

  8. 47 CFR 97.201 - Auxiliary station.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.201 Auxiliary station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be an auxiliary station. A...

  9. 47 CFR 97.121 - Restricted operation.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.121 Restricted operation. (a) If the operation of an amateur... characteristics, are used to receive such transmissions, and this fact is made known to the amateur...

  10. 47 CFR 97.201 - Auxiliary station.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.201 Auxiliary station. (a) Any amateur station licensed to a holder of a Technician, Technician Plus, General, Advanced or Amateur Extra Class operator license may be an...

  11. 47 CFR 97.121 - Restricted operation.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.121 Restricted operation. (a) If the operation of an amateur... characteristics, are used to receive such transmissions, and this fact is made known to the amateur...

  12. 47 CFR 97.201 - Auxiliary station.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.201 Auxiliary station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be an auxiliary station. A...

  13. 47 CFR 97.121 - Restricted operation.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Station Operation Standards § 97.121 Restricted operation. (a) If the operation of an amateur... characteristics, are used to receive such transmissions, and this fact is made known to the amateur...

  14. 47 CFR 97.201 - Auxiliary station.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... Telecommunication FEDERAL COMMUNICATIONS COMMISSION (CONTINUED) SAFETY AND SPECIAL RADIO SERVICES AMATEUR RADIO SERVICE Special Operations § 97.201 Auxiliary station. (a) Any amateur station licensed to a holder of a Technician, General, Advanced or Amateur Extra Class operator license may be an auxiliary station. A...

  15. 7 CFR 97.1 - General.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ..., Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS PLANT VARIETY AND PROTECTION Scope § 97.1 General. Certificates of protection are issued by the Plant Variety... plants. Each certificate of plant variety protection certifies that the breeder has the right, during...

  16. 7 CFR 97.1 - General.

    Code of Federal Regulations, 2011 CFR

    2011-01-01

    ..., Marketing Practices), DEPARTMENT OF AGRICULTURE (CONTINUED) COMMODITY LABORATORY TESTING PROGRAMS PLANT VARIETY AND PROTECTION Scope § 97.1 General. Certificates of protection are issued by the Plant Variety... plants. Each certificate of plant variety protection certifies that the breeder has the right, during...

  17. 40 CFR 97.70 - General requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... with such requirements, the definitions in § 97.2 and in § 72.2 of this chapter shall apply, and the... monitor NOX emission rate, NOX concentration, heat input rate, and stack flow rate, in accordance with §§ 75.71 and 75.72 of this chapter. (2) Install all monitoring systems for monitoring heat input...

  18. 40 CFR 97.370 - General requirements.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... with such requirements, the definitions in § 97.302 and in § 72.2 of this chapter shall apply, and the... unit heat input (including all systems required to monitor NOX emission rate, NOX concentration, stack... required to determine NOX mass emissions and heat input in accordance with § 75.31(b)(2) or (c)(3) of...

  19. 47 CFR 97.113 - Prohibited transmissions.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... station, except an auxiliary, repeater, or space station, may automatically retransmit the radio signals... SERVICE Station Operation Standards § 97.113 Prohibited transmissions. (a) No amateur station shall... rules; (3) Communications in which the station licensee or control operator has a pecuniary...

  20. 47 CFR 97.113 - Prohibited transmissions.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... station, except an auxiliary, repeater, or space station, may automatically retransmit the radio signals... SERVICE Station Operation Standards § 97.113 Prohibited transmissions. (a) No amateur station shall... rules; (3) Communications in which the station licensee or control operator has a pecuniary...